UY33096A - Sal dimetilamina de glifosato cristalina metodo de produccion y uso de la misma - Google Patents

Sal dimetilamina de glifosato cristalina metodo de produccion y uso de la misma

Info

Publication number
UY33096A
UY33096A UY0001033096A UY33096A UY33096A UY 33096 A UY33096 A UY 33096A UY 0001033096 A UY0001033096 A UY 0001033096A UY 33096 A UY33096 A UY 33096A UY 33096 A UY33096 A UY 33096A
Authority
UY
Uruguay
Prior art keywords
glyphosate
crystaline
production
same
glyphosate salt
Prior art date
Application number
UY0001033096A
Other languages
English (en)
Inventor
Wei Wang
Shuguang Zhou
Long Qin
Bufan Ren
Zhingang Qian
Tao Liu
Huiling She
Yaxian Zhang
Original Assignee
Zhejiang Xinan Chemical Industry Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhejiang Xinan Chemical Industry Group Co Ltd filed Critical Zhejiang Xinan Chemical Industry Group Co Ltd
Publication of UY33096A publication Critical patent/UY33096A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/04—Nitrogen directly attached to aliphatic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/03—Monoamines
    • C07C211/04—Mono-, di- or tri-methylamine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Engineering & Computer Science (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Esta invención proporciona el ingrediente activo herbicida, un cristal de sal dimetilamina de N-fosfonometil glicina (glifosato), su proceso de preparación y una formulación sólida que contiene la sal dimetilamina de glifosato cristalina y su aplicación. Dicho proceso comprende agregar glifosato y una cantidad de solvente en un reactor convencional e introducir un gas dimetilamina, en donde la temperatura de reacción se controla entre 5 y 90 ºC. Una vez completada la reacción, la temperatura se reduce lentamente a cierto valor, se precipita una sal dimetilamina de glifosato cristalina (o se precipita después de agregar un cristal semilla).
UY0001033096A 2009-12-09 2010-12-09 Sal dimetilamina de glifosato cristalina metodo de produccion y uso de la misma UY33096A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN200910154988A CN101723973B (zh) 2009-12-09 2009-12-09 一种制备草甘膦二甲胺盐固体的方法

Publications (1)

Publication Number Publication Date
UY33096A true UY33096A (es) 2011-04-29

Family

ID=42445591

Family Applications (1)

Application Number Title Priority Date Filing Date
UY0001033096A UY33096A (es) 2009-12-09 2010-12-09 Sal dimetilamina de glifosato cristalina metodo de produccion y uso de la misma

Country Status (8)

Country Link
US (1) US9221853B2 (es)
CN (2) CN101723973B (es)
AR (1) AR079337A1 (es)
AU (1) AU2010330585B2 (es)
BR (1) BR112012013914A2 (es)
UY (1) UY33096A (es)
WO (1) WO2011069324A1 (es)
ZA (1) ZA201204116B (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101723973B (zh) 2009-12-09 2012-09-26 浙江新安化工集团股份有限公司 一种制备草甘膦二甲胺盐固体的方法
CN102870803A (zh) * 2011-07-11 2013-01-16 浙江新安化工集团股份有限公司 固体除草剂组合物
CN103819375B (zh) * 2014-01-21 2016-04-13 青岛惠国新材料科技有限公司 一种高纯度固体福美钠的合成方法
CN104592014A (zh) * 2015-01-04 2015-05-06 安徽省化工研究院 一种麦草畏二甲胺盐原料药的制备方法
CN106188137B (zh) * 2015-06-01 2018-04-24 浙江金帆达生化股份有限公司 一种制备高含量草甘膦二甲胺盐的方法
CN106279271A (zh) * 2015-06-01 2017-01-04 浙江金帆达生化股份有限公司 一种制备高含量草甘膦异丙胺盐的方法
CN106259324B (zh) * 2016-07-14 2020-03-17 山东润博生物科技有限公司 一种草甘膦二甲胺盐水溶性粒剂及其制备方法
CN106614719A (zh) * 2016-12-27 2017-05-10 四川福思达生物技术开发有限责任公司 一种含草甘膦二甲胺盐和异壬酸二甲胺盐的农药组合物及其制备方法和应用
CN109757482A (zh) * 2017-11-09 2019-05-17 山东润博生物科技有限公司 一种农药二甲胺盐水剂的连续化制备方法
CN109757484A (zh) * 2017-11-09 2019-05-17 山东润博生物科技有限公司 一种农药二甲胺盐水剂的制备方法
CN109757472A (zh) * 2017-11-09 2019-05-17 山东润博生物科技有限公司 一种羧酸类二甲胺盐颗粒剂的制备方法
CN110437279B (zh) * 2019-08-27 2022-02-08 鹤壁市鹤农生物科技有限公司 一种草甘膦铵盐原药的制备方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3799758A (en) * 1971-08-09 1974-03-26 Monsanto Co N-phosphonomethyl-glycine phytotoxicant compositions
US4659860A (en) * 1971-08-09 1987-04-21 Monsanto Company Thioester of n-phosphonomethylglycine
IL101539A (en) * 1991-04-16 1998-09-24 Monsanto Europe Sa Mono-ammonium salts of the history of N phosphonomethyl glycyl which are not hygroscopes, their preparations and pesticides containing
HU214948B (hu) * 1992-10-26 1998-08-28 Monsanto Europe S.A. Eljárás nemhigroszkópos N-(foszfono-metil)-glicin-monoammónium-sók előállítására
CN1260344A (zh) 1999-08-13 2000-07-19 浙江新安化工集团股份有限公司 三氯乙酰氯的制备方法
CN1165541C (zh) 2000-08-31 2004-09-08 浙江新安化工集团股份有限公司 草甘膦酸铵合成工艺
CN1244587C (zh) 2002-09-05 2006-03-08 浙江新安化工集团股份有限公司 气－液－固三相反应及溶剂萃取制备草甘膦酸铵
CN1958594B (zh) * 2006-11-17 2011-08-10 浙江新安化工集团股份有限公司 一种制备草甘膦异丙胺盐固体的方法
CN101186622B (zh) 2006-11-17 2013-03-20 浙江新安化工集团股份有限公司 一种制备固体草甘膦钾盐的方法
CN101723973B (zh) * 2009-12-09 2012-09-26 浙江新安化工集团股份有限公司 一种制备草甘膦二甲胺盐固体的方法

Also Published As

Publication number Publication date
CN101723973B (zh) 2012-09-26
AU2010330585B2 (en) 2016-04-21
AR079337A1 (es) 2012-01-18
CN102803278A (zh) 2012-11-28
ZA201204116B (en) 2013-02-27
US20150307528A1 (en) 2015-10-29
AU2010330585A1 (en) 2012-06-21
WO2011069324A1 (zh) 2011-06-16
US9221853B2 (en) 2015-12-29
BR112012013914A2 (pt) 2016-04-26
CN101723973A (zh) 2010-06-09

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Effective date: 20181127