WO1998037371A1 - Method and equipment for drying an object including water - Google Patents

Method and equipment for drying an object including water Download PDF

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Publication number
WO1998037371A1
WO1998037371A1 PCT/FI1998/000151 FI9800151W WO9837371A1 WO 1998037371 A1 WO1998037371 A1 WO 1998037371A1 FI 9800151 W FI9800151 W FI 9800151W WO 9837371 A1 WO9837371 A1 WO 9837371A1
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WO
WIPO (PCT)
Prior art keywords
gas mixture
space
drying
water
cooling
Prior art date
Application number
PCT/FI1998/000151
Other languages
English (en)
French (fr)
Inventor
Keijo SAARENPÄÄ
Original Assignee
Lvi-Insinööritoimisto Keijo Saarenpää
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Filing date
Publication date
Application filed by Lvi-Insinööritoimisto Keijo Saarenpää filed Critical Lvi-Insinööritoimisto Keijo Saarenpää
Publication of WO1998037371A1 publication Critical patent/WO1998037371A1/en

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/14Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects using gases or vapours other than air or steam, e.g. inert gases
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/06Controlling, e.g. regulating, parameters of gas supply
    • F26B21/08Humidity
    • F26B21/086Humidity by condensing the moisture in the drying medium, which may be recycled, e.g. using a heat pump cycle
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/02Drying solid materials or objects by processes not involving the application of heat by using ultrasonic vibrations
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B2210/00Drying processes and machines for solid objects characterised by the specific requirements of the drying good
    • F26B2210/16Wood, e.g. lumber, timber

Definitions

  • the invention is related to a method and an equipment for drying an object including water, e.g. timber or reindeer meat. Especially, the invention is related to so-called vacuum drying wherein the object is closed in a chamber or equivalent, in which partial vacuum is maintained during the drying, to bring down the boiling point of water and to make the vaporization of water easier.
  • a preferred application of the invention is timber drying, with which a lot of problems are involved.
  • the biggest problem, perhaps, is to make the moisture of the inner part of the timber to move rapidly enough to the outside layer of the timber and therethrough to the ambient gas space, without causing cracks or other drying damages in the timber.
  • Newly cut timber includes a lot of intercellular water, and for drying the timber to a water content of about 6 %, required for furniture wood, also the most of the water bound by the cells must be removed. Intense shrinkage of timber begins from the so-called fiber saturation point, which may be, e. g., about 28 %, and on which the removal of the intercellular water is ended and the extraction of water bound by the cells starts. If the outside layer of the timber is then dried too rapidly in relation to the inner part of the timber, the surface layer is hardened and tensile stresses and as a result thereof cracks are caused therein.
  • the water is advantageously removed from the timber by boiling, because then the drying occurs intensively in both the surface layer and the inner part of the timber, by which the moisture differences and the defects caused thereby are reduced.
  • a temperature of at least 100 °C is needed under normal pressure, and for many kinds of wood such a temperature causes colour defects, e. g. blackening, or deterioration of strength.
  • An advantage of the vacuum drying is that boiling is caused and maintained at a remarkably low temperature.
  • the existence of oxygen in the drying ambient causes at higher temperatures, besides the colour changes, also increased melting of resin. At lower temperatures, which are concerned with vacuum drying, the existence of oxygen contributes to growth of mould and blue stain fungi on the surface of the timber.
  • FI 930081 presents a drying method intended to be used under normal pressure, wherein the timber is dried by means of an air flow directed thereto.
  • the aim is to keep the inside temperature of the timber above the boiling point, and heating and cooling phases are repeated cyclically between an upper temperature limit (100 to 120 °C) and a lower temperature limit, which may not be significantly lower than the boiling point, set for the inside temperature.
  • the intention is that during the cooling moisture is moved from the inner part of the timber towards the surface, from which it is vaporized during the heating.
  • Finnish Nurvac vacuum drier WOODWORKING PUUNTYOSTO No.
  • the timber is placed in a leak-proof chamber, and the temperature is first rised therein under normal pressure.
  • a vacuum pump is switched on, whereby the pressure in the chamber is gradually reduced to about 0, 1 bar.
  • water is still boiling at least at about 45 °C.
  • the vaporated moisture is removed from the chamber through a pipe to a heat exchanger, in which it is condensed and then led out therefrom. With this drier the problem is that the removal of the vaporized moisture through the pipe to outside of the chamber takes a lot of time, and so the whole drying process tends to progress slowly.
  • the drying process is controlled by opening the pressure control valve between the drying chamber and the condensing tank, always when the pressure in the drying chamber exceeds a certain limit. As the valve is opened, vaporated moisture is removed from the drying chamber to the condensing tank having a lower temperature and pressure.
  • the aim of the control is to manage the temperature and the pressure and so the relative humidity of the vapour based on these conditions, and to keep the temperature and the pressure as uniform as possible in the drying chamber.
  • the disadvantage is the bigger the bigger the reduction of the air pressure in the chamber is, because then the density of the mixture of the air and the vaporized moisture and at the same time the specific heat capacity is reduced.
  • some solutions are presented, in which the area of the heating surface and the circulating velocity of the mixture of air and vaporized moisture are increased, and a long enough cooling and settling phase is provided in the end of the drying process.
  • the drying process is made slower also by the handicaps related to the transfer of the vaporized moisture from the drying chamber to the cooling surfaces.
  • the vacuum pump is used also to transfer the mixture of the air and the vaporized moisture.
  • Vacuum pumps provide large pressure differences with a small volume flow, and because the specific volume of the water vapour increases as the temperature and the pressure decrease, some problems are caused.
  • the total pressure of a closed space decreases also with the reduction of temperature. As a result, the relative humidity is increased to 100 %, and drying of the timber is stopped.
  • Narrow channels and pipes and restricted areas of heating and cooling surfaces set a limit to the increase of the circulation velocity.
  • the vapour is kept saturated on the cooling surfaces, although the temperature and pressure thereof are reduced. The reduction only causes the transfer of heat energy from the drying chamber to the cooling surfaces and the reduction of the temperature and pressure also in the drying chamber, i. e. the total pressure becomes rapidly even.
  • the saturated water vapour and the water condensed therefrom act as "a plug" making the drying process slower in the plate heat exchanger, especially.
  • This leveling of the total pressure is prevented in some equipment by installing a shut-off device between the drying chamber and the cooling surfaces, whereby the drying process is made cyclic. This makes the drying process slower, and additional measurement and control techniques are required.
  • An object of the invention is to present a method and an equipment for drying an object including water, e.g. timber or reindeer meat, which remove water both rapidly and gently and with a small energy input, and in which many disadvantages considered above may be avoided.
  • Another object of the invention is to present a solution, by means of which certain qualities desired by the end user may be emphasized in the dried timber.
  • the method for drying an object including water, e. g. timber or reindeer meat in which method: the object is closed to a chamber or equivalent space, wherein a partial vacuum is caused in relation to normal air pressure, so that a gas mixture, which includes water vapour extracted from the object, is formed therein; the object is heated to vaporize water therefrom to the space surrounding it; and water vapour is removed from the space; is characterized in that the gas mixture is circulated effectively via the space surrounding the object, so that the gas mixture leaves from the space to the circulation and returns back to the space from the circulation, and that it includes cycles, in which: during a first phase the gas mixture is heated effectively within the circulation for heating the object to a desired temperature; and during the second phase the gas mixture leaving the space is within the circulation first cooled for condensing water therefrom and removing the water from the circulation and then heated to a desired temperature below the temperature of the object before the return back to the space surrounding the object.
  • the equipment for drying an object including water, e. g. timber or reindeer meat which equipment includes: a leak-proof chamber or equivalent space for the object to be dried and means for causing a partial vacuum in the space in relation to normal air pressure, for forming a low-pressure gas mixture, which includes water vapour extracted from the object, in the space; means for heating the object to vaporize water therefrom to the space; and means for removing water vapour from the space; is characterized in that it includes: means for circulating the gas mixture effectively via the space surrounding the object, so that the gas mixture leaves from the space to the circulation and returns back to the space from the circulation; means for cooling and / or heating the gas mixture effectively within the circulation; and means for controlling circulating means and cooling and heating means to: heat the gas mixture for heating the object to a desired temperature; cool the gas mixture to a desired temperature below the temperature of the object; or to dry the gas mixture by cooling the gas mixture leaving the space surrounding the object for condensing water therefrom and for removing the
  • the drying method according to the invention is based on powerful circulation of the low-pressure gas mixture, including water vapour extracted from the object to be dried, with effective, in relation to the object properly placed fans, and on cyclic variation of the temperature of the gas mixture within a suitable temperature range.
  • the cycles are repeated, in which the gas mixture is first heated effectively to bring the temperature of the object to be dried to a temperature above the boiling point of water, for example to 60 °C.
  • the gas mixture leaving the space surrounding the object is during the circulation first cooled further to condense and remove the water vapour therefrom and then heated again before returning it back to the space surrounding the object.
  • the gas mixture includes nitrogen instead of air to avoid the problems caused by oxygen.
  • Nitrogen is either normal nitrogen or, if reindeer meat or equivalent object is dried, special nitrogen for foodstuff handling.
  • nitrogen-water vapour mixture is circulated from the drying chamber to a channel structure essentially covering the wall, which channel structure is double, so that the inner channel serves as an insulation channel and the outer channel as a cooling channel. From the cooling channel the gas mixture is circulated back to the drying chamber through fan channels, wherein it may also be cooled or heated.
  • the gas mixture acts as a heat carrier, moisture discharger and heat insulator in the insulation channel, the insulation capability thereof being based on the continuous, rapid flow of the gas mixture. Insulation channels and the use of the nitrogen- water vapour mixture as a heat insulator render possible large temperature differences between the drying chamber and the cooling channel and condensing tank thus securing good performance of the drying process.
  • the extraction of water from saturated water vapour is based on centrifugal force, density of water, gravitation, and circulation velocity of the nitrogen- water vapour mixture.
  • Water droplets are drifting to the outer walls of the cooling channel, cool to a temperature close to 0 °C, and run down to the condensing tank, in which they are freezed.
  • the use of the centrifugal force intensifies the extraction of water from the saturated water vapour, which speeds up the drying process.
  • the drying process consisting of two-phase or three-phase cycles provides a lot of alternatives to plan the drying schedule in such a way that total costs (drying time, damages, energy consumption) may be reduced.
  • the cycles and the phases included therein may be varied according to the kind of wood, water content, and thickness of the timber.
  • the cooling surface and the heating surface serve both as heating surfaces during the heating phase, and as cooling surfaces during the freezing phase. During the cooling and drying phase they serve separately as a cooling surface and as a heating surface.
  • the constructional solutions of the invention wide circulation channels, large areas of the cooling and heating surfaces, simultaneous use of cooling and heating surfaces, and normal air pressure fans together with channels which make possible to melt, preheat and predry the timber, make the invention different from the prior art vacuum driers and render possible the reduction of the total drying costs.
  • Figure 1 is a flow chart describing generally the method according to the invention
  • Figure 2 is a schematic presentation, which describes in further detail phases of the method according to the invention
  • Figure 3 is a diagrammatic elevation view, partly cut away, of an embodiment of the equipment according the invention.
  • Figure 4 presents the same embodiment completely including a sectional view taken on line A-A of Fig. 3 together with a diagrammatic presentation of other parts of the equipment;
  • Figures 5 and 6 present a plan view and an elevational view, respectively, of another embodiment of the equipment according to the invention.
  • the low-pressure gas mixture including air or suitable gas instead of air and water vapour derived from the object, is circulated effectively via a drying chamber, into which the object to be dried is located.
  • a drying chamber into which the object to be dried is located.
  • cycles 101, 102, 103, 104 and 105 are repeated, which include at least two successive phases: a heating phase 101a, 104a, and a cooling and drying phase 101b, 104b.
  • a cycle may include also a freezing phase 104c.
  • the number of the cyclically repeated successive cycles may vary depending on the application.
  • the process may include first a certain number m of cycles 101, 102, 103 having two phases, and then, as the fiber saturation point is reached, a certain number n of cycles 104, 105 having also the freezing phase.
  • a certain number n of cycles 104, 105 having also the freezing phase.
  • the gas mixture circulating via the space 202 is heated powerfully, whereby the pressure thereof increases rapidly, and an overpressure is achieved in relation to the object 203 to be dried.
  • the temperature of both the gas mixture and the object is first 10 °C (above), and when the gas mixture is heated to 60 °C and is circulated effectively, heat is transferred therefrom to the object 203 (middle), which eventually reaches the temperature of 60 °C (below).
  • the temperature of the gas mixture is reduced by a certain amount of degrees, defined in the drying schedule, by means of the cooling surfaces 204 located in the cooling channels. This amount of degrees, so called drying range, is here 7 °C.
  • the gas mixture is heated approximately by the same amount of degrees by means of the heating surfaces 206 located in the heating fan channels.
  • the relative humidity of the gas mixture is reduced, and the gas mixture is able to receive water vapour vaporized from the water film on the surface of the object 203 in the drying chamber 202.
  • the water film on the surface takes vaporizing heat from inside of the object, and so the temperature of the object is decreased continuously.
  • the temperature of the gas mixture is maintained at a suitable value lower than the temperature T of the water included in the object to be dried, by means of effective fans and simple control techniques.
  • the cooling and drying phase is continued, until the temperature of the object is descended to such a low temperature, e. g. 10 °C, that vaporization of the water from the object is practically stopped.
  • the temperature of the gas mixture is reduced to -5 °C. Water vapour is then crystallized to snow and ice, and the water content of the circulating gas mixture is only 3 grams in a cubic meter.
  • the operating gas is almost exclusively nitrogen.
  • the equipment includes the following parts: drying chamber 1, transfer carrier 2, supporting grid 4, end walls of the drying chamber 5 and 6, door for ice removal 7, vacuum pump 8, insulation channel 9, cooling channel 10, fan channel 11, condensing tank 12, main wall of the equipment 13, pressure sensor 14, shut-off valves 15 and 16, nitrogen valve 17, circulation fan for nitrogen- water vapour mixture 18, normal air pressure fan 19, tube system for outside heat source 20, heat exchanger 21, heating solution pump 22, valves 23, 24, 25, 26, 27 and 28, cooling solution pumps 29 and 30, heating solution pump 31, control center and computer 32, temperature sensor 33, valve 34, heating battery 35, cooling solution channel 36, nitrogen container 37, main temperature sensor 38, cooling solution container 39, diaphragm expansion containers 40, solution cooling unit 41, temperature sensor 42, cooling solution pump 43, temperature sensor 44, heating solution pump 45, air condenser 46, air condenser fan 47, heating solution container 48, temperature sensors 49 and 50, cooling solution channel for cendenser tank 51, damping material for volume change of ice 52, optical density sensor for water vapour 53, measurement sensor for relative humidity 54, protective agent container
  • Drying chamber 1 is advantageously a cylindrical space free from operating units. The most important operative units are located and the most of the functions of the drying process occur in the circulation channels 9, 10 and 11 for the gas mixture. In relation to the volume of the drying chamber there is room for a large amount of goods 3 to be dried, because there are no operational units causing harm to material transfer, circulation of the gas mixture, and delivering of the mist spray amending the properties of the goods.
  • the basic structure of the equipment is generally symmetrical, and, as is shown in Figure 3, in the longitudal direction of the drying chamber 1 the equipment may be constructed of modules depending on the need of drying capacity.
  • the main wall 13 is made of pressure- tight material with good resistance against mechanical, physical and chemical stresses, for example steel.
  • the insulation channel 9, cooling channel 10, cooling solution channel 36, and normal air pressure channel 62 are located one upon the other in the direction of the radius of the round drying chamber 1, so that two successive channels have one common wall.
  • the channels are essentially as long as the drying chamber.
  • the walls of the circulation channels 9, 10, and 11, and the cooling / heating ribs 60 act as reinforcing elements for the main wall 13, and so the main wall may be made thinner.
  • the circulation channels may be constructed to have large sectional areas, which renders possible the circulation of a big quantity of gas with a small circulation resistance. Respectively, the large cooling and heating surfaces are obtained, whereby big energies may be transferred rapidly. Also the simultaneous use of the surfaces speeds up the drying process.
  • the cooling surfaces are located in the cooling channel 10, in which the circulated saturated water vapour is condensed to water.
  • the surfaces are formed by the main wall 13 and cooling ribs 60.
  • the cooling solution channel 36 forms two cooling surfaces, one working under the vacuum, and another working under the normal pressure, which another one at the same time is the inner wall of the normal air pressure channel 62.
  • the normal air pressure channel is used for melting, preheating, and predrying of timber.
  • the function of the fan channel 11 is to transfer the gas mixture from the cooling channel 10 back to the drying chamber 1.
  • the circulation fans 18 and the heating surfaces 35 are located in the fan channel.
  • the fans are located at both sides of the drying chamber on two levels, so that they never are opposite each other.
  • the motors of the fans act as heating surfaces, too.
  • the location of the fans 18 and the powerful flow of the gas mixture improve delivering and distribution of heat energy to and within the goods 3 to be dried.
  • the condensing tank 12 is designed in such a way that there is room for the whole water amount of the drying process. Condensed water is advantageously freezed, whereby the heat energy released with the freezing may be utilized in the drying process.
  • the inner wall of the condensing tank is provided with a flexible water-repellent damping material 52 having good thermal conductivity, which material accepts the volume change occurring with the freezing of the condensed water.
  • One end wall of the condensing tank 12 is pivoted to provide a pressure-proof door 7, through which the ice is removed.
  • heating solution is during a short time conducted to the cooling solution channels of the cendenser tank, whereby a thin water film is formed between the ice and the damping material and serves as a lubricant when the ice is drawn out.
  • the cooling solution container 39 serves as a store for cooling solution, and the heating solution container 48, respectively, as a store for heating solution. Both of them are also used for leveling the peaks of energy consumption.
  • the cooling solution pumps 29, 30 and 43, and the heating solution pumps 22, 31 and 45 circulate same water-glycol solution, having the same pressure but, respectively, different temperatures, in different parts of the equipment.
  • the sensor 54 for measuring relative humidity is located in the group of main measurement sensors. From the nozzles 58, which are located in front of the fans 18, it is possible to spray agent, for example, which reduces moisture related dimensional changes of wood, to deliver it to the surface of the timber. This is necessary, especially when the timber is dried to a very low percentage of moisture.
  • the fans 18 are utilized for delivering and distributing the spray. When drying reindeer meat, for example, salt solution may me sprayed through the nozzles.
  • the lot of pine timber 3, stacked with sticks on the carrier 2, is transferred to the drying chamber 1.
  • the pine timber lot 3 is supported by the grid 4.
  • the end walls 5 and 6, pivoted to the main wall 13 of the drying chamber 1, and the ice removal door 7 are closed pressure-tightly.
  • the vacuum pump 8 is started by the control center 32.
  • the air in the drying chamber 1, cooling channel 10, fan channel 11, and condensing tank 12 is rarefied, and a partial vacuum is formed therein.
  • the main wall 13 of the equipment serves as a vacuum responsive wall.
  • a message from the pressure sensor 14 stops the vacuum pump, when the total pressure in the vacuum space has reached 40 mbar.
  • the valve 15 is closed, and also the valve 16 still remains closed.
  • the vacuum pump 8 is not started again during the drying process.
  • the shielding nitrogen valve 17 is opened, and nitrogen is introduced to the vacuum space from container 37, until the total pressure reaches 100 mbar.
  • the message from the pressure sensor 14 causes the closing of the valve 17.
  • the control center starts the first heating phase.
  • the fans 18 are activated. They are drived under frequency converter control with a high constant speed of rotation.
  • the fans 19 in the normal air pressure channel 62 are not activated during this drying process, because there is no timber to be predried.
  • Heat energy from outside is taken to the drying process during the first heating phase via the tube system 20.
  • This heat energy is transferred to the water-glycol solution by means of the heat exchanger 21.
  • the pump 22 is run with a high constant speed of rotation.
  • the valves 24, 59 and 25 are open and valves 23, 26, 27 and 28 are closed.
  • the pumps 29, 30, 31, 43 and 45 are not active.
  • the solution cooling unit 41 is not active.
  • the heating ribs 60 intensify the transfer of heat energy to the nitrogen-water vapour mixture.
  • the control center 32 controls the valve 34 according to the value measured by the temperature sensor 33, so that the temperature of water-glycol solution at the place of measurement is constantly kept at + 60 °C.
  • the solution is circulated via the heating battery 35 and the cooling solution channels 36.
  • the heating phase lasts, until the main temperature sensor indicates that the temperature of circulating nitrogen- water vapour mixture is + 60 °C, and the message of the sensor stops the heating phase.
  • the pump 22 is then stopped and the valves 25 and 34 closed.
  • the vacuum space is rapidly filled by saturated nitrogen-water vapour mixture, and the total pressure rises to about 200 mbar during the heating phase.
  • heat enrgy is stored in the timber to be used later for vaporizing water included in the timber.
  • the control center 32 starts the first cooling and drying phase. Solution cooling unit 41 and pumps 31 and 43 are activated.
  • the valves 24 and 23 and 28 are opened.
  • the pumps 30 and 22 are started.
  • the valve 26 is opened and the pump 29 with frequency converter control is started.
  • the control center 32 controls the frequency converter controlled pump 43 according to the value measured by the temperature sensor 49, so that the temperature of the water-glycol mixture at the place of measurement is kept at a desired value, - 10 °C. In the same way the control center 32 controls the speed of rotation of the frequency converter controlled pump 31 according to the value measured by the temperature sensor 44, so that the temperature of the water-glycol mixture at the place of measurement is kept at a desired value, + 40 °C.
  • the diaphragm expansion containers 40 level the pressure variations in the tube system caused by temperature variations of the water-glycol mixture.
  • the control center 32 controls the speed of rotation of the frequency converter controlled pump 29 according to the value measured by the temperature sensor 42, so that the temperature of the water-glycol mixture at the place of measurement is descending and is at the place of measurement 7 °C lower than at the place of the main temperature sensor 38. According to the value measured by the temperature sensor 38 the control center 32 controls the frequency converter controlled pump 22, so that the condensing heat energy bound by the water-glycol solution the temperature of 40 °C is conducted via the heat solution container 48 to the heating batteries 35, so that the temperature of the circulating water-glycol solution is rised approximately by the same amount of degrees, as it was reduced by the cooling.
  • control center 32 controls the frequency converter controlled fans 18, so that the circulated water-glycol solution is at the place of measurement kept as essentially saturated.
  • the vapour pressure of the water-glycol mixture and the total pressure are reduced, and the water film on the surface of the timber starts to vaporize by boiling.
  • the control center 32 controls the frequency converter controlled pump 30 according to the value measured by the temperature sensor 50, so that the temperature of the water- glycol mixture circulating in the cooling solution channels of the condensing tank is at the place of measurement kept at a desired value, - 3 °C.
  • the water is freezed, and the damping material 52 receives the growth of the volume.
  • Heat insulating material 61 covers outside the surface of the cooling solution channels 51 of the condensing tank 12.
  • the drying process produces more heat energy than it consumes.
  • the cooling and drying phase is continued, until the vaporizing energy stored in the timber has been utilized. At that time the temperature of the timber 3 is reduced to the temperature of + 10 °C, and the vaporization of the water film on the surface of timber is ceased. Vaporization is continued through evaporation, and the temperature of the timber lot is still going down. The ending of the vaporization by boiling is observed as a considerable reduction of the speed of rotation of the fans 18, and another heating phase is started.
  • the second and the following heating phases differ from the first heating phase of the drying process so that the valves 28 are open, and that the pump 30, the control thereof, and the solution cooling unit 41 are active. Condensing water is freezed and the melting heat of ice is utilized. The lot of pine timber is heated up to only + 40 °C.
  • the control center 32 drives the frequency converter controlled pump 22 according to the value of measurement of the main temperature sensor 38, until the temperature of the nitrogen- water vapour mixture reaches + 40 °C at the place of measurement. In this drying schedule the heating phase and cooling and drying phase are now carried out successively seven more times.
  • the first phase is started, in which the final percentage of moisture (equilibrium moisture content) is determined.
  • the fans 18 run with a high constant speed of rotation.
  • the solution cooling unit 41 is active.
  • the melting heat of the ice of the condensing tank is utilized.
  • the valves 25, 26 and 27 are closed and the valves 23, 24, 28 and 59 are open.
  • the pumps 29 and 45 are stopped and the pumps 22, 30, 31 and 43 are active.
  • the control center 32 controls the speed of rotation of the frequency converter controlled pump 22 according to the value of measurement of the main temperature sensor 38, so that the temperature of the circulating nitrogen- water vapour mixture at the place of measurement is kept at + 10 °C.
  • the relative humidity sensor 54 measures the relative humidity of the circulating nitrogen-water vapour mixture. When the relative humidity is maintained at an essentially constant value during several minutes, the control center determines the final percentage of moisture.
  • the control center 32 indicates that the constant value of relative humidity is 80 % and determines the value 16.3 % of the final percentage of moisture. Because the required value is 6 ⁇ 1 %, the drying process is continued. The control center 32 performs the eighth heating phase and cooling and drying phase.
  • the first freezing phase is carried out.
  • the valves 26 and 24 are open and the control center 32 drives the pump 29 with a high constant speed of rotation under the control of the main temperature sensor 38, and circulates water-glycol solution, having the temperature of - 10 °C, from the container 39 via the heating batteries 35 and cooling solution channels 36.
  • the water- glycol solution of -10 °C is circulated, until the temperature of the circulating nitrogen- water vapour mixture is reduced to -5 °C, and thereafter the circulation is continued in this drying schedule for about 15 minutes.
  • the control center 32 performs the ninth heating phase and cooling and drying phase and the second freezing phase.
  • the control center 32 indicates that the constant value of relative humidity is 30 % and determines the value 6.2 % of the final percentage of moisture, which is in accordance with the requirements.
  • the drying process is ended: the solution cooling unit 41 and all the pumps are stopped and all the valves are closed.
  • agent which reduces moisture related dimensional changes of wood, is next sprayed to the lot of pine timber.
  • the fans 18 run with a high constant speed of rotation.
  • the open container 55 includes protective agent 56 in liquid form.
  • the valve 57 is opened for a time of 15 seconds.
  • the normal air pressure pushes liquid to the nozzles 58, from which it is sprayed to the circulating nitrogen- water vapour mixture and fluctuates further on the surface of the timber and is absorbed to the surface layer.
  • the fans 18 are stopped after 30 seconds from the opening of the valve 57.
  • the valve 16 is opened and normal air pressure is let to the vacuum space, which at the same time speeds up absorption of the protective agent.
  • the end walls 5 and 6 and the ice removal door 7 are opened.
  • the valves 23 and 27 are opened and the pump 22 is started to run with a high constant speed of rotation.
  • the control center 32 drives the pump for about 15 minutes.
  • the warm water-glycol solution is circulated in the cooling solution channels 51 of the condensing tank 12, whereby a thin film of water is formed between the ice and the damping material 52 and helps with removal of the ice from the condensing tank 12.
  • the ice is conveyed to outdoor air for melting, and the lot of pine timber 3 is transferred out from the drying chamber 1.
  • the vaporization heat of water and melting heat of ice released during the timber drying process may be utilized for melting freezed timber or for preheating or predrying the timber. Then the melting, preheating and predrying may be carried out simultaneously with the drying process applying the principle of one drying chamber within another one, whereby the inner drying chamber is according to the invention, and the normal air pressure channels 62 and fans 19 thereof are utilized.
  • the transfer of heat energy happens from the inner drying chamber by means of the outer pump 45, air condenser 46 and fan 47.
  • the air condenser may be replaced by a liquid condenser.
  • the removal of the ice from the condensing tank 12 may, alternatively, be carried out as a continuous process. Then an ice removal device removes ice from the condensing tank to the normal air pressure in proportion to the formation of ice.
  • the ice serves as a pressure-tight wall or plug and the water as a lubricant and sealing material between the ice and the wall of the condensing tank. In this case the condensing tank may be quite small.
  • Figures 5 and 6 present a very simple equipment accomplishing the method of the invention.
  • An object 3, e. g. timber, to be dried is located in a first part of a ring-shaped tube.
  • Nitrogen- water vapour mixture is caused to move rotatively along a main wall 71 of a cooling channel 70 by means of a fan 73 and a spiral-shaped heat exchanger 80, which is located in a second part of the tube.
  • the first half 81 of the heat exchanger serves as a cooling surface and the second half 82 as a heating surface.
  • the heat exchanger 80 serves as a whole as a cooling surface, and during the heating phase as a whole as a heating surface.
  • the centrifugal force helps to extract water droplets from the saturated water vapour.
  • the control of the drying process is based on utilization of the condition of saturation, the drying range, and the vapour pressure range, and on monitoring the current frequency changes of the frequency converter controlled motors of the circulating fans.
  • the drying range is the magnitude of the temperature difference, amount of degrees, which the gas mixture is during the cooling and drying phase first cooled and then, respectively, heated.
  • the vapour pressure range is the difference between the pressure of the gas mixture and the water vapour pressure in the material to be dried, which difference is temperature related.
  • the main measurement sensors of the drying process are located immediately after the object 3 to be dried in the direction of gas mixture flow. According to the measurement values of these sensors the frequency controlled fans 18 are adjusted steplessly during the cooling and drying phase, so that the drying process is kept in essentially saturated condition at the place of measurement.
  • the stepless control and adjustment of the drying process result in that the water amount condensed from the saturated water vapour is essentially the same as the amount of water which may be vaporized from the object in the drying chamber, i. e. the drying time is the shortest possible as the drying defects are taken into account.
  • the drying process is maintained in a saturated condition between the drying chamber 1 and the heating surfaces 35, and close to the saturated condition in the space after the heating surfaces and in the drying chamber.
  • the use of the vacuum pump to rarefy air only in the beginning of the drying process makes the control of the drying process easier. Then the variations of the total pressure and temperature, which follow the use of the pump, are avoided, and as the amount of variables is reduced the control of the drying process is simplified.
  • the stepless control of the drying process means that no shut-off device, e. g. a pressure control valve, is needed between the drying chamber 1 and the cooling surface 60. No sensors need to be attached to the object 3 to be dried for the purpose of controlling and adjusting the drying process, and it is not necessary to know the percentage of moisture or amount of water of the object when starting the process. In the beginning of the drying process the final percentage of moisture and the identification of the drying schedule, which is based on the kind of wood and the thickness to be dried, are input to the control center 32.
  • a shut-off device e. g. a pressure control valve
  • drying schedules for different kinds of woods are prepared, by means of which the shortest possible drying time is achieved taking into account the thickness to be dried and the minimum amount of drying defects. Additionally, special drying schedules are prepared so that by means of them the properties like colour, strength, stiffness, or dimensional stability in relation to moisture, appreciated by the final user, e. g. a carpenter, may be emphasized.
  • the cooling efficiency of the cooling surfaces 60 is controlled by the temperature sensor 42, which is located between the cooling surface and the heating surface. According to the value measured by this temperature sensor the control center 32 controls the speed of rotation of the frequency converter controlled pump 29 for cooling solution, maintaining the temperature of the nitrogen- water vapour mixture at the desired value at the place of measurement.
  • the value is the amount of the drying range between the main temperature sensor 38 and this so-called cooling temperature sensor 42.
  • the heating efficiency of the heating surfaces 35 is controlled according to the value measured by the main temperature sensor 38, so that the control center 32 adjusts the speed of rotation of the frequency converter controlled pump 22 for heating solution in such a way that the temperature of the gas mixture at the place of measurement is maintained at a certain value in accordance with the drying schedule.
  • the drying process is controlled by the main temperature sensor 38 in accordance with the drying schedule, and the speed of rotation of the fans 18 is limited to a high value corresponding to a certain frequency.
  • the duration of the cooling and drying phase become longer.
  • the duration depends also on the kind of wood and thickness of the timber. According to the lengthening of the duration the control center determines approximately the percentage of moisture of the timber, and determines also the final percentage of moisture (equilibrium moisture content) by means of function point method, for example.
  • a further possibility to amend the method and equipment of the invention may be to direct ultrasound periodically towards the object to be dried during the drying process, especially when timber is dried. It is thought that ultrasound could help leveling the moisture in the object and removal of moisture therefrom. Besides that, it could release the stresses produced in the timber and affect advantageously the cell structure of the timber.
  • the invention is not limited to the above embodiments, but may be varied within the scope of the accompanying claims.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Drying Of Solid Materials (AREA)
PCT/FI1998/000151 1997-02-21 1998-02-19 Method and equipment for drying an object including water WO1998037371A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI970727 1997-02-21
FI970727A FI101423B (sv) 1997-02-21 1997-02-21 Förfarande och anordning för torkning av objekt som innehåller vatten

Publications (1)

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WO1998037371A1 true WO1998037371A1 (en) 1998-08-27

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PCT/FI1998/000151 WO1998037371A1 (en) 1997-02-21 1998-02-19 Method and equipment for drying an object including water

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FI (1) FI101423B (sv)
WO (1) WO1998037371A1 (sv)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2786424A1 (fr) * 1998-11-27 2000-06-02 Arimpex Sarl Procede de traitement thermique d'un materiau ligno-cellulosique par confinement des gaz, et materiau ligno-cellulosique susceptible d'etre obtenu par ce procede
WO2000053983A1 (de) * 1999-03-11 2000-09-14 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und verfahren zum vakuumtrocknen
WO2003014644A1 (en) * 2001-08-11 2003-02-20 Dunne, Terence, Patrick Processing of organic material
EP1593921A1 (de) * 2004-05-03 2005-11-09 Schoell Albrecht Vorrichtung zum Trocknen von Holz
EP1748268A2 (de) * 2005-07-29 2007-01-31 Josef Walderdorff Verfahren zum Trocknen von Gütern
CN110328123A (zh) * 2019-06-24 2019-10-15 深圳市华星光电技术有限公司 真空干燥装置及去除残余溶剂的方法
CN115790106A (zh) * 2022-12-13 2023-03-14 深圳新宙邦科技股份有限公司 一种树脂除水方法及除水装置

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113739556B (zh) * 2021-07-21 2023-01-10 广东申菱环境系统股份有限公司 一种热泵烘干机组及其控制方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3939573A (en) * 1974-10-31 1976-02-24 Furio Berti Process for drying wood
US4058906A (en) * 1975-05-19 1977-11-22 Ernesto Guglielmo Pagnozzi Process for drying large pieces of wood at subatmospheric pressure or in vacuo, particularly for drying delicate wood and/or wood which is easily split
US4246704A (en) * 1978-04-13 1981-01-27 Vincenzo Pagnozzi Process and plant for drying solid wood in planks or semifinished products by means of a superheated steam system

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3939573A (en) * 1974-10-31 1976-02-24 Furio Berti Process for drying wood
US4058906A (en) * 1975-05-19 1977-11-22 Ernesto Guglielmo Pagnozzi Process for drying large pieces of wood at subatmospheric pressure or in vacuo, particularly for drying delicate wood and/or wood which is easily split
US4246704A (en) * 1978-04-13 1981-01-27 Vincenzo Pagnozzi Process and plant for drying solid wood in planks or semifinished products by means of a superheated steam system

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2786424A1 (fr) * 1998-11-27 2000-06-02 Arimpex Sarl Procede de traitement thermique d'un materiau ligno-cellulosique par confinement des gaz, et materiau ligno-cellulosique susceptible d'etre obtenu par ce procede
WO2000053983A1 (de) * 1999-03-11 2000-09-14 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und verfahren zum vakuumtrocknen
WO2003014644A1 (en) * 2001-08-11 2003-02-20 Dunne, Terence, Patrick Processing of organic material
EA008518B1 (ru) * 2001-08-11 2007-06-29 Данн, Теренс Патрик Обработка органического материала
KR100858888B1 (ko) * 2001-08-11 2008-09-17 듄, 테렌스, 패트릭 유기 물질 프로세싱 방법 및 프로세싱 장치
CN100422681C (zh) * 2001-08-11 2008-10-01 特伦斯·帕特里克·邓尼 有机物的处理
EP1593921A1 (de) * 2004-05-03 2005-11-09 Schoell Albrecht Vorrichtung zum Trocknen von Holz
EP1748268A2 (de) * 2005-07-29 2007-01-31 Josef Walderdorff Verfahren zum Trocknen von Gütern
EP1748268A3 (de) * 2005-07-29 2011-11-02 Josef Walderdorff Verfahren zum Trocknen von Gütern
CN110328123A (zh) * 2019-06-24 2019-10-15 深圳市华星光电技术有限公司 真空干燥装置及去除残余溶剂的方法
CN115790106A (zh) * 2022-12-13 2023-03-14 深圳新宙邦科技股份有限公司 一种树脂除水方法及除水装置

Also Published As

Publication number Publication date
FI101423B1 (sv) 1998-06-15
FI970727A0 (fi) 1997-02-21
FI101423B (sv) 1998-06-15

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