WO2002089989A1 - Dispositif de melangeage, concassage et pulverisation et procede de pulverisation de substances au moyen dudit procede - Google Patents
Dispositif de melangeage, concassage et pulverisation et procede de pulverisation de substances au moyen dudit procede Download PDFInfo
- Publication number
- WO2002089989A1 WO2002089989A1 PCT/JP2002/000175 JP0200175W WO02089989A1 WO 2002089989 A1 WO2002089989 A1 WO 2002089989A1 JP 0200175 W JP0200175 W JP 0200175W WO 02089989 A1 WO02089989 A1 WO 02089989A1
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- WIPO (PCT)
- Prior art keywords
- mixing
- cylindrical body
- pulverizing
- plate
- small chambers
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/0005—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor for pharmaceuticals, biologicals or living parts
- A61L2/0011—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor for pharmaceuticals, biologicals or living parts using physical methods
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/50—Mixing liquids with solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/421—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path
- B01F25/422—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path between stacked plates, e.g. grooved or perforated plates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/432—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa
- B01F25/4321—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa the subflows consisting of at least two flat layers which are recombined, e.g. using means having restriction or expansion zones
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/432—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa
- B01F25/4322—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa essentially composed of stacks of sheets, e.g. corrugated sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/44—Mixers in which the components are pressed through slits
- B01F25/441—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits
- B01F25/4413—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits the slits being formed between opposed conical or cylindrical surfaces
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/121—Coherent waves, e.g. laser beams
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/0873—Materials to be treated
- B01J2219/0879—Solid
Definitions
- the present invention relates to an apparatus for mixing various substances into a fluid, an apparatus for pulverizing various substances into fine particles, an apparatus for mixing various substances into a fluid and pulverizing fine particles, and a method for forming fine particles using these substances.
- the present invention relates to an apparatus and a method capable of realizing mixing and / or pulverization without using mechanical power.
- this equipment and method can be used to make food raw materials and pharmaceutical raw materials into fine particles, deactivate enzymes and spores contained in food raw materials and pharmaceutical raw materials, sterilize, deodorize, and detoxify industrial waste. It can be used for such things.
- this stationary mixing apparatus has a cylindrical casing 203 having an inlet 201 and an outlet 202 at both ends, and a casing 2 as shown in FIGS.
- a large-diameter disk 206 in which a large number of polygonal small chambers 204 and 205 with an open front are arranged in a honeycomb shape on opposing surfaces provided in 0 3, and a small-diameter disk 20 And a plurality of flow conducting units formed by concentrically laminating 7 and 7.
- the large-diameter disk 206 has a diameter matching the inner diameter of the casing 203 and has a flow hole 208 formed at the center.
- the large-diameter disk 206 and the small-diameter disk 207 are arranged such that the openings of the small chambers 204 and 205 face each other.
- the small chamber 204 of the large-diameter disk 206 and the small chamber 205 of the small-diameter disk 206 communicate with each other in a plurality of opposing small chambers. Are arranged in different positions. In this way, one large-diameter disk 206 and the small-diameter disk 206 that are opposed to each other form one flow guiding unit.
- the plurality of flow guiding units are circles having the same diameter.
- the boards are superimposed so as to be adjacent to each other and are set in the casing 203.
- large-diameter disks 206 of the flow guiding unit are located at both ends, and the flow holes 208 are communicated with the inlet 201 and the outlet 202 of the casing 203.
- the fluid to be mixed When the fluid to be mixed is pressurized and flows into the interior space of the casing 203 from the inlet 201, the fluid flows through the casing hole 208 of the upstream conducting unit 208. Enter inside. Then, the straight traveling path is obstructed by the small-diameter disk 207 and the direction is changed, and flows radially from the center toward the outer peripheral side through the small chambers 205 and 204 communicating with each other. Next, the gap between the small-diameter disk 207 located on the downstream side and the inner peripheral wall of the casing 203 is broken, and the small-diameter disk 205 side of the small-diameter disk 207 located on the downstream side is opened.
- the straight course is obstructed by the large-diameter disc 206 and the direction is changed, and the fluid flows from the outer peripheral side toward the center through the small chambers 205 and 204 communicating with each other. Then, it flows into the small chamber 204 side of the large-diameter disk 206 located on the next downstream side through the circulation hole 208 of the large-diameter disk 206. This is repeated, and finally discharged from the outlet 202.
- the outer peripheral side small chambers 204a and 205a may have the same polygonal shape. Instead, one or two sides are cut off. If there is such a notch, the fluid will concentrate there. In other words, the fluid flows only into such a notch, and the inflow path in all directions is broken. The so-called short path phenomenon occurs. Thus, the fluid collides with the walls of multiple chambers, reducing the mixing effect due to repeated complex dispersion, inversion, eddy currents, radial dispersion, and aggregation of the flow. This was a drawback of the static mixing device proposed in Japanese Patent Application Publication No. 58-1333382.
- the sealing function is made by making the outer diameter of the disc 206 adopted in Japanese Patent Application Laid-Open No. 58-133382 match the inner diameter of the casing 203. With this, it is difficult to put the disc 206 into and out of the casing 203. Therefore, a method of increasing the inner diameter of the casing 203 by the thickness of the seal and stopping the fluid with the seal has been adopted. Since the casing 203 requires a length for arranging a plurality of flow guide units, a seal must be provided for each flow guide unit over the entire length of the casing 203. However, when the supply pressure of the fluid increases, the seal is broken and a gap is generated even partially between the outer diameter of the disc 206 and the inner diameter of the casing 203. In this case, the fluid flows through the gap along the entire inner peripheral surface of the casing 203 and short-circuits to the outlet 202 without receiving the mixing action. Also in this case, there is a disadvantage that the uniform mixing effect is reduced.
- the static mixing device proposed in Japanese Patent Application Laid-Open No. 58-133382 focuses only on the mixing of fluids, the material is ground while mixing. Other functions and effects such as atomization and modification could not be obtained.
- a material for component extraction and a raw material are evaporated in a gas in a reaction vessel by thermal plasma or the like, and the It is known that it is formed by reacting with a.
- the gas in the reaction vessel in which the ultrafine particles are suspended and dispersed is passed through a heat exchanger equipped with a cooling pipe cooled by a cooling medium. To the collector to capture and collect ultra-fine particles through the filter.
- the circulating fluid which is a mixture of the material for component extraction and the material to be atomized and the liquid
- the atomized particles contained therein are inertized in the flow path under low pressure.
- devices are also known.
- the fine particles flowing into the low-pressure particle collecting means expand and are classified and collected by the primary and secondary filters and the coarse particle collecting means provided in the particle collecting means, respectively. Things.
- the configuration of the apparatus used in this method is relatively large because of its configuration, and the spray nozzle is clogged with the mixture (circulating fluid) of the material to be atomized and the liquid, and each time the nozzle is clogged.
- the spray nozzle is clogged with the mixture (circulating fluid) of the material to be atomized and the liquid, and each time the nozzle is clogged.
- the supply amount of the material to be finely divided must necessarily be prepared in a large amount.
- a large amount of waste material was extracted after the extraction of components, causing problems in the treatment.
- a method of promoting or delaying the generation and decomposition of chemical substances by decomposition treatment of hardly decomposable substances such as environmental pollutants and progress of chemical reaction between gaseous reactants and solid reactants or control of chemical reactions
- those using supercritical processing and electromagnetic waves, ultrasonic waves, infrared rays, far infrared rays, and the like are known.
- the substance to be supercritically processed is pulverized, a fluid in which the substance is mixed is prepared in advance, and the fluid flows into the reaction vessel. Raise to specific numerical levels and place in supercritical conditions.
- a gas-phase oxidizing agent such as air, oxygen, or carbon dioxide or a liquid-phase oxidizing agent is forcibly fed into a reaction vessel to generate an oxidative decomposition reaction or the like to perform treatment.
- Decomposition of decomposed substances and chemical reaction of reactants are basically based on decomposition and mixing by collision of molecules of those substances, and mixing and the like must be performed after introduction into each reactor.
- the pressure inside the equipment is set high, such as under supercritical conditions, problems will occur in the power of the equipment for mixing and stirring the substances introduced into the equipment, and in the sealing of the reaction tank.
- the equipment itself becomes large-scale, There has been a problem that the desired processing is not completely performed.
- An object of the present invention is to propose the following apparatus and method in view of the above-mentioned problems of the related art.
- the above-described known static mixing apparatus is improved to facilitate the assembling, and to facilitate the processing of the inner surface of the cylindrical body constituting the apparatus, thereby reducing the cost. It is intended to provide.
- a mixing device capable of preventing fluid leakage due to the existence of a partial gap and preventing non-uniform mixing due to short-circuit flow (short path) is provided. It is intended to be.
- the aim is to propose a mixing and pulverizing device that can be pulverized into fine particles of approximately spherical shape with a particle size of about lnm to 0.1 l ⁇ m.
- Such a mixing and milling device can also be used as a heat exchanger, and can be used for critical treatment, supercritical treatment, decomposition of substances using electromagnetic waves, ultrasonic waves, infrared rays, far-infrared rays, etc. It can also be used for applications such as reaction acceleration treatment.
- An object of the present invention is to propose a method for atomizing a substance by using the above-mentioned mixing / milling micronization apparatus.
- Such micronization methods are used as a part of processes such as a critical treatment, a supercritical treatment, a decomposition treatment of substances using electromagnetic waves, ultrasonic waves, infrared rays, far infrared rays, etc., and a chemical reaction acceleration treatment. Can be used.
- Including the method of the present invention a series of processes such as decomposition treatment of substances using these electromagnetic waves, ultrasonic waves, infrared rays, far infrared rays, etc.
- the desired reaction result can be obtained by accelerating the reaction and decomposing the substance.
- an apparatus proposed by the present invention has a hollow body inside, a cylindrical body having an inlet opening on one end side, and an outlet opening on the other end side.
- the fluid flow path includes a first structure having a plurality of first small chambers having an open front surface, and a second structure having a plurality of second small chambers having an open front surface. And the front opening of the first small chamber and the front opening of the second small chamber are opposed to each other, and the opposed small chambers are alternated, and each of the other chambers is opposed to each other. It is formed so as to be in close contact with at least one or more small chambers.
- a point on the line A—R connecting the vertex A and the midpoint R on the base B—C of a virtual right-angled isosceles triangle ABC with the vertex A as a right angle.
- S the point at any position on the hypotenuse A—B except points A and B is P
- the point at any position on the hypotenuse A—C except points A and C is Q
- the points P and S When the line segment P—S and the line segment Q—S connecting the point Q and the point S respectively are rotated about the point P, the point where the line segment P—S intersects the base B—C is S 1.
- the point where line segment Q—S intersects base B—C when rotated about point Q is S2, and line segment P—S—Q—S2—R—S1—P It is determined by the enclosed shape.
- the front opening of the small chamber and the front opening of the second chamber are opposed to each other, and the opposing small chambers are alternated, and at least one or more small chambers of other structures facing each small chamber.
- the space in front of the small chambers facing each other is divided by at least one or more small chambers of another structure facing each other.
- the area of the divided part of the small chamber opening and the volume of the divided part are different before and after the fluid flow path.
- the small chambers have their front openings facing each other, and the small chambers facing each other are different from each other, and each small chamber communicates with at least one or more small chambers of the other structure facing each other.
- the fluid material flow path formed from the inlet side to the outlet side of the cylindrical body is formed by a series of divided sections having different shapes and volumes before and after the continuation. Therefore, when the fluid to be mixed and atomized is pressurized and flows into the fluid flow path, the fluid collides with the fluid each time it flows into each of the divided sections that are continuous and have different shapes and volumes. Complex movements such as inversion, eddy currents, radiative dispersion, and aggregation are repeated.
- the fluid that has flowed into the division having a smaller area and volume than the other divisions is subjected to the increased agglutination due to the strong conjugation pressure.
- the fluid that has flowed into the division having a larger area and volume than the other divisions is released from the conjugation pressure at a stretch, and is decomposed and atomized. Since this repetitive action occurs in the fluid distribution channel, extremely uniform mixing and granulation of a desired spherical shape, for example, a nearly spherical shape can be achieved.
- the mixing and pulverizing device of the present invention further comprises a front surface having the characteristic opening shape.
- the fluid is formed in such a manner that the small chambers facing each other are staggered, and each small chamber is in close contact with at least one or more small chambers of the other structure facing each other.
- An object flow path is provided between the inlet opening and the outlet opening. Therefore, when the coarsely pulverized substance and the fluid are mixed, pumped, and passed through the mixing and pulverizing apparatus of the present invention, the primary and secondary packing pressures, and explosion of the mixture of the substance and the liquid are obtained.
- the line segment P-S and the line segment Q-S can be formed by one straight line, a bent line composed of a plurality of straight lines, or a curve such as a sine curve or an arc. You can also. Also, a straight line, a bent line, and a curved line may be combined.
- the points P and Q when defining the opening shapes of the first chamber and the second chamber whose front surfaces are open are respectively hypotenuses A-B , The midpoint of the hypotenuse A—C.
- points P and Q are a midpoint of hypotenuse AB and a midpoint of hypotenuse AC, respectively.
- the intersections of the perpendiculars drawn from the midpoints P and Q to the base B—C and the bases B—C are S 3 and S 4, respectively.
- the area of the rectangle P—S 3—R—S 4—Q—P is half the area of the right-angled isosceles triangle ABC.
- point S 1 is a point where line segment P—S intersects base B—C when line segment P—S is rotated about point P
- point S 2 Is the point where the line segment QS intersects the base BC when the line segment QS is rotated about the point Q. Therefore, in Fig. 1, the area of the part represented by S5 is the area of the part represented by S6. The area of the portion represented by S7 is the same as the area of the portion represented by S8. As a result, the area of the shape surrounded by the line segment P—S—Q—S2—S1—P formed as described above is the area of the virtual right-angled isosceles triangle ABC It is a half of that.
- the points P and Q when defining the opening shapes of the first chamber and the second chamber whose front faces are open are respectively the midpoints of the hypotenuses A and B. If the hypotenuse A-C is set at the midpoint, as described above, before and after the continuation, the fluid material flow path is formed by the continuation of the divided portions having different shapes and volumes, respectively, and mixing is performed.
- the fluid to be micronized is pressurized and flowed in, it can mix extremely uniformly, and can granulate the desired spherical shape, for example, almost spherical shape, as well as the following: This is advantageous because it is effective.
- the points P and Q when defining the shape of the opening of the first chamber and the second chamber whose front faces are open are respectively the midpoint of the hypotenuse A_B and the hypotenuse A—C If it is set to be the middle point, the surface of the first structure in which a plurality of the first small chambers each having an open front surface are provided, and the surface of the second structure in which a plurality of the second small rooms are provided, This means that the first cell and the second cell can be deployed over the entire surface without any gaps.
- FIGS. 1 to 13, 31 (a), 32 (a), 33 (a), and 53 are formed on the basis of a right-angled isosceles triangle in accordance with the definition described above.
- 1 shows an example of the shape of a first small chamber opening and a second small chamber opening provided respectively in a first structure and a second structure of a mixing and pulverizing device of the present invention.
- the first chamber and the second chamber whose front faces are open are similar to the shape enclosed by the line segment P—S—Q—S2—S1—P in these drawings.
- the first structure where the part surrounded by the segment surrounded by the line segment P'-S'-Q'-S2'-S1'-P 'is smaller than or larger than the shape
- An object formed by standing on a second structure.
- Fig. 31 (b), Fig. 32 (b), and Fig. 33 (b) show the shape surrounded by the line segment P—S—Q—S2—S1—P.
- the area of the shape surrounded by the line segment P—S—Q—S2—S1—P is one-half of the area of the original virtual right-angled isosceles triangle ABC.
- the surface of the first structure where a plurality of the first small chambers each having an open front surface are provided and the surface of the second structure where the plurality of the second small chambers are provided, respectively.
- the first and second compartments can be deployed without any gaps over the entire surface. Therefore, if this condition is satisfied, it is not necessary that the line segment S—S—S in the line segment P—S—Q—S 2—S 1—P be a straight line on the base B—C Absent.
- the opening shapes of the first small chamber and the second small chamber whose front faces are open are represented by points P and Q, respectively, where hypotenuse A — B, On A—C, the line is symmetrical with respect to line A—R.
- Line S 2—R— S 1 is either line S 2—R or line R—S 1.
- One of them is a line segment of an arbitrary shape different from the straight line on the base B-C, and a line segment that is point-symmetrical to the arbitrary shape line segment with the center point R as the center is defined as the other line segment. You can also determine by doing.
- FIG. 14 shows an example of such a case, in which the points P and Q are the middle points of the hypotenuses A_B and A-C, respectively.
- the area of the portion indicated by S9 is the same as the area of the portion indicated by S10. Therefore, when defining the opening shapes of the first chamber and the second chamber whose front faces are open, the points P and Q are defined as the midpoints of the hypotenuses A and B, and the hypotenuse A, respectively. The same effect can be obtained as when the midpoint of C is set.
- the fluid material flow path can be formed in the axial direction of the cylindrical body or in a direction orthogonal to the axial direction of the cylindrical body.
- a surface where the front openings of the plurality of first small chambers provided in the first structure and the front openings of the plurality of second small chambers provided in the second structure are opposed to each other.
- the fluid material flow path is provided in the axial direction of the cylindrical body.
- the facing surface is in a direction perpendicular to the axial direction of the cylindrical body
- the fluid distribution channel is provided in a direction perpendicular to the axial direction of the cylindrical body.
- the first structure and the second structure can be mounted in the cylindrical body, and the fluid material flow path is set in the axial direction of the cylindrical body or in the direction orthogonal to the axial direction of the cylindrical body.
- the first structure and the second structure are provided in a concave portion provided in the peripheral wall of the cylindrical body.
- the shape and structure can be fitted and fixed to the structure. This facilitates the processing of the inner peripheral surface of the cylindrical body and the assembly of the device, and also enables the partial inner clearance between the inner peripheral surface of the cylindrical body and the first and second structures. This is advantageous because a large gap can be prevented. That is, the phenomenon of a so-called short path can be prevented.
- the first structure is a cylindrical body
- the plurality of first chambers provided on the first structure and having an open front surface are:
- a plurality of second small chambers formed on the inner peripheral wall of the cylindrical body and having an open front surface provided in the second structure are provided on the outer peripheral wall of the structure mounted in the cylindrical body.
- the structure may be formed as follows. With this configuration, the fluid material flow path is provided in the axial direction of the cylindrical body.
- the fluid material flow path formed by bringing the first structure and the second structure into close contact with the first small chamber opening and the second small chamber opening facing each other has the first structure
- the inner diameter of the cylindrical body as the object and the outer diameter of the second structure are formed so as to correspond to each other, and the second structure is mounted in the cylindrical body as the first structure. It can be formed simply by fitting and fixing to a concave portion provided in the peripheral wall of the body. This also facilitates the processing of the inner peripheral surface of the cylindrical body, the processing of the outer peripheral surface of the second structure, and the assembly of the device. This is advantageous because a partial gap can be prevented from occurring between the two. That is, it is possible to prevent a so-called short path phenomenon from occurring.
- the tubular body is made divisible, and the second structure, which is a structure mounted in the tubular body, can be divided into the tubular body, attached to the tubular body, and removed. It can be.
- the second structure can be easily mounted in the cylindrical body, which is the first structure, and the assembly and maintenance are also facilitated.
- the cylindrical body can be divided, for example, it is possible to adopt a shape and structure that can divide the cylindrical body into two in the axial direction.
- the first plate and the second plate are each provided with a plurality of small chambers each having an open front surface on one surface, Or, the front face on both one side and the other side that is the back side of the one side
- a fluid flow path is formed between these plates that are closely stacked. This facilitates machining of the inner peripheral surface of the cylindrical body and assembly of the device, and also provides a portion between the inner peripheral surface of the cylindrical body and the first and second structures. This is advantageous because it is possible to prevent a gap from occurring. That is, the phenomenon of a so-called short path can be prevented.
- the plurality of small chambers provided on the other surface of the second plate body and having an open front surface are the plurality of small chambers having the front surface opened on one surface of the second plate body.
- the small chambers provided on the one surface are respectively set at a predetermined angle, for example, 45 degrees. , 90 degrees, 180 degrees, can be provided as rotated.
- the plurality of small chambers provided on the other surface of the second plate body and having an open front surface include the plurality of small chambers having a front surface opened on one surface of the second plate body.
- the position may be provided at a position on the back side of the second plate different from the position where the second plate is located.
- the plurality of small chambers provided on the other surface of the second plate body and having an open front surface are provided with the plurality of small chambers having an open front surface on one surface of the second plate body.
- the small chambers provided on the one surface are respectively set at predetermined angles, for example, 45 degrees, 90 degrees, It can also be rotated 180 degrees.
- the right-angled isosceles triangle is used as a basic shape in FIGS. 1 to 14.
- the small chambers having such a shape are arranged so that their front openings are opposed to each other, and the opposed small chambers are alternately arranged so that each of the small chambers can communicate with at least one or more small chambers of the other structures facing each other. Therefore, when a fluid flow path is formed, the shape and size (area, volume) of the space in front of the plurality of small chambers vary greatly. Therefore, the movement caused by collision, diffusion, inversion, generation of eddy current, and the like of the fluid flowing in the fluid flow path can be further complicated, and mixing and pulverization can be promoted.
- the upstream and / or downstream of the position where the fluid flow path is formed by the first structure and the second structure in the cylindrical body are orthogonal to the axial direction of the cylindrical body, and the adjacent frame bodies face each other. It is also possible to adopt a structure in which the openings are stacked so that the openings are at different positions.
- the fluid flowing through the cylindrical body includes collision, diffusion, inversion, and the like when flowing through the fluid flow path formed by the first structure and the second structure.
- the flow path formed by the opening of the frame before and after the fluid flow path adds more complicated movement, which promotes mixing and pulverization. This is advantageous in making
- the cylindrical body can be divided, for example, can be divided in the axial direction, and the first structure and the second structure composed of the first plate or the second plate are provided.
- the object can be detachable by dividing the tubular body and attaching it to the tubular body.
- the cylindrical body can be divided, for example, divided into two in the axial direction, and the first structure composed of the first plate or the second plate is provided.
- the structure and the second structure, and the frame body arranged in a stack can divide the tubular body, attach it to the tubular body, and make it detachable.
- first plate, the second plate, and the frame can be easily mounted in the tubular body, and assembly and maintenance can be facilitated.
- a plurality of first small chambers provided on the first structure and having an open front surface are provided on the second structure. It is desirable that the plurality of second compartments whose front faces are open have the same shape. In this way, the first chamber is rotated 45 degrees, 90 degrees, etc. at the position of the second structure corresponding to the position where the first structure has the first chamber. In this state, a small chamber with a front opening provided in the first structure and a small chamber with a front opening provided in the second structure are provided by a simple method such as providing a second small chamber.
- the small chambers which are opposed to each other are staggered when they are opposed to each other, so that each of the small chambers can communicate with at least one or more small chambers of the other structures facing each other.
- the size of the second small chamber corresponding to the first small chamber is regular, so that an inconvenience such as a short path does not occur, which is advantageous.
- a plurality of first chambers and / or second structures provided on the first structure and having an open front surface are provided.
- a plurality of honeycomb structures may be arranged on the first structure and the second structure, respectively, so that the above-described fluid flow path may be formed.
- the points P and Q are each a virtual right angle If the midpoint of the hypotenuses A-B and A-C of the isosceles triangle is set, the first and second compartments are separated from each other by the front of the predetermined surface of the first and second structures. It can be deployed without.
- the upstream side and the downstream side of the position where the fluid flow path is formed by the first structure and the second structure in the cylindrical body are provided.
- a frustoconical inlet-side space whose diameter increases toward the downstream side from the inlet opening and a frustoconical-shaped outlet-side space whose diameter decreases toward the outlet opening are provided.
- the fluid flowing through the cylindrical body includes collisions, diffusion, inversion, and the like that occur when the fluid flows in the fluid flow path formed by the first structure and the second structure.
- the first structure is a cylindrical body, and the first structures are provided with a plurality of first small chambers each having an open front surface. Are formed on the inner peripheral wall of the cylindrical body, and the plurality of second small chambers provided on the second structure and having an open front surface are formed on the outer periphery of the structure mounted in the cylindrical body. It can be a structure formed on the wall. In this case, the fluid flow path is formed between the circumference of the cylindrical body and the circumference of the structure mounted inside the cylindrical body.
- the first structure and / or the second structure may be a carbon material, a metal composite material composed of carbon and other metal components, ceramics, and minerals. It can be composed of any one of the materials.
- the tubular body can be made of any one of a carbon material, a metal composite material composed of carbon and other metal components, ceramics, and a mineral material.
- first structure and the Z or the second structure can be made of any one of a resin and a synthetic resin.
- the tubular body can also be made of any one of resin and synthetic resin.
- first structure, the second structure, and the cylindrical body are made of a heat conductive material such as copper, aluminum, or carbon, and are used as a mixing / particulation device that can be used as a heat exchanger. You can also.
- first structure, the second structure, and the cylindrical body can naturally be made of metal such as SUS.
- the outside of the cylindrical body is also provided. It is possible to adopt a structure in which a magnet is attached to the periphery.
- the outer shape of the cylindrical body may be any shape such that its cross section is circular, elliptical, or polygonal (triangular, quadrangular, etc.).
- the central part is a cylindrical body whose cross section is circular, elliptical, or polygonal (triangular, quadrangular, etc.), and corresponds to the entrance side and the exit side. It can also be in the form provided.
- any one or more of the ultrasonic irradiation device, the electromagnetic wave irradiation device, the high frequency irradiation device, and the laser light irradiation device are connected to the upstream and / or downstream of any of the mixing and pulverizing device of the present invention. Can be used.
- any of the above-mentioned mixing / crushing and finely pulverizing apparatuses of the present invention can be used by connecting a foreign substance injection port upstream and / or downstream thereof.
- the oxidation reaction of the object to be treated is drawn out, and when the object to be treated contains an acid-forming component such as chlorine, etc.
- an acid-forming component such as chlorine, etc.
- various substances, the to-be-decomposed substance, etc. can be ground
- the device itself of the present invention can be used as a continuous mixing / separation reaction generating device.
- An electromagnetic wave irradiator, an infrared irradiator, an ultrasonic irradiator, etc. are installed downstream of the apparatus of the present invention and, if necessary, upstream, to decompose environmental pollutants and hardly decomposable substances, And the processing of accelerating the decomposition can be greatly improved.
- a method of atomizing a substance proposed by the present invention uses any one of the above-mentioned mixing and pulverizing apparatus of the present invention.
- the substance is formed into fine particles by pressurized inflow from the inlet opening to the outlet opening of the cylindrical body constituting the above.
- Another method of atomizing a substance proposed by the present invention uses any one of the above-described mixing and pulverizing apparatus of the present invention, wherein a fluid containing a substance to be atomized is mixed. Is continuously pressurized and flowed from the inlet opening to the outlet opening of the cylindrical body constituting the mixing and pulverizing / micronizing device, and the substance is continuously and critically or supercritically formed in the cylindrical state. It is to be made into fine particles.
- the critical state is a state in which a substance is placed at a temperature higher than the critical temperature of the substance and under a pressure higher than the critical pressure of the substance, so that it is difficult to be referred to as a gas or a liquid.
- the supercritical state refers to a state in which the state becomes higher than the critical state and there is no distinction between gas and liquid.
- Critical temperature and critical pressure are determined by substances.
- a fluid in which a substance to be atomized is mixed with a gas phase oxidizing agent such as air, oxygen, or carbon dioxide, or a liquid phase oxidizing agent is used in the present invention.
- Critical pressure and a critical pressure or a supercritical state for the substance to be atomized which continuously flows under pressure from the inlet opening to the outlet opening of the cylindrical body that constitutes the mixing and pulverization atomizer, and This can be achieved by setting the critical temperature.
- the pressure can be controlled by adjusting the pressure at the time of pressurizing and inflowing the fluid into the cylindrical body of the mixing and pulverization micronization apparatus of the present invention, and the temperature can be controlled by the mixing and pulverization micronization apparatus of the present invention. It can be controlled by adjusting the temperature at which the cylindrical body is heated.
- the industrial waste is pulverized and fluidized, and the mixed and pulverized micropulverizer of the present invention is mixed with pure oxygen gas under pressure.
- the mixing and pulverizing device of the present invention and the method of pulverizing a substance using the same carbon dioxide or the like as a solvent is mixed with a fluid in which a substance to be micronized is mixed.
- the material is continuously pressurized and flowed into the device, so that a critical process or a supercritical process is continuously performed in the cylindrical body, and the material is converted into ultrafine particles, decomposed, and reformed. be able to.
- At least one or more of electromagnetic wave irradiation means, ultrasonic irradiation means, infrared irradiation means, far infrared irradiation means, and laser light irradiation means is provided on the upstream side and / or downstream side of the cylindrical body. If the configuration provided with is adopted, the ultrafine particles of the substance can be more effectively subjected to the ridging, decomposing, and reforming reactions.
- the mixing and pulverizing apparatus and the method for pulverizing a substance using the apparatus according to the present invention For example, it is possible to effectively perform reactions such as decomposition and reforming of hardly decomposable substances, harmful organic substances, environmental pollutants, and chemical substances.
- the present invention provides a line segment connecting an arbitrary point on the two hypotenuses of a right-angled isosceles triangle and an arbitrary point on a perpendicular line from the vertex to the base, clockwise and clockwise with respect to the arbitrary point on the hypotenuse. Each of them is rotated counterclockwise to intersect with the base, and the basic shape is a figure having an area of 1/2 of the right isosceles triangle formed by connecting them.
- the opening and the front opening of the other small room face each other, and the small rooms facing each other are staggered so that each small room can communicate with at least one or more small rooms on the other side facing each other.
- the fluid distribution channel thus formed is formed by a series of divided portions having different shapes and volumes before and after the fluid distribution channel.
- the substance to be atomized in the fluid is first-ordered in a continuous divided portion having different shapes and volumes. Continuously receives internal and external pressures such as packing pressure, secondary packing pressure, explosion, twisting, swelling, kneading, and friction.
- internal and external pressures such as packing pressure, secondary packing pressure, explosion, twisting, swelling, kneading, and friction.
- FIG. 1 is a view for explaining an embodiment in which the shape of a small chamber having a front opening formed on the surface of a structure for forming a fluid material flow path in the mixing and pulverization micronization apparatus of the present invention is described.
- FIG. 2 is a diagram for explaining an embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 3 is a view for explaining an embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 4 is a diagram for explaining an embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 5 is a view for explaining an embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 6 is a view for explaining an embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 7 is a view for explaining an embodiment for defining the shape of a small chamber with another front opening (
- FIG. 8 is a view for explaining an embodiment for defining the shape of a small chamber with another front opening (
- FIG. 9 is a diagram illustrating an embodiment that defines the shape of a small chamber with another front opening.
- ⁇ FIG. 10 is a diagram illustrating an embodiment that defines the shape of a small chamber with another front
- FIG. 11 is a diagram for explaining an embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 12 is a view for explaining another embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 13 is a view for explaining an embodiment in which the shape of a small chamber having another front opening is defined.o
- FIG. 14 is a view for explaining an embodiment in which the shape of another small chamber with a front opening is defined.
- FIG. 15 (a) is a cross-sectional view in which a part of the embodiment of the mixing and pulverizing microparticulation device of the present invention is omitted, and (b) is a side view of (a).
- FIG. 16 (a) is an enlarged plan view of the first plate provided in the apparatus shown in FIG. 15 (a)
- FIG. 16 (b) is an enlarged plan view of the apparatus shown in FIG. 15 (a).
- FIG. 4 is an enlarged plan view of a second plate body provided.
- FIG. 17 (a) is a sectional view taken along line AA of FIG. 16 (a), and FIG. 17 (b) is a sectional view taken along line BB of FIG. 16 (b).
- FIG. 18 is a perspective view of the first plate shown in FIG. 16 (a).
- FIG. 19 is a perspective view of the second plate shown in FIG. 16 (b).
- FIG. 20 is a perspective view illustrating a state in which the first plate and the second plate are stacked.
- FIG. 21 (a) is a plan view illustrating a state in which a first plate and a second plate are stacked
- FIG. 21 (b) is a plan view illustrating a state in which a fluid flows.
- a) is a cross-sectional view in which a part of a C-C line portion is omitted.
- FIG. 22 is a perspective view illustrating an embodiment of the external appearance of the mixing / crushing micronization apparatus of the present invention shown in FIG. 15 (a).
- FIG. 23 illustrates an assembled state of another mixing / crushing / micronizing apparatus of the present invention. It is an exploded perspective view.
- FIGS. 24 (a) to (h) are diagrams for explaining the components of the mixing / crushing micronization device shown in FIG. 23, and (a) is a diagram of a cylindrical body having a lid.
- (B) is a side view of the state shown in (a)
- (c) is a cross-sectional view with a part of the internal structure of the cylindrical body omitted
- (d) is a state shown in (c).
- E) is a front view illustrating a plate fitted into the cylindrical body
- (f) is a side view of the state shown in (e)
- (g) is a cross-sectional view of the lid
- (H) is a side view of the state shown in (g).
- FIG. 25 is a partially omitted cross-sectional view illustrating a state in which a fluid to be mixed and atomized flows in the mixing and crushing and atomizing apparatus shown in FIG.
- FIG. 26 is a partially enlarged view of FIG. 25.
- FIGS. 27 (a) and (b) are diagrams for explaining still another mixing / crushing micronization device of the present invention, wherein (a) is a cross-sectional view with a part omitted, and (b) is a) It is a side view of the state of illustration.
- Fig. 28 (a) is a front view of the mixing and pulverizing device shown in Figs. 27 (a) and (b), in which a part of the structure to be fitted into the cylindrical body is omitted, and (b) is ( a) is a side view of the state shown in the figure, and (c) is a sectional view taken along line D-D of (a).
- FIGS. 29 (a) and (b) are views for explaining the assembled state of the mixing and pulverizing and atomizing apparatus shown in FIGS. 27 (a) and (b), and (a) is fitted into a cylindrical body.
- FIG. 2B is a front view in which a part of the structure is omitted
- FIG. FIG. 30 is a view for explaining an embodiment in which the shape of the small chamber of the front opening in another embodiment is defined.
- FIG. 31 (a) is a view for explaining an embodiment in which the shape of a small chamber with a front opening in another embodiment is defined
- FIG. 31 (b) is a view showing a small chamber having the shape defined by (a).
- FIG. 32 (a) is a view for explaining an embodiment in which the shape of the small chamber with the front opening in another embodiment is defined
- FIG. 32 (b) is an oblique view showing the small chamber having the shape defined by (a).
- FIG. 33 (a) is a view for explaining an embodiment for defining the shape of a small chamber with a front opening in another embodiment
- FIG. 33 (b) is an oblique view showing a small chamber having the shape defined by (a).
- FIG. Fig. 34 (a) is a plan view of a plate body provided with a small chamber with a front opening having the shape defined in Figs. 31 (a) and (b)
- (b) is a side view of (a). It is.
- FIG. 35 (a) is a plan view of a plate body having a small opening chamber formed on both sides in the shape defined in FIGS. 31 (a) and (b), and (b) is a plan view of (a).
- FIG. 35 (a) is a plan view of a plate body having a small opening chamber formed on both sides in the shape defined in FIGS. 31 (a) and (b), and (b) is a plan view of (a).
- FIG. 36 is a cross-sectional view of the mixing and pulverizing device of the present invention in which a fluid flow path is formed using the plate shown in FIGS. 35 (a) and (b). ) Is a side view.
- FIG. 37 is a view for explaining the flow state of the fluid in the mixing / crushing / micronizing apparatus shown in FIG. 36.
- FIG. 38 is a micrograph of the fluid before the experiment was performed using the mixing / crushing micronization device shown in FIG. 36.
- FIG. 39 is an enlarged view of the micrograph of FIG. 38.
- FIG. 40 is a micrograph of the fluid one minute after the start of the experiment using the mixing / crushing micronization device shown in FIG. 36.
- FIG. 41 is a micrograph of the fluid 3 minutes after the start of the experiment using the mixing / crushing micronization device shown in FIG. 36.
- FIG. 42 is a micrograph of the fluid 5 minutes after the start of the experiment using the mixing / crushing micronization device shown in FIG. 36.
- FIG. 43 (a) is a front view of a mixing and pulverizing microparticulating apparatus according to still another embodiment of the present invention, and (b) is a side view of (a).
- FIG. 44 is a front view illustrating a state in which two mixing / crushing micronization devices shown in FIG. 43 (a) are connected.
- Fig. 45 (a) is a cross-sectional view of the mixing and pulverizing and atomizing device shown in Fig. 43 (a) with a part of the inlet side and the outlet side omitted, and (b) is a sectional view of Fig. 43 ( a) It is a cross-sectional view in which a part of a central portion of the illustrated mixing / pulverizing / micronizing device is omitted.
- FIG. 46 (a) is a plan view illustrating a mounting state of a frame body in the mixing / milling fine particle generating apparatus shown in FIG. 43 (a), and (b) is a plan view illustrating a mounting state of a structure.
- FIG. 47 (a) is a front view illustrating a fluid material flow path formed by the frame in the mixing / milling apparatus shown in FIG. 43 (a), and (b) is a fluid formed by the structure.
- FIG. FIG. 48 (a) is a plan view of the first plate-like body employed in the mixing / crushing fine-granulating apparatus shown in FIG. 43 (a), (C) is a perspective view of (a).
- FIG. 49 (a) is a plan view of a second plate-like body employed in the mixing and pulverizing / micronizing apparatus shown in FIG. 43 (a), (b) is a sectional view taken along line FF of (a), (C) is a perspective view of (a).
- Fig. 50 (a) is a plan view showing the laminated state of the frames used in the mixing and pulverizing and atomizing device shown in Fig. 43 (a), and (b) is a GG cross section of (a). (C) is a perspective view of (a).
- FIG. 51 (a) is a cross-sectional view showing an embodiment for explaining the flow state of the mixing / micronization fluid in the mixing / milling / micronization device shown in FIG. 43 (a), and FIG. FIG. 13 is a cross-sectional view illustrating another embodiment for explaining a flow state of a fluid to be mixed and atomized.
- FIG. 52 is a front perspective view of a mixing / pulverizing microparticulating apparatus according to another embodiment of the present invention.
- FIG. 53 is an explanatory view defining the shape of the small chamber having the front opening forming the fluid flow path in the embodiment shown in FIG. 52.
- Fig. 54 (a) is a front view illustrating a cylindrical body in the mixing and pulverizing fine particle device shown in Fig. 52, and (b) is a channel body unit in the mixing and pulverizing fine particle device shown in Fig. 52.
- FIG. 52 (c) is an exploded view for explaining the structure of FIG. 52, and FIG. 52 (c) is a front view for explaining a connecting portion in the mixing and pulverizing fine particle forming apparatus shown in FIG.
- FIG. 55 is a perspective view illustrating the flow state of the fluid subjected to the mixing / micronization treatment in the mixing / milling / micronization device shown in FIG. 52.
- FIG. 56 is a front view for explaining an embodiment when the mixing / crushing fine-graining device shown in FIG. 52 is used as a device for ultra-fine-graining soybean.
- FIG. 57 (a) is a block diagram illustrating one embodiment of the mixing and pulverization in which the method of pulverization using the mixing and pulverization pulverization apparatus of the present invention is employed
- FIG. 57 (b) is another block diagram.
- FIG. 9 is a block diagram illustrating an embodiment
- FIG. 9C is a block diagram illustrating still another embodiment.
- FIG. 58 is a block diagram illustrating an embodiment in which a waste plastic is atomized by continuous supercritical processing using the mixing / crushing atomization apparatus of the present invention.
- Fig. 59 (a) is a cross-sectional view for explaining the operation of the conventional static mixing device, (b) is a perspective view of a large-diameter disk provided in the conventional static mixing device, (c) FIG. 1 is a perspective view of a small-diameter disc provided in a conventional static mixing apparatus.
- FIGS. 15 (a) to 29 (b) show a first embodiment of the present invention.
- FIG. 15 (a) is a schematic cross-sectional view with a part omitted.
- First and second structures that form a fluid flow path are provided in a cylindrical body 1 having a hollow portion therein and an inlet opening 2 at one end and an outlet opening 3 at the other end. Mixing 'pulverizing and atomizing equipment.
- the first and second structures that form the fluid flow path provided in the hollow portion inside the cylindrical body 1 include a first plate body 4 and a second plate body 5 that are cylindrical bodies.
- a plurality of sheets are arranged so as to be orthogonal to one axial direction.
- the first plate body 4 has an outer peripheral shape corresponding to the inner peripheral shape of the hollow space inside the tubular body 1, and an outer peripheral portion of the tubular body 1 as shown in FIG. It is a plate that is tightly mounted on the inner circumference of the inner hollow part.
- a plurality of pentagonal small chambers 6 each having an open front surface are arranged in a honeycomb shape, and have an opening 7 formed in the center.
- the second plate member 5 is a plate having an outer peripheral shape in which a gap is formed between the outer peripheral portion and the inner peripheral portion of the inner hollow portion of the cylindrical member 1 when the second plate member 5 is mounted on the inner peripheral portion of the inner hollow portion of the cylindrical member 1.
- a pentagonal small chamber 6a having an open front surface is arranged in a plurality of honeycomb shapes, and has a recess 9 in the center.
- Fig. 15 (a) The mixing and pulverizing device shown in Fig. 15 is placed on the diagonal of the cylindrical body 1 whose appearance is rectangular or cylindrical (Fig. 22). (B) Provide flanges 10 and 10 protruding outward as shown in the figure, and attach to flanges 10 and 10 Assembled with girder bolts 1 1 and disassembled.
- the inner peripheral cross section of the inner hollow portion of the cylindrical body 1 has a substantially square shape, and the first plate 4 and the second plate 5 is formed in a substantially square shape as shown in FIGS. 16 (a) and (b), and is attached to the cylindrical body 1.
- quadrangular pyramid-shaped lids 12 are detachably provided.
- an inlet opening 2 and an outlet opening 3 having an arbitrary shape are provided.
- the object to be mixed and the object to be atomized are injected from the inlet opening 2, and the object that has been mixed and atomized is discharged from the outlet opening 3.
- the members constituting the mixing and pulverizing and atomizing apparatus of the present invention are made of carbon material, carbon and copper, carbon and aluminum, carbon and magnesium. It can be formed of a metal composite material composed of carbon and various metals such as carbon and tungsten, carbon and titanium oxide, or a mineral material such as ceramics and tourmaline, a resin, and the like.
- the first and second structures forming the fluid flow path provided in the hollow portion inside the cylindrical body 1 are a first plate body 4 and A plurality of second plate members 5 are arranged so as to be orthogonal to the axial direction of the cylindrical member 1.
- the first plate 4 and the second plate 5 are arranged in the horizontal direction in the axial direction of the cylindrical body 1, that is, in the horizontal direction in FIG. 15 (a).
- a plurality of sheets may be stacked in the direction and mounted in the hollow portion inside the tubular body 1.
- FIG. 16 (a) is an enlarged plan view of the first plate member 4, and FIG. 16 (b) is an enlarged plan view of the second plate member 5.
- 17 (a) and 17 (b) are a sectional view taken along the line AA in FIG. 16 (a) and a sectional view taken along the line BB in FIG. 16 (b).
- FIG. 18 is a perspective view of the first plate 4, and
- FIG. 19 is a perspective view of the second plate 5.
- the first plate 4 is slightly larger than the mounting portion 14 provided inside the cylindrical body 1 of the mixing and pulverizing fine particle generator 13.
- a hexagonal through-hole 7 having a shape in which four pentagonal front-opening small chambers 6 are gathered and having four long sides and two short sides.
- the second plate 5 is obtained by deleting arbitrary portions 5a on four sides of the square base plate, At the center of a base plate 15a (FIG.
- a concave portion 9 having a shape in which 14 small chambers 6a having a pentagonal front opening are assembled is provided.
- substantially the same number of pentagon-shaped front opening small chambers 6 a are continuously arranged in the outer side direction from the recess 9.
- a stabilizing pin 8 (FIG. 19) for stabilizing the superposition with the first plate body 4 is provided at a position close to each convex side.
- the shape of the base plate 15a of the second plate body 5 may be a shape in which four corner portions 5a are cut off. As such, there is a space in which the fluid material can flow into the next plate located on the downstream side, and any shape may be used as long as the outer diameter of the first plate 4 is the same.
- FIG. 20 is a perspective view for explaining a state in which the first plate 4 and the second plate 5 are stacked to form one unit
- FIG. 21 (a) is a perspective view of the stacked plate.
- the plan view of the unit, FIG. 21 (b) is a cross-sectional view taken along the line CC in FIG. 21 (a).
- the opening 7 formed in the center of the first plate 4 and the central concave portion 9 of the second plate 5 face each other, and the pentagonal small chamber 6 of the first plate 4
- the opening and the opening of the pentagonal small chamber 6 a of the second plate 5 are opposed to each other, and the opposed small chamber 6 of the first plate 4 and the small chamber 6 a of the second plate 5 are staggered. Both are laminated so that For example, the small chambers 6 of the first plate 4 and the small chambers 6a of the second plate 5 are rotated 90 degrees and are brought into close contact with each other so as to be in opposite directions.
- each of the small chambers 6 of the first plate 4 and the small chambers 6a of the second plate 5 communicates with at least one or more small chambers of the plate facing each other.
- the back surface of the second plate member 5 ' is laminated on the back surface of the second plate member 5 back to back.
- the other first plate 4 ′ is connected to the other first plate 4 ′ at the center of the other first plate 4 ′ with respect to the other second plate 5 ′.
- the central recess 9 of the second plate 5 ′ faces each other, the opening of the pentagonal chamber 6 of the other first plate 4 ′, and the pentagon of the other second plate 4 ′.
- a unit is formed by the first plate 4, the second plate 5, the second plate 5 ', and the first plate 4' which are stacked as shown in FIG.
- a plurality of units or a single unit is arranged in the cylindrical body 1.
- the pentagonal small chamber 6 of the first plate body 4 and the pentagonal small chamber 6 of the second plate body 5 face each other, for example, are rotated 90 degrees, and are stuck alternately.
- 16 (a) and (b) as shown in the figure the space on the front side of the pentagonal small chamber 6 that is laid out in a honeycomb shape without gaps is shown in FIG. 21 ( a) As shown, each is divided into three parts.
- the fluid flowing into the mixing / milling device 13 under pressure flows into the second plate through the through hole 7 of the first plate 4 as shown in FIG. It hits the concave portion 9 of the plate 5, flows into each of the upper and lower pentagonal small chambers 6 where the front space is divided into three, and repeatedly collides, while radially dispersing outward.
- it strikes the base plate 15 of the first plate body 4 and flows into each of the upper and lower pentagonal small chambers 6 where the front space is divided into three, repeating collisions, It flows toward the center.
- the cylindrical body 1, the first plate body 4, the second plate body 5, etc. are made of a carbon material, carbon and copper, carbon and aluminum, carbon and aluminum.
- a catalyst effect can also be exhibited by molding a composite material consisting of carbon and various metals such as gnesium, carbon and tungsten, and carbon and titanium oxide, or a mineral such as ceramics and tourmaline.
- FIG. 22 is a perspective view of a cylindrical body 1 of the mixing / crushing fine-graining apparatus 13 in which the outer shape is cylindrical.
- N poles 16 & and 3 poles 16 b of magnets 16 which generate a magnetic force at positions obtained by equally dividing the outer circumference of the cylindrical body 1 into eight parts are opposed to each other. It can be engaged in the state. In this way, when a fluid is pressurized and flows into the mixing and atomizing device 13, the magnetic force of the N pole 16 a and the S pole 16 b of the magnet 16 causes the fluid Molecules can be further subdivided and dispersed, and the mixing efficiency and the efficiency of micronization can be improved. Further, as another external shape that can be adopted in the mixing and pulverizing particle forming apparatus of the present invention, a shape in which a flange is provided from the center in the horizontal direction of the cylindrical body 1 and divided into two in the horizontal direction may be used.
- FIG. 23 to 26 show another embodiment of the present invention.
- FIG. 23 is an exploded perspective view
- FIGS. 24 (a) to (h) are exploded views thereof.
- FIG. 26 is a cross-sectional view showing the flow of a fluid object and a partially enlarged partial cross-sectional view.
- the inner peripheral walls of the four sides of the cylindrical body 1 of the mixing and pulverizing and atomizing apparatus are plate bodies 17 each having a pentagonal small chamber 6 with a front opening arranged in a honeycomb shape.
- the structure fitted into the cylindrical body 1 is a plate body 18 in which four outer peripheral walls are arranged in a honeycomb shape with a pentagonal small chamber 6 having a front opening.
- Lids 12 are attached to the flanges 10 at both ends of the mixing and pulverizing and atomizing device.
- the fluid to be subjected to the mixing process and the micronization process is injected under pressure from the inlet 2 formed in the lid 12.
- FIGS. 27 (a) to 29 (b) show that pentagonal small chambers 6 with front openings are continuously arranged in a honeycomb shape on each inner surface in the cylindrical body 1 of the mixing and pulverizing micronization device.
- Another embodiment according to the present invention in which the assembly plate 17 can be engaged and the plate 18 fitted in the cylindrical body 1 can also be engaged with the base 19 as well. It is.
- a plurality of substantially triangular concave portions 20 provided at arbitrary positions are provided in the cylindrical body 1 and on four surfaces of the base portion 19, and a pentagonal small chamber 6 is provided in the plate 17 and the plate 18.
- a substantially triangular convex portion 21 that can be fitted into the substantially triangular concave portion 20 on the back side of the surface, the plate members 17 and 18 formed of different materials are formed. It is easily replaceable. (Example 2)
- the pentagonal shape is adopted as the small chamber 6 having the front opening, but the shape of the small chamber 6 is not limited to this.
- FIG. 30 is a diagram showing definitions of various shapes of a small chamber having a front opening formed in a plate body.
- the midpoints P and Q of the hypotenuse of ABC are the absolute points, and the virtual point S on the perpendicular from the vertex A to the base BC is defined as the midpoint R of the vertex A and the base. Set in places that are excluded.
- the shape surrounded by these points P—S—Q—S 2—S 1—P is the shape of the small chamber with the front opening formed in the plate.
- the shapes of the small chambers formed in this way can be various shapes as shown in FIGS. 1 to 14, but in any case, when the small chambers are laid in a honeycomb shape on a plate body. However, it is possible to lay small chambers on the entire board without gaps.
- FIGS. 31 (a) to 33 (b) show specific examples of the shape of the small chamber described above with reference to FIG.
- FIGS. 31 (b), 32 (b) and 33 (b) are diagrams of FIGS. 31 (a), 32 (a) and 33 (a).
- FIG. 3 is a perspective view of a small chamber formed in a manner similar to the above.
- a point S is set at any position except points A and R on a line A—R connecting vertex A and midpoint R.
- the line P-S connecting the midpoint P and the point S is a combination of an arc and a straight line from the midpoint between P and S to the point S and to the midpoint P.
- the Q_S line connecting the midpoint Q and the point S is a combination line of a straight line that is a straight line from the midpoint between Q and S to the point S side, an arc line to the midpoint Q side, and an arc line.
- the P-S line is rotated clockwise with the middle point P as the base point, and the Q-S line is rotated counterclockwise with the middle point Q as the base point.
- the contact points on the base B-C are S 1 and S 2.
- points P, S, Q, S2, S1, and P are connected, an asymmetrical outer shape is formed.
- the portion sandwiched between the segment S 1 ′ — S 2 ′, the line segment Q, and the shape surrounded by one S 25 rises as the wall of the small room 22.
- the bases S 1 -S 2 may not be straight lines, but S 1 -R may be sine curves, and S 2 -R may be base lines of different line types having a straight line.
- the area of the shape of the portion connected by the line segment P—S—Q—S 2—S 1—P is a virtual right-angled isosceles. It is desirable that the area of the triangle ⁇ C be half of the area.
- the midpoints P, Q, and R on the hypotenuse A-B, A-C and base B-C of the virtual right-angled isosceles triangle The point S is set at any position except the point A on the line A—R connecting the vertex A and the midpoint R.
- the line P-S connecting the midpoints P and Q and the point S is a convex arc line, and the Q-S line is a straight line.
- the P-S line is rotated clockwise with the midpoint P as the base point
- the Q_S line is rotated counterclockwise with the midpoint Q as the base point.
- the contact points on the base B-C are S1 and S2.
- Connecting points P, S, Q, S2, S1, and P forms an asymmetrical outer shape.
- the part sandwiched by the shape surrounded by the segment S 15 -S 2 'and the line segment Q, — S 2' rises as the wall of the small chamber 23 as shown in Fig. 32 (b). is there.
- the midpoints P, Q, and R on the hypotenuse A-B, A-C and the base B-C of the virtual right-angled isosceles triangle A point S is set at any position on the line A-R connecting the vertex A and the midpoint R except for the points A and R.
- the line P-S connecting the midpoints P and Q and the point S is a free line
- the Q-S line is the line with the corner of the free line as R.
- the part sandwiched by the shape surrounded by S 2 ′ stands up as the wall of the small room 24 as shown in FIG. 33 (b).
- FIGS. 34 (a) and (b) show the small chambers 22 formed in the above-described manner spread over the surface of the plate.
- the upper and lower sides are formed by a fence 25 having the same height as the height of the inner peripheral wall of the cylindrical body 1 constituting the mixing and atomizing apparatus of the present invention.
- FIGS. 35 (a) and (b) show the small chambers 22 formed in the manner described above, which are arranged on the front and back surfaces of the plate.
- the small chambers 22 arranged on the front side and the small chambers 22 arranged on the back side are arranged so that they are alternately positioned when they are stacked, and are further rotated by 180 degrees with respect to each other. It is provided in the position where it is done.
- the upper and lower sides are formed by a wall 26 having the same height as the height of the inner peripheral wall of the cylindrical body 1 constituting the mixing and atomizing apparatus of the present invention.
- FIGS. 36 (a) and (b) show a plurality of plates shown in FIGS. 35 (a) and (b) stacked in the cylindrical body 1 in the axial direction of the cylindrical body 1.
- 1 shows a specific example of a mixing and micronizing apparatus according to the present invention.
- the appearance is a cylindrical body 27 with flanges formed at both ends.
- the internal space 28 of the cylindrical body 27 is a frustoconical body, and the plate shown in FIGS. 35 (a) and 35 (b) is regularly arranged around the inner surface of the internal space 28. The arrangement is formed in an array.
- the fitting body 29 closely fitted to the internal space 28 has a conical shape.
- the flanges formed at both ends are provided with O-rings 30a and the like for sealing a fluid.
- a cover 30 that hermetically covers the inside of the internal space 28 is attached with bolts 31 and nuts 32.
- the inner space 33 of the lid 30 has a conical shape slightly larger than the conical shapes formed at both ends of the fitting body 29.
- An object to be subjected to the mixing process and the fine-particle process is flowed under pressure from the inlet 34.
- a spiral flow path mechanism is attached by bolts 35.
- FIG. 36 (a) In the mixing and pulverizing and atomizing apparatus shown in the figure, the internal space 28 has a frusto-conical shape, and the fitting body 29 has the same frusto-conical shape.
- the small chambers 22 formed on both sides of the plurality of plates stacked in the axial direction of the cylindrical body 1 2 2
- the opening sides of the chambers are in close contact with each other, and each of the chambers passes through a flow path that can communicate with at least one or more opposing chambers, thereby performing mixing and / or generation of fine particles and granulation. Can be.
- the mixing and pulverizing device shown in FIG. 36 (a) can be used as a mixer, a pulverizer, or a device for granulating spherical fine particles. Further, it can be used as a device for producing a critical fluid or a supercritical fluid that reacts and treats an object under supercritical conditions in which the pressure and temperature exceed the critical point of gas-liquid.
- the structures, etc., constituting the pulverizing and atomizing device are made of constituent materials that can withstand the critical temperature and supercritical temperature of the substance to be mixed, pulverized and atomized, respectively, the mixing shown in Fig. 36 (a) ⁇ It can be used as a reaction vessel that performs critical processing and supercritical processing while performing mixing, pulverization, and micronization processing using a pulverization / micronization device.
- FIG. 37 is an explanatory diagram for explaining the flow path of the mixture processing object / particulate processing object flowing into the cylindrical body 27 in the embodiment shown in FIG. 36 (a).
- the plate body is arranged such that the front opening sides of the small chambers 22 face each other, and one of the small chambers 22 is brought into close contact with the other opposing small chamber 22 by rotating it 180 degrees, and is laminated to form a cylindrical body. It is located within 27.
- the object to be mixed which has been pressurized and flowed in from the inflow port 34 The fluid 36 containing the object to be atomized flows into the first division of the flow path, which is larger than the other divisions 37 Then, it flows into the next division 38.
- the fluid 36 that has flowed into the dividing portion 37 is blocked by the fence 39 in which the walls formed by the above-mentioned midpoints P and P 'and Q and Q' overlap vertically and form the small chamber 22. It collides with the wall, gets over it, and flows into the next division 38.
- the area and volume of the dividing part 38 are about 90% smaller than the area and volume of the dividing part 37, and the number of divisions is doubled, so that the flow velocity of the fluid 36 becomes faster.
- the flow velocity becomes slower in the dividing section 40 where the area and the volume ratio are increased by 2.15 times as compared with the dividing section 38, and the flow velocity becomes higher again in the dividing section 41, and the flow proceeds to the next dividing section 42.
- the flow velocity decreases.
- the mixed object in the fluid 36 flowing into each of the divided sections having different areas and volumes and the object to be atomized are subjected to pressure when they flow into the small divided section and the flow velocity becomes faster.
- An increased compression and coagulation effect is added.
- the repetition of these compression and coagulation actions and release actions enables the production and granulation of high-quality fine particles (for example, spherical fine particles).
- soybean micronization was carried out under the following conditions by the micronization method of the present invention using the mixing / milling micronization apparatus of the present invention shown in the figure.
- This device cylindrical type Material S U S 3 16
- Fig. 36 (a) Middle, left and right length 230mm
- Fig. 35 (a), (b) Front and back channel assembly (plate) shown: 2 sets Fig. 34 (a), (b) Front channel assembly (plate) shown: 2 sets Electron microscope : Magnification 1000 times (1 scale two 1.538 microns)
- Fig. 38 to Fig. 42 show that 2.Okg of pre-ground soybean flour was mixed with 10 liters of water, and then circulated and pressurized into this device by a pressure pump under the above conditions. This is a photomicrograph of the soybean fiber collected at 1 minute, 3 minutes, and 5 minutes after circulating pressure inflow, and the state of the soybean fiber was confirmed with an optical microscope.
- Reference numeral 43 in FIG. 38 shows the state before soybean fiber is fed under pressure.
- Fig. 39 is an enlarged photograph of this part, showing countless fibrous soybean fibers 43 of different sizes.
- FIG. 40 shows a state after a lapse of 1 minute from the circulation pressurization. Some soy fiber 43 is still visible, but a lot of soy particulates 44 are found.
- FIG. 41 shows a state where three minutes have passed after the circulation pressurization flow. Most fibrous soybean fibers are finely divided without being diagnosed, and are almost uniform.
- Fig. 42 shows the state after 5 minutes of circulating pressurized inflow and the fibrous soybean fiber disappeared. Only spherical soybean fine particles 44 were obtained.
- FIG. 43 (a) is a front view of a mixing-crushing micronizing apparatus according to another embodiment constructed based on the present invention
- FIG. 43 (b) is a side view of the same.
- the main body case 45 of this mixing and pulverizing and atomizing device has a cylindrical shape, and a lid 48 having an inlet 46 and an outlet 47 can be attached to both ends. A plurality of bolt holes 49 are provided at arbitrary positions above and below the main body case 45.
- the main body case 45 has a configuration capable of being divided into two parts in the horizontal axis direction as shown in FIGS. 45 (a) and (b) and FIGS. 46 (a) and (b).
- a plurality of mixing / milling fine-graining apparatuses may be connected by connecting metal fittings 50.
- the processing target to be mixed and fine-grained is mixed more uniformly.
- it can be made into fine particles.
- Fig. 45 (a), (b), Fig. 46 (a), (b), Fig. 47 (a), (b) show the mixed / milled fine particles shown in Fig. 43 (a), (b) It shows a state in which the conversion device is divided into two parts in the horizontal axis direction.
- FIGS. 45 (a) and (b) are side views with some parts omitted, and FIG. 45 (a) is a side view of the inlet 46 side or the outlet 47 side.
- FIG. 45 (b) is a cross-sectional view of the central part of the main body case 45 as viewed from a side with a part thereof omitted.
- FIGS. 46 (a) and (b) correspond to plan views, and FIG. 46 (a) shows the mounting and dismounting of the frame 58 described in FIGS. 50 (a) to (c).
- FIG. 9 is a diagram for explaining a state.
- FIG. 46 (b) is a diagram illustrating a state in which the structure 52 forming the fluid flow path described with reference to FIGS. 48 (a) to 49 (c) is attached and detached.
- FIGS. 47 (a) and (b) correspond to the front view, and FIG. 47 (a) shows the fluid distribution constituted by the frame 58 described in FIGS. 50 (a) to 50 (c).
- Road section FIG. FIG. 47 (b) is a diagram illustrating the structure 52 described in FIGS. 48 (a) to 49 (c).
- a first recess 51 is provided on the inner peripheral wall of the main body case 45 (FIG. 46 (a)).
- the first recess 51 has a first plate-shaped body 52 shown in FIGS. 48 (a) to (c) and a second plate shown in FIGS. 49 (a) to (c).
- the state body 53 is fitted and fixed.
- the first plate-shaped body 52 has a plurality of pentagonally-opened small chambers 54, 55 arranged on both sides, respectively. Is what it is.
- the small chambers 55 of the front opening have the same shape as each other, they are provided at different positions that are staggered up and down, and at positions that are rotated 180 degrees from each other.
- the second plate-shaped body 53 has at least one surface, in the case of this embodiment, on the upper surface side, a pentagon-shaped small opening chamber 5. 6 is a multiple arrangement.
- the first plate-shaped body 52 and the second plate-shaped body 53 are each composed of a small chamber 54 having a front opening provided in each plate-shaped body. 55, 56 oppose each other, and the opposing small chambers 54, 55, 56 alternate with each other, and communicate with at least one or more small chambers of the other plate-like bodies, each of which opposes. They are arranged close to each other.
- the small chamber 54 formed on the upper surface side and the small chamber 55 formed on the lower surface side are alternately arranged vertically.
- the first plate-shaped member 52 and the first plate-shaped member 52 are provided at different positions and rotated 180 degrees from each other.
- a fluid flow path passing through the small chambers 54 and 55 is formed in a portion where and are closely arranged to each other.
- the fluid flow path is formed so that the first plate-shaped body 52 and the second plate-shaped body 53 are formed in close contact with each other.
- the position of the pentagon-shaped front opening small chamber 56 formed in the second plate-shaped body 53 is different from that of the small chambers 54, 55 formed in the first plate-shaped body 52.
- predetermined At an angle, for example, 45 degrees, or at a position that is staggered when placed opposite each other for both compartments 54, 55. There is.
- the back side (the lower side in FIG. 49 (b)) of the second plate-shaped body 53 is brought into close contact with the second plate-shaped body 53, and this is sandwiched in the middle. It is also possible to form a fluid flow path as a form in which the first plate-like bodies 52, 52 are closely arranged on both sides.
- a second recess 57 is provided on the inner peripheral wall of the main body case 45 (FIG. 46 (b)).
- Frames 58, 58 described with reference to FIGS. 50 (a) to (c) are fitted and fixed in the second recess 57.
- the frame 58 has a plurality of openings 59 formed in a honeycomb shape that communicate with each other in the axial direction of the main body case 45.
- the frame portions 58 adjacent to each other are connected alternately so that the plurality of frame members 58 are orthogonal to the axial direction of the main body case 45. It is stacked and arranged so as to be in a position.
- FIGS. 45 (a) and 50 (a) to (c) In the illustrated embodiment, the shape of the opening 59 is a pentagon.
- FIG. 48 (a) is a front view of the first plate-shaped body 52
- FIG. 48 (b) is a sectional view taken along the line E-E
- FIG. 48 (c) is a perspective view thereof. is there.
- the first plate-shaped body 52 is formed by arranging a plurality of small chambers 54, 55 each having a pentagonal front opening on both sides thereof.
- the small chambers 54 formed on the upper surface side and the small chambers 55 formed on the lower surface side are at different positions that are alternately arranged vertically, and are also rotated by 180 degrees with each other. It is provided in the position where it was done.
- the size of the small chambers 54, 55 having the front opening is not limited to the first plate-shaped body 52 of the present embodiment, but may be determined according to the characteristics and mixing ratio of the object to be mixed and finely divided. It may be formed by changing the number of the small chambers 54 and 55.
- FIG. 49 (a) is a front view of the second plate 53
- FIG. 49 (b) is a sectional view taken along line FF of FIG. 49
- FIG. 49 (c) is a perspective view.
- the shape of the front opening small chamber 56 formed on one side is the first plate-like small chamber 52 Although the shape is the same as that of 54, 55, as described above, the position of the small chamber 56 at the front opening is located in either of the small chambers 54, 55 formed in the first plate-shaped body 52. In contrast, when they are arranged at a predetermined angle, for example, 45 degrees, or when they are placed opposite to each other with respect to the compartments 54, 55. It is formed in an alternate position.
- the size of the small chamber 56 with the front opening is changed according to the characteristics and the mixing ratio of the object to be mixed and finely divided, without being limited to the second plate-like body 53 of the present embodiment.
- the number of the small chambers 56 may be increased or decreased.
- FIG. 50 (a) is a front view showing a state in which a plurality of frame bodies 58 which can be easily fitted and fixed to the second recess 57 are stacked
- FIG. 50 (b) is FIG. 50 (c) is a perspective view of a cross section taken along line G-G.
- the frame 58 has a plurality of pentagonal openings 59, 59 penetrating the frame 58.
- the adjacent frame members 58 and 58 are stacked such that the opposing openings 59 and 59 are in alternate positions as shown in FIGS. 50 (a) and (b). Are located.
- the outer shape of the frame body 58 is molded in the same manner as the second recess 57 provided on the inner peripheral wall of the main body case 45, and can be easily fitted and fixed to the second recess 57, It is also removable.
- the frame 58 may be formed by changing the size of the opening 59 according to the characteristics of the mixture, the mixing ratio, and the like, and increasing or decreasing the number of the opening 59.
- a portion indicated by reference numeral 61 is a positioning projection
- a portion indicated by reference numeral 62 is a positioning recess.
- the main body case 45 can be divided into two parts in the horizontal axis direction, and the first plate-shaped body 52 and the second plate-shaped body 53 are fitted into the first concave part 51 and the second concave part After fitting the frames 58, 58 to 7, the positioning protrusion 61 is fitted to the positioning recess 62, and the bolt is inserted through the bolt hole 49, and it can be fixed and assembled. . Therefore, it is easy to assemble, and it is also easy to disassemble for maintenance.
- FIGS. 45 (a) to 47 (b) a portion indicated by reference numeral 63 is a packing, and a seal is achieved by this.
- FIG. 51 (a) shows the flow formed by the frames 58, 58 mounted in the body case 45. Fluid 6 in which an object to be mixed / particulate treated is mixed into the body flow path and the fluid flow path formed by the first plate-shaped body 52 and the second plate-shaped body 53.
- FIG. 3 is a schematic cross-sectional state diagram illustrating a state where 0 flows in and flows.
- Fluid 6 0 is fed by suitable consisting pumping means from the inlet 4 6 of the cover 4 8, firstly, the fluid distribution passage formed by the openings 5 9, 5 9 of the frame 5 8, 5 8 It circulates and at this time a certain dispersing action occurs.
- the fluid flows into the fluid flow path formed by the first plate-shaped body 52 and the second plate-shaped body 53, and collides with the walls forming the small chambers 54, 55, and 56. Then, the dispersion, the vortex flow, and the inversion are repeated, and the mixture proceeds in the direction of the discharge port 47 while the mixture is being mixed or while the fine particle object is being finely divided.
- the fluid flows through the fluid flow path formed by the openings 59, 59 of the frames 58, 58 provided on the discharge port 47 side, and finally, the discharge port of the lid 48. It is discharged from 47.
- FIG. 51 (b) shows a case where the close contact arrangement between the first plate-shaped member 52 and the second plate-shaped member 53 is reversed from that shown in FIG. 51 (a).
- FIG. 3 is a schematic cross-sectional state diagram illustrating a state in which fluid 60 flows in and circulates.
- FIGS. 52 to 55 show a case where small chambers serving as flow paths are formed in the manner described with reference to FIGS. 30 to 33 (b), and small chambers having front openings formed in this manner are arranged.
- 4 is a view for explaining another mixing / crushing fine-graining apparatus of the present invention which employs a plate body.
- FIG. 52 is a front perspective view with a part omitted.
- FIGS. 54 (a) to (c) are exploded views of FIG. 52.
- the mixing and pulverizing device shown in FIG. 52 comprises a cylindrical body 64 having a cylindrical appearance.
- a cylindrical hollow portion 65 is formed in the cylindrical body 64.
- the channel body unit 67 is completely fitted in the hollow portion 65. This complete fitting prevents the so-called short path phenomenon from occurring.
- connection screws 68, 68 for connecting and connecting a plurality of other devices and the present device can be freely attached.
- the connection screw 68 also has an effect that the flow path unit 67 fitted in the cylindrical body 64 does not protrude outward.
- the flow path unit 67 is provided with a small opening 70, 73, 75, 76, 7 A plate 90 on which 8, 8 1, 8 3 and 8 4 are arranged, and a small chamber 6 with a front opening on one side
- the plate body 91 in which the openings of these small chambers face each other, and,
- the opposing small chambers are alternately arranged, and the small chambers are arranged in close contact with each other so as to communicate with at least one or more small chambers of another opposing plate.
- the small chamber 69 of the front opening of the plate 91 communicates with the small chamber 70 of the front opening of the plate 90, and the small chamber 70 of the front opening of the plate 90 is connected to the front of the plate 91.
- the channel body 67 is formed by closely adhering the plate body 91.
- the fluid material flow path is formed by the continuation of the plurality of small chambers 69 to 85 communicating with at least one or more small chambers having the front opening provided on the opposing plate members.
- FIG. 53 defines the shapes of the small chambers 69 to 85,... Formed in the plates 90, 91 constituting the flow path unit 67.
- the small chamber 69, etc. has a shape in which the bottom is a straight line and the other sides are arc-shaped.
- Arbitrary points P and Q are set on the hypotenuses A—B and A—C of the right-angled isosceles triangle ⁇ ⁇ C.
- An arc curve connecting the arbitrary points P, Q on the hypotenuse and the arbitrary point S on the perpendicular A—R, the P—S line, Q—S line, and the P—S clockwise around the arbitrary points P, Q, Q—S Are rotated counterclockwise by 90 degrees, respectively, and the points that abut on base B—C are S 1 and S 2.
- the shape is surrounded by the arc curve P—S, Q—S, the arc curve P—Sl, Q—S2, and the line S1—S2 connecting the points S1 and S2.
- the P-S line and the Q-S line may be various linear shapes such as a straight line, a curve, a sine curve, an arc line, and a polygonal line.
- the area of the shape enclosed by the line segment P—S—Q—S2—S1—P formed as described above should be half the area of the right-angled isosceles triangle ABC. I just need. This is because small chambers can be spread over the plates 90 and 91 without gaps. Therefore, if this condition is satisfied, the arbitrary points P, Q, and S may be set at any positions on the sides A—B, A—C, and the perpendicular A—R.
- the line connecting the point S l and the point R on the base may be a straight line
- the point S 2 and the point R on the base may be a curve.
- the channel unit 67 can be formed by dividing a columnar shape having conical portions at both ends into two parts, and can be formed integrally by guide bins provided at arbitrary positions.
- the small chambers 69 to 85 formed in the plates 90 and 91 constituting the flow channel unit 67 are arranged such that the front openings thereof are opposed to each other and are closely arranged as shown in FIG. b) As shown above and below, it is desirable to arrange them so that they are rotated 180 degrees from each other.
- the opposing small chambers 70, 73, 75, 76, 78, 81, 83, 84, and 69, 71, 7 of the plate bodies 90, 91 arranged in layers are arranged. 2, 7, 4, 7, 7, 79, 80,
- the small chamber on 90, 91 communicates with at least one or more small chambers of another opposing plate.
- FIG. 55 is a schematic explanatory view for explaining a flow in a state in which a fluid 92 mixed with an object to be subjected to the mixing / particulation processing flows into the flow channel unit 67.
- the fluid 92 entering the small chamber 69 provided in the lower plate 91 enters the small chamber 70 of the opposed plate 90, and then the small chambers 71, 7 of the opposed plate 91. It is divided into 2 and then merges into the opposing small chamber 73 of the plate 90. From the small chamber 73 of the plate 90, it enters the small chamber 74 of the opposite plate 91, is divided into the small chambers 75, 76 of the opposite plate 90, and then merges. Then, it enters the small room 77 of the opposing plate body 91.
- the fluid 92 continuously undergoes dispersion, concentration, confluence, compression by pressurization, and release of pressure repeatedly. This promotes the mixing of the substances to be mixed or the ultrafine and molecularization of the substances to be microparticulated.
- FIG. 56 is an overall configuration diagram showing one embodiment in which the mixing and pulverizing fine-graining apparatus of the present invention described in the above-described first to fourth embodiments is employed in an apparatus for converting soybeans into ultrafine particles.
- the mixing and pulverizing device 100 using soybeans as ultra-fine particles can be moved by wheels 101 attached thereto.
- Mixing and crushing and atomizing equipment A power motor 103 capable of operating the pressure pump 102 is provided in a lower portion of the inside of the 100, and an Invar 107 is mounted.
- a hopper 104 for charging soybeans is attached to the upper part of the mixing and pulverizing device 100, and is installed near the discharge port 105 of the mixing and pulverizing device 100. Is a collection container 106 for collecting ultrafine soybean ultrafine particles.
- the fluid mixed with soybeans When the fluid mixed with soybeans is put into the hopper 104, the fluid passes through the piping, receives an appropriate pressure from the pressure pump 102, and flows into the inlet of the mixing / pulverization / micronization device 100. (Not shown). Then, the fluid flows in the fluid flow path in the flow path unit 57 described in FIGS. 52 and 54 (a) and (b) as described in FIG. At this time, the soybeans pumped to each of the small chambers 69-85, etc., are continuously destructed by the internal and external discharge pressures when the soybeans explode themselves under the action of strong compression by strong pressure and instantaneous release. It is converted to ultrafine particles and discharged from the outlet 105 into the collection container 106. As explained in Fig.
- the fluid in which soy is mixed is subjected to continuous compression by strong pressure and instantaneous release as it flows through the flow path of the fluid so that the soybeans themselves
- the destruction that continues to be destroyed by the explosive internal and external discharge pressures and becomes ultrafine particles is explained by the so-called dissipation theory.
- FIGS. 57 (a) to (c) show various processes in which the process for carrying out the method of the present invention by the mixing and comminution device of the present invention described in Examples 1 to 4 above is employed.
- FIG. 4 is a block diagram illustrating an embodiment.
- FIG. 57 (a) is a block diagram schematically illustrating an example of wet pulverization by the mixing / pulverization micronizing apparatus according to the present invention.
- the raw material is put into a coarse-grain pulverizer for coarsely pulverizing the raw material, and the coarse-grained raw material is pumped to a heater by a pump, and the coarse-grain pulverization is performed by the action of the channel unit 57 of the apparatus of the present invention.
- the raw material is converted into fine particles and stored in a container as a desired fine particle diameter.
- a filter or the like provided between the apparatus and the container of the present invention and the particles that do not pass through the filter are returned to the coarse particle grinder again by a return pipe, converted into ultrafine particles in the same process, stored in the container, and stored in the container in the next step ( Processing line).
- Fig. 57 (b) outlines an embodiment in which the present apparatus is combined with an ultrasonic, electromagnetic wave and laser light apparatus to form a reaction processing apparatus including continuous supercritical processing with carbon dioxide.
- FIG. 57 (b) outlines an embodiment in which the present apparatus is combined with an ultrasonic, electromagnetic wave and laser light apparatus to form a reaction processing apparatus including continuous supercritical processing with carbon dioxide.
- the raw material which has been coarsely ground beforehand, and an extraction solvent, for example, carbon dioxide, are mixed through a pressure pump and a dry pump to form a mixture, and the mixture is subjected to supercritical conditions by a pressure pump and a heater. Pressure and temperature. Then, it is pressure-fed into a cylindrical body constituting the apparatus of the present invention, and continuously supercritically processed while the mixture under supercritical conditions is converted into ultrafine particles in the cylindrical body. Next, the thus treated material is subsequently reacted or decomposed by ultrasonic waves, electromagnetic waves, laser light or the like.
- the product obtained in this way is collected in a collection container, and the liquefied extraction solvent is gasified by a pressure control valve (not shown) and recycled.
- FIG. 57 (c) is a block diagram schematically illustrating an embodiment in which the present apparatus is combined with a high-frequency, ultrasonic and laser light apparatus to form a reaction processing apparatus including continuous supercritical processing with various solvents.
- the liquid extraction solvent and the substance to be decomposed are mixed by a pressure pump, pressurized and heated to a supercritical condition of the substance to be decomposed by a heating pump, and pumped into a cylinder constituting the apparatus of the present invention. Then, a supercritical treatment is continuously performed while the mixture under supercritical conditions is converted into ultrafine particles in the cylindrical body. Next, the thus treated material is subsequently reacted with ultrasonic waves, electromagnetic waves, laser light, or the like, or decomposed.
- FIG. 58 is a block diagram for explaining another embodiment in which the process for performing the micronization method of the present invention by the mixing and pulverizing micronization device of the present invention described in Examples 1 to 4 is employed. It is.
- the waste plastic which has been pulverized in advance and the carbon dioxide used in the extraction solvent, the oxidation reaction, and the hydrolysis are directed toward the inlet opening of the cylindrical body constituting the apparatus of the present invention by a pressure pump and a pressure pump. It is heated by a heating element such as a heater while being sent under pressure.
- the applied pressure and temperature are set to 7.38 MPa and a temperature of 31 ° C, which are supercritical conditions of carbon dioxide.
- the fluid that has been mixed with the waste plastic that has been ground in advance and that is under supercritical conditions flows from the inlet opening of the cylindrical body that constitutes the apparatus of the present invention through the above-described fluid flow path. It is pumped towards the outlet opening.
- the waste plastic is continuously supercritically processed in the cylindrical body constituting the device of the present invention while being pulverized into fine particles.
- the treated material discharged from the outlet opening is separated into gas and plastic powder by a cooling device and a decompression device.
- the separated powder material is collected in a collection container, and the gas is returned and reused.
- carbon dioxide was used for the extraction solvent, the oxidation reaction, and the hydrolysis.However, for the object to be treated, the critical treatment and the supercritical treatment were performed while the pulverized fine particles were treated. As long as the extraction solvent can be used at this time, it is possible to use other than carbon dioxide.
- waste plastics such as polyethylene, polystyrene, polyethylene terephthalate, and polyvinyl chloride
- waste plastics such as polyethylene, polystyrene, polyethylene terephthalate, and polyvinyl chloride
- virgin materials and synthetic resins are used.
- waste plastics so-called virgin materials, synthetic resins, and the like have been frozen in pellet form and then pulverized into powder. This is because there was no technology for powdering pellets at room temperature. However, this refrigeration required very high costs.
- the micronization method of the present invention is performed by the mixing / milling micronization apparatus of the present invention and the processing is performed as shown in FIGS. 58 and 57 (b) and (c), the pulverization A critical process and a supercritical process are continuously performed while forming particles, and further, a gas and a processed material (powder-like material) can be continuously and easily separated.
- the mixing and pulverizing microparticulation apparatus of the present invention can be said to be an apparatus having both functions of dry pulverization and wet pulverization. Industrial applicability
- the material to be subjected to the mixing and pulverization treatment flowing there is compression by pressurization and instantaneous explosive release and compression. And release and turbulence in the flow channel, and the addition of holding pressure and release pressure are continuously applied, and the stress decomposition of the material to be micronized can be performed, and the generation and granulation of fine particles are performed. The effect is obtained. In other words, as described by the so-called dissipation theory, extremely excellent mixing and micronization are performed.
- fibrous substances can be reduced to fine spherical particles.
- a cylindrical body constituting the mixing and pulverizing / micronizing apparatus of the present invention, a first structure provided with a small chamber having a front opening, a second structure, a frame, etc. are made of carbon and copper,
- a catalytic effect can be obtained by forming from a wide variety of metal composite materials such as carbon and aluminum, carbon and magnesium, carbon and tungsten, carbon and titanium oxide, and mineral materials such as ceramics and tourmaline.
- first structure and the second structure in which the small chambers having the front opening constituting the mixing and pulverization / micronization device of the present invention are provided are molded products of resin or synthetic resin, a right-angled isosceles triangle A small chamber with a front opening having a shape characteristic of the present invention determined on the basis of the above can be manufactured with high accuracy.
- the mixing and the pulverizing process should be performed.
- the fluid can be re-molecularized by magnetic force, the mixing power can be further increased, and the atomization can be promoted.
- a structure for forming a fluid material flow path and a structure unit are attached to and detached from the cylindrical body constituting the mixing / crushing fine particle forming apparatus of the present invention by dividing the cylindrical body into two parts.
- the structure and the structure unit are placed in concave portions formed in the inner peripheral wall of the body. It can be done by fitting or fixing or removing. Therefore, assembly, disassembly and maintenance are extremely easy.
- the structure and the structure unit that form the fluid flow path can be easily attached and detached, so that the fluid flow path is formed by using a structure and a structure unit each made of a different material. It is possible to perform an optimal mixing process and a micronization process on a substance to be mixed and micronized.
- the small chamber of the front opening provided in the structure for forming the fluid flow path may be used depending on the characteristics of the substance to be mixed and atomized, the proportion of the substance contained in the fluid stream, etc., the small chamber of the front opening provided in the structure for forming the fluid flow path may be used. By changing the size, number, shape or material. Optimum mixing and micronization treatments can be performed on substances to be mixed and micronized.
- pressure is applied together with the pure oxygen gas into the fluid flow passage of the apparatus of the present invention, so that dispersion and collision that occur when flowing through each small chamber are performed. Due to the repetitive action of the vortex, the bonded molecules in the substance to be mixed and atomized can be decomposed and made harmless.
- the cylindrical body, the structure for forming the fluid flow path, and the like in the mixing and pulverization fine particle forming apparatus of the present invention may be formed of a heat conductive material, for example, copper, aluminum, carbon, or the like. As a result, it can be used as a heat exchanger, and it has the effect of simultaneously mixing and atomizing and heat exchange.
- a fluid in which the substance to be atomized is mixed is pressurized and flows into the fluid flow path of the mixing / crushing / micronizing apparatus of the present invention
- the fluid is formed by the small chambers of the front openings facing each other. In this process, it repeatedly flows into and out of one chamber to two chambers, and from two chambers to one chamber. , Receive strong compression repeatedly.
- the substance to be micronized can be made ultra-fine and molecular.
- dioxin which is a hardly decomposable substance such as industrial waste, for example, an environmental pollutant, etc. Can be decomposed and detoxified.
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- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Medicinal Chemistry (AREA)
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Description
Claims
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/476,892 US20040135017A1 (en) | 2001-05-07 | 2002-01-15 | Mixing, crushing, and pulverizing device, and method of pulverizing substances using the device |
JP2002565156A JP3451285B2 (ja) | 2001-05-07 | 2002-01-15 | 混合・粉砕微粒子化装置及びこれを用いた物質の微粒子化方法 |
US11/415,282 US20060192038A1 (en) | 2001-05-07 | 2006-05-02 | Apparatus for mixing and/or crushing substance into fine particles and method of crushing substances into fine particles using such apparatus |
US11/892,467 US20080067271A1 (en) | 2001-05-07 | 2007-08-23 | Apparatus for mixing and/or crushing substances into fine particles and method of crushing substances into fine particles using such apparatus |
US12/797,039 US20100243769A1 (en) | 2001-05-07 | 2010-06-09 | Apparatus for mixing and/or crushing substances into fine particles and method of crushing substances into fine particles using such apparatus |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2001136229 | 2001-05-07 | ||
JP2001-136229 | 2001-05-07 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US11/415,282 Continuation US20060192038A1 (en) | 2001-05-07 | 2006-05-02 | Apparatus for mixing and/or crushing substance into fine particles and method of crushing substances into fine particles using such apparatus |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2002089989A1 true WO2002089989A1 (fr) | 2002-11-14 |
Family
ID=18983551
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/JP2002/000175 WO2002089989A1 (fr) | 2001-05-07 | 2002-01-15 | Dispositif de melangeage, concassage et pulverisation et procede de pulverisation de substances au moyen dudit procede |
Country Status (3)
Country | Link |
---|---|
US (4) | US20040135017A1 (ja) |
JP (1) | JP3451285B2 (ja) |
WO (1) | WO2002089989A1 (ja) |
Cited By (10)
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WO2004045752A1 (ja) * | 2002-11-08 | 2004-06-03 | Sukeyoshi Sekine | 混合・粉砕微粒子化装置 |
JP2005186048A (ja) * | 2003-12-24 | 2005-07-14 | Yamato Yusetsu Kk | 気体、固形物及び液状物の混砕微粒化装置 |
WO2009154188A1 (ja) * | 2008-06-16 | 2009-12-23 | アイセル株式会社 | 混合要素、混合装置、攪拌翼、混合機、混合システム及び反応装置 |
JP2010023026A (ja) * | 2008-06-16 | 2010-02-04 | Isel Co Ltd | 混合要素、混合装置、混合方法、攪拌翼、攪拌装置及び攪拌方法 |
JP2010194522A (ja) * | 2009-02-27 | 2010-09-09 | Isel Co Ltd | 反応装置、反応方法及び触媒ユニット |
JP2011121020A (ja) * | 2009-12-14 | 2011-06-23 | Isel Co Ltd | 混合要素、混合装置、混合方法、攪拌翼、攪拌装置及び攪拌方法 |
JP2014104374A (ja) * | 2012-11-22 | 2014-06-09 | Mg Grow Up:Kk | 静止型流体混合装置 |
JPWO2013137136A1 (ja) * | 2012-03-13 | 2015-08-03 | アイセル株式会社 | 混合要素、これを用いた装置、流体混合方法及び流体物 |
US9656223B2 (en) | 2008-06-16 | 2017-05-23 | Isel Co., Ltd. | Mixing unit and device, fluid mixing method and fluid |
JP6326172B1 (ja) * | 2017-07-21 | 2018-05-16 | 株式会社エコグローバルユニオン | 水素含有率の高い水を製造するシステム |
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JP4142675B2 (ja) * | 2005-08-10 | 2008-09-03 | 株式会社ABsize | フラーレン分散液の製造方法 |
WO2009068535A1 (de) * | 2007-11-30 | 2009-06-04 | Basf Se | Verfahren und vorrichtung zur konditionierung einer magnetisierbare partikel enthaltenden suspension |
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US8865055B2 (en) | 2008-07-16 | 2014-10-21 | Materials And Electrochemical Research (Mer) Corporation | Production of sintered three-dimensional ceramic bodies |
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JP5933298B2 (ja) * | 2011-03-23 | 2016-06-08 | 株式会社粉研パウテックス | 連続混練装置 |
PL2775928T3 (pl) | 2011-11-08 | 2019-09-30 | Auxocell Laboratories Inc. | Systemy i metody przetwarzania komórek |
US9993748B2 (en) | 2014-08-11 | 2018-06-12 | Auxocell Laboratories, Inc. | Centrifuge clip and method |
USD748462S1 (en) | 2014-08-11 | 2016-02-02 | Auxocell Laboratories, Inc. | Centrifuge clip |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3856270A (en) * | 1973-10-09 | 1974-12-24 | Fmc Corp | Static fluid mixing apparatus |
DE19927556A1 (de) * | 1999-06-16 | 2000-12-28 | Inst Mikrotechnik Mainz Gmbh | Statischer Mikromischer |
JP2001029776A (ja) * | 1999-07-19 | 2001-02-06 | S G Eng Kk | 物質の微粒化装置 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3526391A (en) * | 1967-01-03 | 1970-09-01 | Wyandotte Chemicals Corp | Homogenizer |
US3782694A (en) * | 1972-09-18 | 1974-01-01 | Western Controls Inc | Apparatus and method for mixing materials |
US5411216A (en) * | 1992-12-11 | 1995-05-02 | O'keefe; Dennis | Tire shredder and process for shredding tires |
US5244159A (en) * | 1993-01-29 | 1993-09-14 | Grindmaster Corporation | Grinding burrs for coffee bean grinders |
US5971307A (en) * | 1998-02-13 | 1999-10-26 | Davenport; Ricky W. | Rotary grinder |
JPH0856629A (ja) * | 1994-08-24 | 1996-03-05 | Kankyo Kagaku Kogyo Kk | 液状食品の殺菌装置および製造装置 |
US5547281A (en) * | 1994-10-11 | 1996-08-20 | Phillips Petroleum Company | Apparatus and process for preparing fluids |
DE19712653C2 (de) * | 1997-03-26 | 2002-10-24 | Voith Paper Fiber Systems Gmbh | Verfahren und Vorrichtung zur Dispergierung eines Altpapierfaserstoffes |
US5944271A (en) * | 1997-08-28 | 1999-08-31 | J&L Fiber Services, Inc. | High consistency damless refiner plate for wood fibers |
US6211253B1 (en) * | 1998-05-20 | 2001-04-03 | Ernesto Marelli | Process for producing emulsions, particularly emulsions of liquid fuels and water, and apparatus used in the process |
US5967658A (en) * | 1998-07-28 | 1999-10-19 | Kam Controls Incorporated | Static mixing apparatus and method |
EP1134020B1 (en) * | 1998-10-26 | 2008-08-20 | Matrix Global Technology Ltd. | Mixing element body for stationary type mixer |
JP4009035B2 (ja) * | 1999-03-05 | 2007-11-14 | 株式会社フジキン | 静止型混合攪拌装置 |
-
2002
- 2002-01-15 US US10/476,892 patent/US20040135017A1/en not_active Abandoned
- 2002-01-15 JP JP2002565156A patent/JP3451285B2/ja not_active Expired - Fee Related
- 2002-01-15 WO PCT/JP2002/000175 patent/WO2002089989A1/ja active Application Filing
-
2006
- 2006-05-02 US US11/415,282 patent/US20060192038A1/en not_active Abandoned
-
2007
- 2007-08-23 US US11/892,467 patent/US20080067271A1/en not_active Abandoned
-
2010
- 2010-06-09 US US12/797,039 patent/US20100243769A1/en not_active Abandoned
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3856270A (en) * | 1973-10-09 | 1974-12-24 | Fmc Corp | Static fluid mixing apparatus |
DE19927556A1 (de) * | 1999-06-16 | 2000-12-28 | Inst Mikrotechnik Mainz Gmbh | Statischer Mikromischer |
JP2001029776A (ja) * | 1999-07-19 | 2001-02-06 | S G Eng Kk | 物質の微粒化装置 |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004045752A1 (ja) * | 2002-11-08 | 2004-06-03 | Sukeyoshi Sekine | 混合・粉砕微粒子化装置 |
JP2005186048A (ja) * | 2003-12-24 | 2005-07-14 | Yamato Yusetsu Kk | 気体、固形物及び液状物の混砕微粒化装置 |
JP4512360B2 (ja) * | 2003-12-24 | 2010-07-28 | ヤマト油設株式会社 | 気体、固形物及び液状物の混砕微粒化装置 |
WO2009154188A1 (ja) * | 2008-06-16 | 2009-12-23 | アイセル株式会社 | 混合要素、混合装置、攪拌翼、混合機、混合システム及び反応装置 |
JP2010023026A (ja) * | 2008-06-16 | 2010-02-04 | Isel Co Ltd | 混合要素、混合装置、混合方法、攪拌翼、攪拌装置及び攪拌方法 |
US9656223B2 (en) | 2008-06-16 | 2017-05-23 | Isel Co., Ltd. | Mixing unit and device, fluid mixing method and fluid |
JP2010194522A (ja) * | 2009-02-27 | 2010-09-09 | Isel Co Ltd | 反応装置、反応方法及び触媒ユニット |
JP2011121020A (ja) * | 2009-12-14 | 2011-06-23 | Isel Co Ltd | 混合要素、混合装置、混合方法、攪拌翼、攪拌装置及び攪拌方法 |
JPWO2013137136A1 (ja) * | 2012-03-13 | 2015-08-03 | アイセル株式会社 | 混合要素、これを用いた装置、流体混合方法及び流体物 |
JP2014104374A (ja) * | 2012-11-22 | 2014-06-09 | Mg Grow Up:Kk | 静止型流体混合装置 |
JP6326172B1 (ja) * | 2017-07-21 | 2018-05-16 | 株式会社エコグローバルユニオン | 水素含有率の高い水を製造するシステム |
JP2019018187A (ja) * | 2017-07-21 | 2019-02-07 | 株式会社イ・ジ・ユ | 水素含有率の高い水を製造するシステム |
Also Published As
Publication number | Publication date |
---|---|
US20040135017A1 (en) | 2004-07-15 |
JP3451285B2 (ja) | 2003-09-29 |
US20100243769A1 (en) | 2010-09-30 |
JPWO2002089989A1 (ja) | 2004-08-19 |
US20080067271A1 (en) | 2008-03-20 |
US20060192038A1 (en) | 2006-08-31 |
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