WO2001089683A3 - Vorrichtung und verfahren zur durchführung von heterogen katalysierten gasphasenreaktionen mit wärmetönung - Google Patents

Vorrichtung und verfahren zur durchführung von heterogen katalysierten gasphasenreaktionen mit wärmetönung Download PDF

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Publication number
WO2001089683A3
WO2001089683A3 PCT/EP2001/006034 EP0106034W WO0189683A3 WO 2001089683 A3 WO2001089683 A3 WO 2001089683A3 EP 0106034 W EP0106034 W EP 0106034W WO 0189683 A3 WO0189683 A3 WO 0189683A3
Authority
WO
WIPO (PCT)
Prior art keywords
reactor chamber
carrying
gas phase
reaction gas
heterogeneously catalysed
Prior art date
Application number
PCT/EP2001/006034
Other languages
English (en)
French (fr)
Other versions
WO2001089683A2 (de
WO2001089683A9 (de
Inventor
Franz Josef Broecker
Mathias Haake
Manfred Stroezel
Otto Woerz
Ekkehard Schwab
Original Assignee
Basf Ag
Franz Josef Broecker
Mathias Haake
Manfred Stroezel
Otto Woerz
Ekkehard Schwab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag, Franz Josef Broecker, Mathias Haake, Manfred Stroezel, Otto Woerz, Ekkehard Schwab filed Critical Basf Ag
Priority to EP01957805A priority Critical patent/EP1289650A2/de
Priority to US10/296,255 priority patent/US20030159799A1/en
Priority to JP2001585916A priority patent/JP2003534299A/ja
Publication of WO2001089683A2 publication Critical patent/WO2001089683A2/de
Publication of WO2001089683A3 publication Critical patent/WO2001089683A3/de
Publication of WO2001089683A9 publication Critical patent/WO2001089683A9/de

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D9/00—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D9/04—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being formed by spirally-wound plates or laminae
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B01J12/007—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
    • C07C45/38—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a primary hydroxyl group
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00085—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00096—Plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1944—Details relating to the geometry of the reactor round circular or disk-shaped spiral
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324—Composition or microstructure of the elements
    • B01J2219/32466—Composition or microstructure of the elements comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324—Composition or microstructure of the elements
    • B01J2219/32466—Composition or microstructure of the elements comprising catalytically active material
    • B01J2219/32475—Composition or microstructure of the elements comprising catalytically active material involving heat exchange

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • General Engineering & Computer Science (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

Die Erfindung betrifft eine Vorrichtung zur weitgehend isothermen Durchführung einer heterogen katalysierten Reaktion in der Gasphase mit hoher Wärmetönung, aufweisend mindestens einen Reaktorraum (101) mit Einlass (131, 141) und Auslass (143), wobei der Reaktorraum durch wärmeabführende Wände begrenzt ist, die einen im wesentlichen konstanten Abstand längs der Hauptströmungsachse eines Reaktionsgases von ≤ 30 mm aufweisen, der Reaktorraum mit Katalysator beschichteten Bändern (120, 132) bestückt ist, die Bänder in allen Raumrichtungen flexibel und für das Reaktionsgas durchlässig sind, ein Oberfläche-zu-Volumen-Verhältnis von 50 bis 5000 m2/m3 sowie eine gute Wärmeleitfähigkeit aufweisen, das Reaktionsgas den Reaktorraum mit einer Geschwindigkeit von ≥200 m?3 pro m2¿ angeströmte Fläche und pro Stunde durchströmt, und+auf der dem Reaktorraum abgewandten Seite der Reaktorwand ein Wärmeaustauschmittel strömt.
PCT/EP2001/006034 2000-05-24 2001-05-25 Vorrichtung und verfahren zur durchführung von heterogen katalysierten gasphasenreaktionen mit wärmetönung WO2001089683A2 (de)

Priority Applications (3)

Application Number Priority Date Filing Date Title
EP01957805A EP1289650A2 (de) 2000-05-24 2001-05-25 Vorrichtung und verfahren zur durchführung von heterogen katalysierten gasphasenreaktionen mit wärmetönung
US10/296,255 US20030159799A1 (en) 2000-05-24 2001-05-25 Device and method for carrying out heterogeneously catalysed gas phase reactions with heat tonality
JP2001585916A JP2003534299A (ja) 2000-05-24 2001-05-25 発熱を伴う不均一系触媒作用の気相反応を行うための方法及びそのための装置

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10025382.2 2000-05-24
DE10025382A DE10025382A1 (de) 2000-05-24 2000-05-24 Vorrichtung und Verfahren zur Durchführung von heterogen katalysierten Gasphasenreaktionen mit Wärmetönung

Publications (3)

Publication Number Publication Date
WO2001089683A2 WO2001089683A2 (de) 2001-11-29
WO2001089683A3 true WO2001089683A3 (de) 2002-05-10
WO2001089683A9 WO2001089683A9 (de) 2004-11-11

Family

ID=7643165

Family Applications (1)

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PCT/EP2001/006034 WO2001089683A2 (de) 2000-05-24 2001-05-25 Vorrichtung und verfahren zur durchführung von heterogen katalysierten gasphasenreaktionen mit wärmetönung

Country Status (7)

Country Link
EP (1) EP1289650A2 (de)
JP (1) JP2003534299A (de)
KR (1) KR20030022131A (de)
CN (1) CN1188212C (de)
DE (1) DE10025382A1 (de)
TW (1) TW575462B (de)
WO (1) WO2001089683A2 (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10139046C2 (de) * 2001-08-08 2003-10-02 Ballard Power Systems Vorrichtung zur selektiven Oxidation von Bestandteilen eines Stoffstroms
CN112717684A (zh) * 2020-12-17 2021-04-30 安徽燃博智能科技有限公司 一种卷板式自热催化氧化器
CN114160083A (zh) * 2021-11-12 2022-03-11 大连理工大学 一种回旋式聚合反应器

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1427252A (en) * 1972-04-29 1976-03-10 Getters Spa Catalytic cartridges
EP0560157A1 (de) * 1992-03-12 1993-09-15 Bayer Ag Festbettreaktoren mit kurzem Katalysatorbett in Strömungsrichtung
JPH0631165A (ja) * 1992-07-15 1994-02-08 Sekiyu Sangyo Kasseika Center 水蒸気改質用薄膜状触媒
DK169060B1 (da) * 1990-10-29 1994-08-08 Topsoe Haldor As Reaktor til dampreforming af carbonhydrider under varmeveksling
EP0965384A1 (de) * 1998-06-19 1999-12-22 Basf Aktiengesellschaft Tränkverfahren zur Aufbringung von Aktivmasse auf strukturierte Träger oder Monolithe
EP1074294A2 (de) * 1999-08-02 2001-02-07 Basf Aktiengesellschaft Vorrichtung und Verfahren zur isothermen Durchführung von heterogen katalysierten Dreiphasenreaktionen

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3402713A1 (de) * 1984-01-26 1985-08-08 Linde Ag, 6200 Wiesbaden Verfahren und reaktor zur durchfuehrung einer endothermen reaktion
DE19725378A1 (de) * 1997-06-16 1998-12-17 Gerhard Friedrich Kompakter Festbettreaktor für katalytische Reaktionen mit integriertem Wärmeaustausch

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1427252A (en) * 1972-04-29 1976-03-10 Getters Spa Catalytic cartridges
DK169060B1 (da) * 1990-10-29 1994-08-08 Topsoe Haldor As Reaktor til dampreforming af carbonhydrider under varmeveksling
EP0560157A1 (de) * 1992-03-12 1993-09-15 Bayer Ag Festbettreaktoren mit kurzem Katalysatorbett in Strömungsrichtung
JPH0631165A (ja) * 1992-07-15 1994-02-08 Sekiyu Sangyo Kasseika Center 水蒸気改質用薄膜状触媒
EP0965384A1 (de) * 1998-06-19 1999-12-22 Basf Aktiengesellschaft Tränkverfahren zur Aufbringung von Aktivmasse auf strukturierte Träger oder Monolithe
EP1074294A2 (de) * 1999-08-02 2001-02-07 Basf Aktiengesellschaft Vorrichtung und Verfahren zur isothermen Durchführung von heterogen katalysierten Dreiphasenreaktionen

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Section Ch Week 199411, Derwent World Patents Index; Class E36, AN 1994-079440 *
DATABASE WPI Section Ch Week 199430, Derwent World Patents Index; Class E19, AN 1992-251305, XP002185820 *
PATENT ABSTRACTS OF JAPAN vol. 018, no. 248 (C - 1198) 12 May 1994 (1994-05-12) *

Also Published As

Publication number Publication date
WO2001089683A2 (de) 2001-11-29
DE10025382A1 (de) 2001-12-06
TW575462B (en) 2004-02-11
CN1437506A (zh) 2003-08-20
JP2003534299A (ja) 2003-11-18
CN1188212C (zh) 2005-02-09
WO2001089683A9 (de) 2004-11-11
KR20030022131A (ko) 2003-03-15
EP1289650A2 (de) 2003-03-12

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