US3902862A - Nickel-base superalloy articles and method for producing the same - Google Patents

Nickel-base superalloy articles and method for producing the same Download PDF

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Publication number
US3902862A
US3902862A US288234A US28823472A US3902862A US 3902862 A US3902862 A US 3902862A US 288234 A US288234 A US 288234A US 28823472 A US28823472 A US 28823472A US 3902862 A US3902862 A US 3902862A
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United States
Prior art keywords
nickel
article
tantalum
tungsten
base superalloy
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US288234A
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English (en)
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John H Moll
August Kasak
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Crucible Materials Corp
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Crucible Inc
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Priority to US288234A priority Critical patent/US3902862A/en
Priority to GB1897273A priority patent/GB1384212A/en
Priority to SE7306634A priority patent/SE401206B/xx
Priority to IT50117/73A priority patent/IT985117B/it
Priority to DE2326284A priority patent/DE2326284A1/de
Priority to FR7319291A priority patent/FR2199002B1/fr
Priority to JP48059423A priority patent/JPS5143802B2/ja
Priority to AT471773A priority patent/AT329887B/de
Publication of US3902862A publication Critical patent/US3902862A/en
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Assigned to COLT INDUSTRIES OPERATING CORP. reassignment COLT INDUSTRIES OPERATING CORP. MERGER AND CHANGE OF NAME Assignors: CRUCIBLE CENTER COMPANY (INTO) CRUCIBLE INC. (CHANGED TO)
Assigned to CRUCIBLE MATERIALS CORPORATION reassignment CRUCIBLE MATERIALS CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST. Assignors: COLT INDUSTRIES OPERATING CORP.
Assigned to MELLON BANK, N.A. FOR THE CHASE MANHATTAN BANK (NATIONAL ASSOCIATION) AND MELLON BANK N.A., CHASE MANHATTAN BANK, THE (NATIONAL ASSOCIATION) AS AGENT reassignment MELLON BANK, N.A. FOR THE CHASE MANHATTAN BANK (NATIONAL ASSOCIATION) AND MELLON BANK N.A. SECURITY INTEREST (SEE DOCUMENT FOR DETAILS). 1ST Assignors: CRUCIBLE MATERIALS CORPORATION, A CORP. OF DE.
Assigned to MELLON FINANCIAL SERVICES CORPORATION, MELLON BANK, N.A. AS AGENT FOR MELLON BANK N.A. & MELLON FINANCIAL SERVICES CORPORATION reassignment MELLON FINANCIAL SERVICES CORPORATION SECURITY INTEREST (SEE DOCUMENT FOR DETAILS). 2ND Assignors: CRUCIBLE MATERIALS CORPORATION, A CORP. OF DE.
Assigned to CRUCIBLE MATERIALS CORPORATION reassignment CRUCIBLE MATERIALS CORPORATION RELEASED BY SECURED PARTY (SEE DOCUMENT FOR DETAILS). Assignors: MELLON BANK, N.A.
Assigned to MELLON BANK, N.A. AS AGENT reassignment MELLON BANK, N.A. AS AGENT SECURITY INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: CRUCIBLE MATERIALS CORPORATION, A CORPORATION OF DE
Assigned to MELLON BANK, N.A. reassignment MELLON BANK, N.A. SECURITY INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: CHASE MANHATTAN BANK (NATIONAL ASSOCIATION), THE
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    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C19/00—Alloys based on nickel or cobalt
    • C22C19/03—Alloys based on nickel or cobalt based on nickel
    • C22C19/05—Alloys based on nickel or cobalt based on nickel with chromium
    • C22C19/051—Alloys based on nickel or cobalt based on nickel with chromium and Mo or W
    • C22C19/056—Alloys based on nickel or cobalt based on nickel with chromium and Mo or W with the maximum Cr content being at least 10% but less than 20%
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C1/00—Making non-ferrous alloys
    • C22C1/04—Making non-ferrous alloys by powder metallurgy
    • C22C1/0433—Nickel- or cobalt-based alloys

Definitions

  • Nickel-base superalloys are conventionally used as constructional materials for high-temperature service applications, such as the components for jet engines which are subject during service to high operating temperatures. In many applications the components made from these alloys must exhibit high strength and hardness at elevated temperatures. This is customarily achieved by increasing the alloy content of strengthening elements, such as titanium, aluminum, columbium, tantalum, hafnium, tungsten and molybdenum.
  • FIGS. 1, 2 and 3 are photomicrographs at a magnification of 100X of three compacted powder alloy articles, with the articles of FIGS. 1 and 2 being in accordance with the present invention and with the article of FIG. 3 being outside the scope of the present invention.
  • FIGS. 4, S and 6 are photographs at a magnification of 15X of the articles of FIGS. 1, 2 and 3, respectively, showing the features of specimens of these articles treated in tension.
  • nickel-base superalloys within the composition limits of Table I in the form of prealloyed powder and compacted to form articles having a density exceeding of theoretical, are characterized by a uniform distribution of minor phases. This, as will be shown hereinafter, provides articles of improved strength and ductility. Consequently, the term fully dense as used herein means a compacted article having a density exceeding 95% of theoretical density.
  • the size of the particles used for compacting in accordance with the present invention typically does not exceed minus 16 mesh US. Standard and generally will not exceed minus 30 mesh.
  • Alloys A and B of Table II are within the scope of this invention; whereas, Alloy C is outside the scope of the invention.
  • Prealloyed powder suitable for compacting was prepared from each of the alloys of Table II by melting a charge of the composition under an inert atmosphere, atomizing a stream of the molten metal by striking it with a jet of argon gas and subsequently rapidly cooling the atomized particles to ambient temperature.
  • the powder was collected and screened to minus 100 mesh and loaded in cylindrical mild-steel containers having a height of 9 inches and a diameter of 2.6 inches. The containers were evacuated to remove any moisture present therein and sealed against the atmosphere.
  • FIGS. 1, 2 and 3 are photomicrographs, as earlier described, of articles from Alloys A,, B and C, respectively.
  • FIGS. 4, 5 and 6 are photographs as earlier described of fractured tensile specimens of the articles of Alloys A, B and C, respectively.
  • the fracture of Alloy C, as shown in FIG. 6, is characterized by the ball and socket type fracture, which indicates fracture propagation along the spherical path of a particle boundary at which minor-phase concentration had occurred.
  • test specimen was machined from a consolidated powder product of Alloy A and tested in tension at 1950F under a constant head speed of 0.1 in./min.
  • the test temperature selected is representative of that normally used to fabricate nickel-base alloys into useful shapes by forging, extrusion or rolling. The results of the test were as follows:
  • a nickel-base superalloy compacted, fully dense article produced by elevated-temperature compacting of prealloyed powder particles consisting essentially of, in weight percent, carbon 0.15 to 0.25, chromium 10.5 to 14.5, cobalt 8 to 10, molybdenum l to 3, tungsten. 3 to 5, tantalum 3 to 5, titanium 3.2 to 5, aluminum 2.2 to 4.2, boron 0:00] to 0.03, zirconium 0.01 to 0.20, balance essentially nickel, said article being characterized by the absence of minor phase concentrations at prior powder-particle boundaries.
  • a nickel-base superalloy compacted, fully dense article produced by elevated-temperature compacting of prealloyed powder particles consisting essentially of, in weight percent, carbon 0.01 to 0.20, chromium 12 to 16, cobalt 7 to 9, molybdenum 2.5 to 4.5, tungsten 2.5 to 4.5, columbium 2.5 to 4.5, titanium 1.5 to 3.5, aluminum 2.5 to 4.5, boron 0.001 to 0.03, zirconium 0.01 to 0.20, balance essentially nickel, said article being characterized by the absence of minor phase concentrations at prior powder-particle boundaries.
  • prealloyed powder particles consisting essentially of, in weight percent, carbon 0.2 to 0.4, chromium 10 to 14, cobalt 9 to 11, molybdenum l to 4, tungsten 5 to 7, tantalum 0.5 to 2.5, titanium 2 to 4, aluminum 3.5 to'5.5, boron 0.001 to 0.03, zirconium 0.01 to 0.20, balance essentially nickel, said article being characterized by the absence of minor phase concentrations at prior powder-particle boundaries.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Powder Metallurgy (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
US288234A 1972-09-11 1972-09-11 Nickel-base superalloy articles and method for producing the same Expired - Lifetime US3902862A (en)

Priority Applications (8)

Application Number Priority Date Filing Date Title
US288234A US3902862A (en) 1972-09-11 1972-09-11 Nickel-base superalloy articles and method for producing the same
GB1897273A GB1384212A (en) 1972-09-11 1973-04-19 Nickel-base superalloy articles
SE7306634A SE401206B (sv) 1972-09-11 1973-05-10 Helt tett pressat foremal av nickelbaserad varmhallfast legering
IT50117/73A IT985117B (it) 1972-09-11 1973-05-22 Articoli in superlega a base di nichel
DE2326284A DE2326284A1 (de) 1972-09-11 1973-05-23 Werkstueck aus einer verdichteten superlegierung auf ni-basis
FR7319291A FR2199002B1 (enrdf_load_stackoverflow) 1972-09-11 1973-05-28
AT471773A AT329887B (de) 1972-09-11 1973-05-29 Werkstuck aus einer verdichteten superlegierung auf nickelbasis
JP48059423A JPS5143802B2 (enrdf_load_stackoverflow) 1972-09-11 1973-05-29

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US288234A US3902862A (en) 1972-09-11 1972-09-11 Nickel-base superalloy articles and method for producing the same

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US3902862A true US3902862A (en) 1975-09-02

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US (1) US3902862A (enrdf_load_stackoverflow)
JP (1) JPS5143802B2 (enrdf_load_stackoverflow)
AT (1) AT329887B (enrdf_load_stackoverflow)
DE (1) DE2326284A1 (enrdf_load_stackoverflow)
FR (1) FR2199002B1 (enrdf_load_stackoverflow)
GB (1) GB1384212A (enrdf_load_stackoverflow)
IT (1) IT985117B (enrdf_load_stackoverflow)
SE (1) SE401206B (enrdf_load_stackoverflow)

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4066449A (en) * 1974-09-26 1978-01-03 Havel Charles J Method for processing and densifying metal powder
US4492672A (en) * 1982-04-19 1985-01-08 The United States Of America As Represented By The Secretary Of The Navy Enhanced microstructural stability of nickel alloys
US5130086A (en) * 1987-07-31 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloys
US5130087A (en) * 1989-01-03 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloys
US5130089A (en) * 1988-12-29 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloy
US5130088A (en) * 1987-10-02 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloys
US5330711A (en) * 1991-02-07 1994-07-19 Rolls-Royce Plc Nickel base alloys for castings
US6120853A (en) * 1996-10-30 2000-09-19 Fuji Photo Film Co., Ltd. Slide bead coating method and apparatus
US20040223868A1 (en) * 2003-05-09 2004-11-11 General Electric Company Nickel-base alloy
US20050120941A1 (en) * 2003-12-04 2005-06-09 Yiping Hu Methods for repair of single crystal superalloys by laser welding and products thereof
FR2935396A1 (fr) * 2008-08-26 2010-03-05 Aubert & Duval Sa Procede de preparation d'une piece en superalliage base nickel et piece ainsi obtenue.
US10247480B2 (en) 2017-04-28 2019-04-02 General Electric Company High temperature furnace
US20210292873A1 (en) * 2018-07-31 2021-09-23 Safran Nickel-based superalloy for manufacturing a part by powder forming
US20210301372A1 (en) * 2018-08-02 2021-09-30 Lpw Technology Ltd Nickel-based alloy powder
US20210355564A1 (en) * 2018-09-13 2021-11-18 Aubert & Duval Nickel-based superalloys
EP4257716A1 (en) * 2022-04-08 2023-10-11 General Electric Company Compositions, articles and methods for forming the same

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2555205B1 (fr) * 1983-11-22 1989-05-19 Metalimphy Alliages a base de nickel pour la metallurgie des poudres destines a des disques de turbines a gaz
JPS6179754A (ja) * 1984-09-26 1986-04-23 Hitachi Ltd 焼結Ｎｉ基耐熱合金の製造法
JP3067416B2 (ja) * 1992-08-20 2000-07-17 三菱マテリアル株式会社 高温耐熱部品製造用Ｎｉ基合金粉末
RU2308354C1 (ru) * 2006-03-02 2007-10-20 Открытое акционерное общество "Всероссийский институт легких сплавов" (ОАО "ВИЛС") Способ получения изделий из гранул жаропрочных никелевых сплавов
RU2299919C1 (ru) * 2006-03-02 2007-05-27 Открытое акционерное общество "Всероссийский институт легких сплавов" (ОАО "ВИЛС") Порошковый жаропрочный сплав на основе никеля
FR2899240B1 (fr) * 2006-03-31 2008-06-27 Snecma Sa Alliage a base de nickel
RU2368683C1 (ru) * 2008-03-05 2009-09-27 Открытое акционерное общество "Всероссийский Институт Легких сплавов" (ОАО ВИЛС) Порошковый жаропрочный никелевый сплав
RU2371495C1 (ru) * 2008-06-20 2009-10-27 Открытое акционерное общество "Всероссийский Институт Легких сплавов" (ОАО ВИЛС) Жаропрочный порошковый никелевый сплав
FR2935395B1 (fr) * 2008-08-26 2010-09-24 Aubert & Duval Sa Procede de preparation d'une piece en superalliage base nickel et piece ainsi preparee
GB2567492B (en) * 2017-10-16 2020-09-23 Oxmet Tech Limited A nickel-based alloy
CN116949320A (zh) * 2023-09-21 2023-10-27 苏州倍丰智能科技有限公司 一种3d打印用高温合金粉末、制备方法及打印方法

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2920956A (en) * 1956-10-08 1960-01-12 Universal Cyclops Steel Corp Method of preparing high temperature alloys
US3343950A (en) * 1963-12-23 1967-09-26 Int Nickel Co Nickel-chromium alloys useful in the production of wrought articles for high temperature application
US3390023A (en) * 1965-02-04 1968-06-25 North American Rockwell Method of heat treating age-hardenable alloys
US3459545A (en) * 1967-02-20 1969-08-05 Int Nickel Co Cast nickel-base alloy
US3524744A (en) * 1966-01-03 1970-08-18 Iit Res Inst Nickel base alloys and process for their manufacture
US3561955A (en) * 1966-08-30 1971-02-09 Martin Marietta Corp Stable nickel base alloy
US3615376A (en) * 1968-11-01 1971-10-26 Gen Electric Cast nickel base alloy
US3649256A (en) * 1970-02-16 1972-03-14 Latrobe Steel Co Fully dense consolidated-powder superalloys
US3655458A (en) * 1970-07-10 1972-04-11 Federal Mogul Corp Process for making nickel-based superalloys
US3671230A (en) * 1969-02-19 1972-06-20 Federal Mogul Corp Method of making superalloys
US3677748A (en) * 1969-11-19 1972-07-18 Martin Marietta Corp Alloy
US3681061A (en) * 1970-02-16 1972-08-01 Latrobe Steel Co Fully dense consolidated-powder superalloys

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1224804A (en) * 1968-10-18 1971-03-10 Gen Electric Co Ltd Improvements in or relating to sintered nickel-based alloys

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2920956A (en) * 1956-10-08 1960-01-12 Universal Cyclops Steel Corp Method of preparing high temperature alloys
US3343950A (en) * 1963-12-23 1967-09-26 Int Nickel Co Nickel-chromium alloys useful in the production of wrought articles for high temperature application
US3390023A (en) * 1965-02-04 1968-06-25 North American Rockwell Method of heat treating age-hardenable alloys
US3524744A (en) * 1966-01-03 1970-08-18 Iit Res Inst Nickel base alloys and process for their manufacture
US3561955A (en) * 1966-08-30 1971-02-09 Martin Marietta Corp Stable nickel base alloy
US3459545A (en) * 1967-02-20 1969-08-05 Int Nickel Co Cast nickel-base alloy
US3615376A (en) * 1968-11-01 1971-10-26 Gen Electric Cast nickel base alloy
US3671230A (en) * 1969-02-19 1972-06-20 Federal Mogul Corp Method of making superalloys
US3677748A (en) * 1969-11-19 1972-07-18 Martin Marietta Corp Alloy
US3649256A (en) * 1970-02-16 1972-03-14 Latrobe Steel Co Fully dense consolidated-powder superalloys
US3681061A (en) * 1970-02-16 1972-08-01 Latrobe Steel Co Fully dense consolidated-powder superalloys
US3655458A (en) * 1970-07-10 1972-04-11 Federal Mogul Corp Process for making nickel-based superalloys

Cited By (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4066449A (en) * 1974-09-26 1978-01-03 Havel Charles J Method for processing and densifying metal powder
US4492672A (en) * 1982-04-19 1985-01-08 The United States Of America As Represented By The Secretary Of The Navy Enhanced microstructural stability of nickel alloys
US5130086A (en) * 1987-07-31 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloys
US5130088A (en) * 1987-10-02 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloys
US5130089A (en) * 1988-12-29 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloy
US5130087A (en) * 1989-01-03 1992-07-14 General Electric Company Fatigue crack resistant nickel base superalloys
US5330711A (en) * 1991-02-07 1994-07-19 Rolls-Royce Plc Nickel base alloys for castings
US6120853A (en) * 1996-10-30 2000-09-19 Fuji Photo Film Co., Ltd. Slide bead coating method and apparatus
CN100355922C (zh) * 2003-05-09 2007-12-19 通用电气公司 镍基合金
US6902633B2 (en) * 2003-05-09 2005-06-07 General Electric Company Nickel-base-alloy
US20040223868A1 (en) * 2003-05-09 2004-11-11 General Electric Company Nickel-base alloy
US20050120941A1 (en) * 2003-12-04 2005-06-09 Yiping Hu Methods for repair of single crystal superalloys by laser welding and products thereof
US7250081B2 (en) 2003-12-04 2007-07-31 Honeywell International, Inc. Methods for repair of single crystal superalloys by laser welding and products thereof
WO2010023405A3 (fr) * 2008-08-26 2014-09-04 Aubert & Duval Procédé de préparation d'une pièce en superalliage base nickel et pièce ainsi obtenue
US20110150693A1 (en) * 2008-08-26 2011-06-23 Raisson Gerard Method for preparing a nickel superalloy part, and the part thus obtained
FR2935396A1 (fr) * 2008-08-26 2010-03-05 Aubert & Duval Sa Procede de preparation d'une piece en superalliage base nickel et piece ainsi obtenue.
US8889064B2 (en) 2008-08-26 2014-11-18 Aubert & Duval Method for preparing a nickel superalloy part, and the part thus obtained
US10247480B2 (en) 2017-04-28 2019-04-02 General Electric Company High temperature furnace
US20210292873A1 (en) * 2018-07-31 2021-09-23 Safran Nickel-based superalloy for manufacturing a part by powder forming
US12435392B2 (en) * 2018-07-31 2025-10-07 Safran Nickel-based superalloy for manufacturing a part by powder forming
US20210301372A1 (en) * 2018-08-02 2021-09-30 Lpw Technology Ltd Nickel-based alloy powder
US12006558B2 (en) * 2018-08-02 2024-06-11 Lpw Technology Ltd Nickel-based alloy powder
US20210355564A1 (en) * 2018-09-13 2021-11-18 Aubert & Duval Nickel-based superalloys
EP4257716A1 (en) * 2022-04-08 2023-10-11 General Electric Company Compositions, articles and methods for forming the same

Also Published As

Publication number Publication date
JPS4965909A (enrdf_load_stackoverflow) 1974-06-26
SE401206B (sv) 1978-04-24
IT985117B (it) 1974-11-30
GB1384212A (en) 1975-02-19
DE2326284A1 (de) 1974-04-04
JPS5143802B2 (enrdf_load_stackoverflow) 1976-11-25
AT329887B (de) 1976-06-10
FR2199002B1 (enrdf_load_stackoverflow) 1976-04-23
ATA471773A (de) 1975-08-15
FR2199002A1 (enrdf_load_stackoverflow) 1974-04-05

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Free format text: SECURITY INTEREST;ASSIGNOR:CRUCIBLE MATERIALS CORPORATION, A CORPORATION OF DE;REEL/FRAME:006090/0656

Effective date: 19920413