WO2003008517A1 - Composition pour sol contenant des dechets industriels comme composant principal - Google Patents

Composition pour sol contenant des dechets industriels comme composant principal Download PDF

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Publication number
WO2003008517A1
WO2003008517A1 PCT/JP2002/007294 JP0207294W WO03008517A1 WO 2003008517 A1 WO2003008517 A1 WO 2003008517A1 JP 0207294 W JP0207294 W JP 0207294W WO 03008517 A1 WO03008517 A1 WO 03008517A1
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WO
WIPO (PCT)
Prior art keywords
composition
soil
fly ash
diatomaceous earth
zeolite
Prior art date
Application number
PCT/JP2002/007294
Other languages
English (en)
Japanese (ja)
Inventor
Kyungsik Kang
Kaneyoshi Nakashima
Original Assignee
Columbus Corporation Co., Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Columbus Corporation Co., Ltd. filed Critical Columbus Corporation Co., Ltd.
Publication of WO2003008517A1 publication Critical patent/WO2003008517A1/fr

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K17/00—Soil-conditioning materials or soil-stabilising materials
    • C09K17/40—Soil-conditioning materials or soil-stabilising materials containing mixtures of inorganic and organic compounds
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F7/00—Fertilisers from waste water, sewage sludge, sea slime, ooze or similar masses
    • C05F7/02—Fertilisers from waste water, sewage sludge, sea slime, ooze or similar masses from sulfite liquor or other waste lyes from the manufacture of cellulose

Definitions

  • the present invention relates to a novel soil composition and a method for producing it. More specifically, the present invention relates to a novel soil composition mainly composed of industrial waste and a method for producing the same. And its uses relate to soil conditioners, soil moisture regulators, garbage treatment agents, manure treatment agents, putrefaction agents, fertilizer raw materials, dehumidifiers or deodorants. Background art
  • Korean Patent Publication No. 98-63340 discloses an invention of a method of using fly ash (Fly ash) for fertilizing a strongly acidic amino acid fermentation waste liquid generated in a seasoning plant.
  • Fly ash fly ash
  • An object of the present invention is to improve the above disadvantages despite the advantages of a major Korean patent having the above-mentioned general soil improvement and moisture control effects.
  • it can be used as a fertilizer raw material at any stage of crop growth.
  • Soil types can be used not only in general paddy soil, but also in large plastic greenhouse complexes with a large amount of salt accumulation and soil in general fruit orchard fields. Irrespective of the growth stage of the plant or cultivated crop, it is used regularly at any time to maximize the effect as a soil composition and significantly promote crop growth. It is an object of the present invention to provide a new soil composition mainly composed of industrial waste, which can be developed.
  • Another object of the present invention is to provide a soil conditioner, a soil moisture control agent, a garbage treatment agent, a manure treatment agent, a septic treatment agent, a fertilizer raw material, a dehumidifier or a deodorant using the soil composition. Is to provide a method of manufacturing the same. Further, other objects of the present invention will become apparent from the following detailed description.
  • the object of the present invention is to select inorganic materials from industrial waste, determine the composition ratio thereof, produce a desired soil composition, and then use the soil composition of the present invention to produce various crops. This was achieved by applying the method to cultivation and evaluating the results of growth experiments, or by applying the method to garbage, manure, putrefaction, etc., and evaluating its water regulation ability, deodorization ability, and dehumidification ability.
  • the present invention includes the following inventions.
  • composition for soil characterized by the following.
  • the present invention provides a step of selecting an inorganic material excellent as a soil improvement, deodorizing effect, moisture control effect, fertilizer raw material, and determining the composition ratio of the industrial waste; and a step of producing a soil composition.
  • the industrial wastes selected in the present invention are pulp and paper sludge discarded in paper mills and fly ash generated from thermal power plants.
  • Raw materials suitable for maximizing the water retention capacity of soil are Zeolite and diatomaceous earth.
  • pinestone (trade name Glaston) can also be suitably used.
  • fly ash selected in the present invention aims at supplying siliceous, aluminum, calcareous, iron, boron and the like. Therefore, fly ash, which is a constituent material of the composition of the present invention, plays a promoting role in the formation of soil aggregates, and ultimately maximizes the soil porosity. Fly ash is fine ash collected from the smoke that burns fine powder.
  • the active ingredient as a fertilizer is boron, which contains 52-63% of Keiic acid. Its effect is high as a boron fertilizer, and Improve the root of Ne.
  • the major part of the papermaking sludge selected in the present invention is occupied by cellulose and lignin.
  • cellulose and lignin In this case, for example, much of the cellulose is decomposed during the composting process, and the proportion of lignin and ash becomes significantly higher.
  • the application of paper sludge is suitable for all crops.
  • phosphoric acid fertilizer may be inferior due to the effect of aluminum nitrate. When using it for winter crops, it is recommended to apply 20 to 30% more phosphate fertilizer.
  • Diatomaceous earth which is a fine powder of the constituent materials of the composition of the present invention, is a fine powder and has been selected because it has an effective action for producing a granular product of the product of the present invention by cross-linking with CMC which is an aqueous adhesive.
  • a preferred composition of the composition of the present invention is 10-90, preferably 20-80, more preferably 30-70% by weight of papermaking sludge, 10-80 of fly ash, preferably 20-75, more preferably 30 to 70 weight 0/0, Zeoraito (Zeolite) 5 to 50, preferably 10 to 40 wt%, diatomaceous earth 20-50, preferably 25 to 40 wt%, optionally aqueous adhesive for example CMC ( Carboxymethylcellulose) from 0.5 to 10, preferably from 1 to 3% by weight.
  • This ratio means the ratio of each component when it is used, and it is not necessary to include all components.
  • composition of the present invention include the following combinations. % Means% by weight.
  • diatomaceous earth and / or zeolite can use pinestone (graston) as a substitute in the same ratio.
  • These compositions can be used as soil moisture regulators, soil conditioners, and fertilizer raw materials. Although the above ratio has been exemplified as being optimal, more favorable results can be obtained by performing quantitative adjustment according to soil conditions.
  • Particularly suitable compositions are as follows: 113478 is useful as a soil moisture regulator and fertilizer raw material, and 25656 is useful as a soil conditioner.
  • the preparations (1) to (4) or the preparations excluding CMC from them are useful and effective in adjusting the water content, deodorizing, and dehumidifying garbage, manure, and putrefactive substances. Diatomaceous earth and Z or zeolite had the same effect if pinestone (glaston) was replaced in the same ratio.
  • Natural fertilizer raw materials include raw garbage, squeezed waste after juice production of various fruits (eg, apples, mandarins, etc.), cow dung, horse droppings, fallen leaves, etc., but are widely applicable to what is called natural fertilizer.
  • the mixing ratio is 0.01 to: L00 with respect to 1 of the composition of the present invention in terms of volume ratio.
  • 1 of the composition of the present invention in terms of volume ratio.
  • 1: 0.:!-3 weight ratio 1: 0.01-2
  • the mixing method is not particularly limited, but it is preferable to use, for example, a rotary mixer in order to ensure a uniform mixing state. Mixing is possible at room temperature. After mixing, it must be added to the fermentation process in order to produce natural fertilizer. Fermentation is performed under appropriate temperature (eg, 15 to 28 ° C) with appropriate humidity and preservation treatment for about 20 to 90 days to achieve fertilization.
  • a rotary mixer in order to ensure a uniform mixing state. Mixing is possible at room temperature. After mixing, it must be added to the fermentation process in order to produce natural fertilizer. Fermentation is performed under appropriate temperature (eg, 15 to 28 ° C) with appropriate humidity and preservation treatment for about 20 to 90 days to achieve fertilization.
  • composition of the present invention for water control and deodorization of food waste, manure, and decay It is done by direct contact and mixing with food waste, manure and decay.
  • a garbage disposer is mixed and filled with the composition of the present invention and treated.
  • manure treatment of animals such as pigs when manure is collected, it is mixed with the composition of the present invention and stored for one to several days.
  • the treatment of garbage and various fruits (eg apples, mandarin oranges, etc.) after juice production, such as scum and other decay, is substantially the same as the treatment of manure.
  • the composition of the present invention is preferably 0.01 to 1, more preferably 0.05 to 0, for 1 of the target substance. 5, optimally in a weight ratio of 0.1 to 0.3.
  • the composition of the present invention is used for moisture adjustment, it is determined by the following formula according to the target moisture percentage.
  • composition of the present invention can appropriately adjust the mixing ratio for controlling water content.
  • composition of the present invention When the composition of the present invention is used as a dehumidifier or a deodorant, a predetermined amount of the composition of the present invention is sprayed on a target space to be treated.
  • Application rate is generally from 0.05 to 1, although preferred properly is 0. 5 ⁇ 1 Kg / m 2, Ru appropriately changeable der the sealed space.
  • Applications include under eaves, attics, spaces between floors, wall spaces, odor storage areas, and so on.
  • the composition of the present invention When the composition of the present invention is used in combination with building materials, it can also function as a dehumidifier or a deodorant for rooms and buildings. In this case, the building material and the composition of the present invention are mixed and used directly as wall soil or the like.
  • the composition of the present invention thus used exhibited an effective dehumidification / deodorization effect, for example, by spraying under the eaves.
  • Fly ash (Fly ash) 59 weight 0/0 Zeorai preparative 14 wt% diatomaceous earth 24% by weight aqueous adhesive (Binder) 3 wt%
  • the present composition is useful as a soil improver.
  • This composition is useful as a soil moisture regulator and a raw material for fertilizers.
  • the analysis results are as follows.
  • This composition is useful as a soil moisture regulator and a raw material for fertilizers.
  • the analysis results are as follows.
  • composition is useful as a soil conditioner.
  • This composition is useful as a soil moisture regulator and a raw material for manure.
  • the analysis results are as follows.
  • Papermaking sludge 69% by weight Pinestone 29% by weight Aqueous adhesive (Binder) 2% by weight This composition is useful as a soil moisture regulator and a fertilizer raw material.
  • Example 1 The product was granulated and dried in a heating dryer at 130-: 150 ° C for 20-30 minutes to obtain the final product.
  • a variety of water-based adhesives can be used as the water-based adhesive used for adhesion between raw material components and for promoting granulated products in the mixer, but CMC is most desirable.
  • Example 1 1
  • Example 13 The composition of any one obtained in Examples 1, 3, 4, and 7 to 9 and the cow dung raw material were mixed at a volume ratio of 1: 1 with a rotary mixer, and this was mixed at room temperature (about 15 to 25 ° C). In), fermentation was carried out for about 30 days to produce natural fertilizer.
  • the fertilizer has a great effect on water absorption and deodorization. It became practically dry, and no odor derived from cow dung was detected at all in a sensory test of 10 people.
  • Example 13 The composition of any one obtained in Examples 1, 3, 4, and 7 to 9 and the cow dung raw material were mixed at a volume ratio of 1: 1 with a rotary mixer, and this was mixed at room temperature (about 15 to 25 ° C). In), fermentation was carried out for about 30 days to produce natural fertilizer. The fertilizer has a great effect on water absorption and deodorization. It became practically dry, and no odor derived from cow dung was detected at all in a sensory test of 10 people.
  • Example 14 Using the composition of the present invention of any one of Examples 1 to 9, for any one of chicken dung, horse manure, mandarin rot, and household garbage, a test sample 1 was added in a weight ratio of 0.3 to the composition of the present invention 0.3. They were mixed and subjected to a sensory test for odor. An odor test was performed on the compositions of Examples 1 to 9 by eight collaborators.As a result, it was confirmed that the odor was reduced by half at 48 hours after preparation, and no odor was completely observed after storage for one week. Was.
  • Example 14 Using the composition of the present invention of any one of Examples 1 to 9, for any one of chicken dung, horse manure, mandarin rot, and household garbage, a test sample 1 was added in a weight ratio of 0.3 to the composition of the present invention 0.3. They were mixed and subjected to a sensory test for odor. An odor test was performed on the compositions of Examples 1 to 9 by eight collaborators.As a result, it was confirmed that the
  • Example 11 Plant growth experiments were performed using soil obtained by using the fertilizer obtained in Example 11 as a base fertilizer and using 10% VV. A few days after sowing, shoots emerged, and after about 10 days, the flowers blossomed. Thus, it was confirmed that the natural fertilizer prepared using the composition of the present invention as a fertilizer raw material is also extremely useful for promoting the growth of flowers. Since the composition of the present invention alone, which was performed in the target experiment, had the effect of adjusting the soil moisture and improving the soil, it was confirmed that the growth was moderate. In addition, a comparison was made using conventional flowering plant soil, and almost the same growth effect was confirmed.
  • Example 17 Example 17
  • the composition produced according to Example 11 or 12 was used as a bovine excreta treating agent on a farm of a cooperator residing in Wakayama Prefecture.
  • manure processing agent 1: 1.
  • the rise in fermentation degree and temperature was about twice faster than the first.
  • compositions produced in Examples 1 to 8 except for the water-based adhesive were used as a cattle excreta treatment agent on a farm of a cooperator living in Wakayama Prefecture.
  • the mixing ratio was 0.3 for each cow manure.
  • both composition groups obtained excellent effects on water absorption and deodorization of manure.
  • no odor was found after using the composition for one week after treatment.
  • compositions prepared in Examples 1 to 8 except for the water-based adhesive were used as a dehumidifier or a deodorant in a residential area of a co-worker resident in Wakayama Prefecture.
  • the application rate was 1-0.5 kg per lm 2 under the eaves.
  • all of the composition groups had excellent effects on dehumidification and deodorization under the eaves.
  • the soil composition of the present invention has a remarkable growth promoting effect on test crops among horticultural crops.
  • the effect of the soil composition prepared in the present invention significant superiority was confirmed in terms of the hardness and strength of stems and leaves, the gloss and the number of flowers.
  • the composition of the present invention was confirmed to have a water controlling ability and a deodorizing ability, which were not present as a food waste treating agent, a manure treating agent, a putrefactive agent, a dehumidifying agent, and a deodorizing agent.
  • the present invention is a very useful invention in the waste industry and the fertilizer industry.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Soil Sciences (AREA)
  • Materials Engineering (AREA)
  • Fertilizers (AREA)
  • Treatment Of Sludge (AREA)
  • Processing Of Solid Wastes (AREA)
  • Soil Conditioners And Soil-Stabilizing Materials (AREA)

Abstract

L'invention concerne une composition pour sol contenant des déchets industriels comme composant principal. Cette composition est préparée par introduction, dans un mélangeur rotatif, d'un adhésif aqueux et d'une composition renfermant une boue issue d'un procédé de fabrication de papier, des cendres volantes, des zéolites et/ou de la terre à diatomées, par mélange de la composition à une vitesse comprise entre 50 et 100 tours-minute, par formation de la composition en granules au moyen d'une extrudeuse, puis par chauffage et séchage des granules à une température comprise entre 130 °C et 150 °C pendant 20 à 30 minutes au moyen d'un séchoir chauffant. La composition pour sol susmentionnée exerce une activité favorisant la croissance d'une plante, d'où une forte augmentation du rendement dans certaines grandes cultures. Par ailleurs, cette composition pour sol contenant une boue issue d'un procédé de fabrication de papier et des cendres volantes est utile comme agent de traitement d'ordures ménagères, d'excréments et de matières putrescibles, comme agent déshumidificateur et comme désodorisant.
PCT/JP2002/007294 2001-07-19 2002-07-18 Composition pour sol contenant des dechets industriels comme composant principal WO2003008517A1 (fr)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2001220341 2001-07-19
JP2001-220341 2001-07-19
JP2001268087A JP2003096452A (ja) 2001-07-19 2001-09-04 産業廃棄物を主材とした土壌用組成物
JP2001-268087 2001-09-04

Publications (1)

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WO2003008517A1 true WO2003008517A1 (fr) 2003-01-30

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CN (1) CN1280382C (fr)
WO (1) WO2003008517A1 (fr)

Cited By (5)

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Publication number Priority date Publication date Assignee Title
CN101781568B (zh) * 2010-02-03 2011-08-31 北京海亚地大生化科技有限公司 一种土壤调理剂及其制备方法和应用
CN103396808A (zh) * 2013-07-29 2013-11-20 湖北省农业科学院植保土肥研究所 一种用于冷浸田土壤的改良剂及其应用
CN104059410A (zh) * 2013-05-03 2014-09-24 攀钢集团攀枝花钢铁研究院有限公司 抗锈转化层形成剂及其制备方法和用途
JP2018145338A (ja) * 2017-03-08 2018-09-20 東京農大発株式会社全国土の会 セルロース系バイオマス焼却灰を利用した機能性人工砂及びその製造方法
CN113861996A (zh) * 2021-10-20 2021-12-31 四川农业大学 一种针对于石灰性紫色土的复合土壤改良剂及其施用方法

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CN102040356B (zh) * 2009-10-21 2013-01-16 财团法人工业技术研究院 轻质隔热复合粒料及其制造方法
CN102187777A (zh) * 2010-03-19 2011-09-21 许水茂 植栽土壤及其制备方法
CN101905998B (zh) * 2010-07-08 2012-10-17 四川大学 一种含有有机铁元素的边坡人工土壤专用肥料的制备方法
CN101905996B (zh) * 2010-07-08 2012-10-17 四川大学 一种含有有机硼元素的边坡人工土壤专用肥料的制备方法
CN101905997B (zh) * 2010-07-08 2012-10-17 四川大学 一种含有有机钼元素的边坡人工土壤专用肥料的制备方法
CN101863706B (zh) * 2010-07-08 2012-09-19 李桓宇 一种用造纸污泥生产的有机复合肥料及其制造方法
JP5915831B2 (ja) * 2011-07-28 2016-05-11 株式会社日健総本社 フォルミジウム・ルリドムの培養方法
CN103012012B (zh) * 2012-12-10 2014-07-23 武汉纺织大学 生产具备保水且可生物降解肥料的方法
CN105481497A (zh) * 2015-10-19 2016-04-13 南宁市金稻源农资有限公司 用于丝瓜的化肥
CN106613476A (zh) * 2016-11-10 2017-05-10 陈建峰 一种利用生活垃圾焚烧飞灰培育基质营养土的方法
CN107502362B (zh) * 2017-08-29 2020-06-05 泰谷生态科技集团股份有限公司 用造纸黑液制备酸性土壤调理剂的方法及其应用
JP6536973B2 (ja) * 2017-11-06 2019-07-03 常陽化成株式会社 土壌改良材の製造方法
CN108329010B (zh) * 2018-02-01 2021-02-26 东北师范大学 一种适用于草地的空心多孔隙球型水分调节器

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JPH03126688A (ja) * 1989-10-09 1991-05-29 Honmachi:Kk 糞尿の有機肥料化処理剤と処理方法
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101781568B (zh) * 2010-02-03 2011-08-31 北京海亚地大生化科技有限公司 一种土壤调理剂及其制备方法和应用
CN104059410A (zh) * 2013-05-03 2014-09-24 攀钢集团攀枝花钢铁研究院有限公司 抗锈转化层形成剂及其制备方法和用途
CN103396808A (zh) * 2013-07-29 2013-11-20 湖北省农业科学院植保土肥研究所 一种用于冷浸田土壤的改良剂及其应用
CN103396808B (zh) * 2013-07-29 2016-04-20 湖北省农业科学院植保土肥研究所 一种用于冷浸田土壤的改良剂及其应用
JP2018145338A (ja) * 2017-03-08 2018-09-20 東京農大発株式会社全国土の会 セルロース系バイオマス焼却灰を利用した機能性人工砂及びその製造方法
CN113861996A (zh) * 2021-10-20 2021-12-31 四川农业大学 一种针对于石灰性紫色土的复合土壤改良剂及其施用方法

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JP2003096452A (ja) 2003-04-03
CN1526003A (zh) 2004-09-01

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