WO2002061015A1 - Procede et appareil de fabrication de combustible liquide a partir de dechets plastiques et de dechets de raffinerie - Google Patents

Procede et appareil de fabrication de combustible liquide a partir de dechets plastiques et de dechets de raffinerie Download PDF

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Publication number
WO2002061015A1
WO2002061015A1 PCT/IN2001/000061 IN0100061W WO02061015A1 WO 2002061015 A1 WO2002061015 A1 WO 2002061015A1 IN 0100061 W IN0100061 W IN 0100061W WO 02061015 A1 WO02061015 A1 WO 02061015A1
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WO
WIPO (PCT)
Prior art keywords
condenser
waste
vessel
temperature
receiving
Prior art date
Application number
PCT/IN2001/000061
Other languages
English (en)
Inventor
Umesh Arun Zadgaonkar
Alka Umesh Zadgaonkar
Original Assignee
Umesh Arun Zadgaonkar
Alka Umesh Zadgaonkar
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Umesh Arun Zadgaonkar, Alka Umesh Zadgaonkar filed Critical Umesh Arun Zadgaonkar
Publication of WO2002061015A1 publication Critical patent/WO2002061015A1/fr

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/10Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal from rubber or rubber waste

Definitions

  • the invention relates to an improved apparatus for manufacturing of Petrol / Kerosene/ diesel/ furnace oil/ lubricating oil fractions, Petroleum gases and coke from any type of waste plastic and refinery waste, refinery residue, coal tar or any type of secondary residue or any type of waste oil.
  • the invention relates to an improved apparatus wherein higher yield distillate consist of Petrol/ Kerosene / diesel / furnace oil / lubricating oil fractions obtained with monitored & controlled temperature and fully controlled reaction process.
  • the- -inventor has — f ⁇ und-a —improved -apparatus- for— manufacturing of Petrol / Kerosene/ diesel/ furnace oil/ lubricating oil fractions, Petroleum gases and coke from any type of waste plastic and refinery waste, refinery residue, coal tar or any type of secondary residue or any type of waste oil to obtain lighter distillate in a full proof manner wherein refinery waste is charged with waste plastic and additives to obtain higher yield of distillate up to 95% with high purity / quality.
  • the refinery waste hereto mentioned means apart from refinery waste, refinery residue coal tar or any other type of bitumen or any other type of secondary residue or any other type of waste oil and/or a mixture thereof.
  • Waste plastic means polypropylene, low density , polyethylene , high density polyethylene or any other plastic and/or mixture thereof.
  • distillate means of combination of petrol/ kerosene / diesel / furnace oil / lubricating oil fraction.
  • the refinery waste, waste plastic and distillates referred wherever desired hereunder are consists of above definitions.
  • the principle object of this invention is therefore to provide an improved apparatus for the utilisation and conversion of waste plastic into usable product such as petrol / kerosene / diesel / furnace oil / lubricating oil fractions, petroleum gases & coke. All are usable products that too without any waste or hazardous by-product.
  • Still further object of this invention is to provide an improved apparatus for manufacturing of Petrol / Kerosene/ diesel/ furnace oil / lubricant oil fractions, Petroleum gases and coke from any type of waste plastic and refinery waste, refinery residue, coal tar or any type of secondary residue or any type of waste oil to obtain higher yield of distillates at controlled temperature by means of electric sensor.
  • an improved apparatus for manufacturing of Petrol / Kerosene/ diesel/ furnace oil/ lubricating oil fractions, Petroleum gases and coke from any type of waste plastic and refinery waste, refinery residue, coal tar or any type of secondary residue or any type of waste oil to provide an improved apparatus consisting of coking chamber / coking section, codenser / condensing section , receiving unit , receiving section.
  • an electronic / electrical device to control & monitor the temperature within the coking chamber and other sections to achieve higher yields of distillate with high purity thereby cost effective, safe and userfriendly.
  • Still further object of this invention is to provide an improved apparatus for manufacturing of Petrol / Kerosene/ diesel/ furnace oil/ lubricating oil fractions, Petroleum gases and coke from any type of waste plastic and refinery waste, refinery residue, coal tar or any type of secondary residue or any type of waste oil wherein a value added useful product is obtained from the waste material
  • an improved apparatus consisting of a cylindrical or rectangular cooking vessel (1) heated by electrical heating coils or any other form of energy said vessel is made from stainless steel or mild steel and surrounded by heat reflector & insulator to avoid heat loss & to achieve maximum heating inside locked at the top Lid (2) with temperature sensor which extended upto the centre of the vessel; the other end protruding outside is connected to a controlled unit by means of wiring; said lid is provided with high temperature gasket for locking by means of lock & bolt; said coking vessel is provided at its side an outlet vent to connect condensing section / condenser (10) the other end of the condenser is connected to the receiving section; said condenser is provided with outer jacket for circulating cold water or thermic fluid from the bottom (11) as & when required for the conversion of gaseous form of product in to liquid state; the said condenser is connected to the receiving assembly / unit (12) by means of suitable conduit (13) in tandem with other receiving units (14) or gasometer (15) and a outlet vent towards the
  • Figure 1 is a prospective view of the improved apparatus
  • FIG. 1 provided an improved apparatus consisting of a cylindrical rectangular a coking vessel (1) heated by electrical heating coils or any other form of energy said vessel is made from stainless steel or mild steel and (surrounded by heat reflector & insulator to avoid heat loss & to achieve maximum heating inside) locked at the top (2) with temperature sensor which extended upto the center of the vessel; the other end protruding outside is connected to a controlled unit by means of wiring; said lid is provided with high temperature gasket for locking by means of lock & bolt; said coking vessel is provided at its side an outlet vent to connect condensing section / condenser (10) the other end of the condenser is connected to the receiving section; said condenser is provided with outer jacket for circulating cold water or thermic fluid from the bottom (11) as & when required for the conversion of gaseous form of product into liquid state; the said condenser is connected to the receiving assembly / unit (12) by means of suitable conduit (13) in tandem with other receiving units (14) or gasometer (15) and a outlet vent towards
  • RAW MATERIAL Any type of waste Plastic ( like Polypropylene, Low Density Polyethylene, High Density Polyethylene or any other plastic or combination of them )
  • Acidic Chemical like Alumina or any form of Aluminium or Neutral additive like Benzoquinon having concentration in the range of 0.001%) to 5.0%) depending upon the type of Refinery waste & type of waste plastic.
  • EQUIPMENT Equipment is assembled in mainly three units.
  • Thickness of the material is in proportion of size of the Colter and to withstand the heavy temperature.
  • - Shape Cylindrical or Rectangular. If Cylindrical, diameter 9 cm (+ 15%) or in proper / viable proportion of the mentioned diameter for the purpose of industrial or commercial utilisation. Having height 30 cm ( ⁇ 20%) or in proper / viable proportion of the mentioned height for the purpose of industrial or commercial utilisation. If Rectangular, then having sides ad- measuring 8cm ( ⁇ 15%) each or in proportion of 8 cm and height of 30 cm ( ⁇ 15 )) or in proportion of 30 cm for the purpose of industrial or commercial utilisation.
  • An Air-tight lid is provided.
  • One Vent of 2 cm ( ⁇ 15 >) diameter or in proportion of the mentioned size coking chamber still at the upper side of coking chamber is provided which can be exactly fitted to a condensing system / device via Mild steel or Stainless Steel Tube.
  • An arrangement/ provision to raise the temperature of the coking chamber is made.
  • the heating of the coking chamber can be done so as to raise the Temperature up to 600°C. Heating is done Electrically or by any other suitable energy source. Complete coking chamber is given proper insulation to minimise heat loss.
  • a Condenser is made up of Stainless Steel or Mild Steel or Glass or any other material which does not react with distillate.
  • An arrangement for circulation of water or any Thermic Fluid through the outer tube is designed in such manner in order to condense the product vapours at initial stage and to raise the temperature at latter stage to avoid chocking due to waxy material in the inner tube of condenser.
  • Outlet of the condenser device is connected to the receiving assembly made up of Stainless Steel or Mild Steel or Glass or any other material which does not react with the distillate to collect the total distillate formed.
  • An arrangement is made to measure the volume & rate of flow of distillate, continuously or intermittently at any point of time.
  • This receiving assembly can be cooled down by suitable cooling device up to [-]20 °C or it can be heated up to 100° C, as and when required.
  • This receiving container is provided with outlet vent for exit of Coker Gases which can be collected and utilised. Received Liquid or gas fuels can be partially utilised to raise the temperature of cocking chamber/section. Thus at such stage the full process and apparatus runs without any outside energy.
  • the principle object of this invention is therefore to provide an improved process for the utilization and conversion of waste plastic into usable product such as petrol / kerosene / diesel / furnace oil / lubricating oil fractions / petroleum gases & coke. All are usable products that too without any waste or hazardous by- products.
  • Still further object of this invention is to provide an improved process for manufacturing of Petrol / Kerosene/ diesel/ furnace oil/ lubricating oil fractions, Petroleum gases and coke from any type of waste plastic and refinery waste, refinery residue, coal tar or any type of secondary residue or any type of waste oil to obtain higher yield of distillates at controlled temperature.
  • Still further object of this invention is to provide an improved process for manufacturing of Petrol / Kerosene/ diesel/ furnace oil/ lubricating oil fractions, Petroleum gases and coke from any type of waste plastic and refinery waste, refinery residue, coal tar or any type of secondary residue or any type of waste oil wherein a value added useful product is obtained from the waste material .
  • the total distillate collected is transferred to a flask. First this total distillate was analyzed for important properties like specific gravity, viscosity (Kinematic or Redwood), aniline point, refractive index etc. Next the ASTM distillation of total distillate was carried out and different fractions namely fraction I - IBP-140°C (Light Naphtha cut), Fraction II- 140°C- 200°C (Heavy Naphtha and gasoline component), fraction III - 200°C-250°C (kerosene fraction), fraction IV - above 250°C (Diesel Fractions furnace oil / Lubricating Oil were collected).
  • fraction I - IBP-140°C Light Naphtha cut
  • Fraction II- 140°C- 200°C Heavy Naphtha and gasoline component
  • fraction III - 200°C-250°C kerosene fraction
  • fraction IV - above 250°C Diesel Fractions furnace oil / Lubricating Oil were collected).

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

Cette invention concerne un appareil amélioré comportant un récipient (1) de cokéfaction cylindrique ou rectangulaire, chauffé au moyen de serpentins de chauffage électriques ou d'une autre forme d'énergie quelconque. Ce récipient est fabriqué à partir d'acier inoxydable ou d'acier doux et est entouré d'un réflecteur thermique et d'un calorifuge servant à éviter toute perte thermique et à obtenir un chauffage intérieur maximum. La partie supérieure (2) dudit récipient est fermée par un capteur thermique dont une extrémité s'étend jusqu'au centre du récipient ; l'autre extrémité, située à l'extérieur du récipient, est connectée à une unité de commande au moyen d'un câblage ; le couvercle est pourvu d'un joint à haute température permettant le verrouillage au moyen d'un dispositif de verrouillage et de pêne ; ce récipient de cokéfaction comporte, sur le côté, un orifice de sortie permettant de se connecter au condenseur (10). Ledit condenseur est relié, à l'extrémité opposée, à une partie réceptrice. Ce condenseur est pourvu d'une enveloppe extérieure dans laquelle circule de l'eau froide ou un fluide thermique à partir de la base (11) lorsque cela s'avère nécessaire pour transformer un produit d'une forme gazeuse en un état liquide. Ce condenseur est relié à l'unité réceptrice (12) au moyen d'un conduit (13) approprié qui achemine le liquide tout d'abord dans l'unité réceptrice, puis dans une seconde unité réceptrice (14), puis dans un gazomètre (15) comportant un orifice de sortie permettant au liquide de s'écouler vers l'unité de récupération du gaz et l'unité d'étanchéité (16), ladite unité réceptrice étant maintenue à une température comprise entre 40 °C et la température ambiante, ou à une température plus élevée de manière à recueillir le produit distillé par lots ou en mode continu.
PCT/IN2001/000061 2001-01-29 2001-03-29 Procede et appareil de fabrication de combustible liquide a partir de dechets plastiques et de dechets de raffinerie WO2002061015A1 (fr)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
IN103MU2001 2001-01-29
IN102MU2001 2001-01-29
IN102/MUM/2001 2001-01-29
IN103/MUM/2001 2001-01-29

Publications (1)

Publication Number Publication Date
WO2002061015A1 true WO2002061015A1 (fr) 2002-08-08

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Application Number Title Priority Date Filing Date
PCT/IN2001/000061 WO2002061015A1 (fr) 2001-01-29 2001-03-29 Procede et appareil de fabrication de combustible liquide a partir de dechets plastiques et de dechets de raffinerie

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WO (1) WO2002061015A1 (fr)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5584969A (en) * 1993-07-29 1996-12-17 Hitachi Zosen Corporation Apparatus for thermally decomposing plastics and process for converting plastics into oil by thermal decomposition
CN1236804A (zh) * 1999-05-06 1999-12-01 杨健 废塑料、废橡胶制石油产品的方法和装置

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5584969A (en) * 1993-07-29 1996-12-17 Hitachi Zosen Corporation Apparatus for thermally decomposing plastics and process for converting plastics into oil by thermal decomposition
CN1236804A (zh) * 1999-05-06 1999-12-01 杨健 废塑料、废橡胶制石油产品的方法和装置

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Section Ch Week 200015, Derwent World Patents Index; Class A35, AN 2000-161729, XP002189916 *

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