US2876494A - Process and device for dry spinning - Google Patents
Process and device for dry spinning Download PDFInfo
- Publication number
- US2876494A US2876494A US520329A US52032955A US2876494A US 2876494 A US2876494 A US 2876494A US 520329 A US520329 A US 520329A US 52032955 A US52032955 A US 52032955A US 2876494 A US2876494 A US 2876494A
- Authority
- US
- United States
- Prior art keywords
- spinning
- shaft
- spinneret
- cell
- wall
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000578 dry spinning Methods 0.000 title description 11
- 238000000034 method Methods 0.000 title description 8
- 238000009987 spinning Methods 0.000 description 20
- 210000004027 cell Anatomy 0.000 description 10
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 9
- 210000002421 cell wall Anatomy 0.000 description 6
- 229920002239 polyacrylonitrile Polymers 0.000 description 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 239000011888 foil Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
Images
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16K—VALVES; TAPS; COCKS; ACTUATING-FLOATS; DEVICES FOR VENTING OR AERATING
- F16K31/00—Actuating devices; Operating means; Releasing devices
- F16K31/12—Actuating devices; Operating means; Releasing devices actuated by fluid
- F16K31/36—Actuating devices; Operating means; Releasing devices actuated by fluid in which fluid from the circuit is constantly supplied to the fluid motor
- F16K31/40—Actuating devices; Operating means; Releasing devices actuated by fluid in which fluid from the circuit is constantly supplied to the fluid motor with electrically-actuated member in the discharge of the motor
- F16K31/406—Actuating devices; Operating means; Releasing devices actuated by fluid in which fluid from the circuit is constantly supplied to the fluid motor with electrically-actuated member in the discharge of the motor acting on a piston
- F16K31/408—Actuating devices; Operating means; Releasing devices actuated by fluid in which fluid from the circuit is constantly supplied to the fluid motor with electrically-actuated member in the discharge of the motor acting on a piston the discharge being effected through the piston and being blockable by an electrically-actuated member making contact with the piston
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/04—Dry spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/02—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F6/18—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds from polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide
Definitions
- the spinning shaft is generally provided with a heating jacket through which superheated steam or a heating liquid is passed at a high temperature; this is necessary to maintain the required high temperature in the shaft.
- Fig. 1 is a top view of a bundle of filaments produced by conventional dry spinning methods.
- Fig. 2 is a vertical section of a spinning cell according to the present invention.
- the filaments quietly move through the shaft if the temperature at which the gas arrives at the shaft is 10 to 70 C. and preferably 20 to 40 C. higher than the temperature of the shaft wall in the vicinity of the spinneret.
- the following measures increase the favorable effect of the temperature difference between shaft wall and entering air:
- the hot gas is admitted at the top of the shaft through gauze or a plate or foil with holes.
- the gas is moreover preferably admitted into the space which is separted by the said gauze or plate or foil from the spinning shaft, by means of an annular tube with holes.
- a truncated cone surrounds the spinneret at point adjacent the annular slot so that the additional hot gas stream enters the shaft between shaft wall and cone.
- 1 is the spinning shaft, 2 the heating jacket around the shaft, 5 the filaments bundle and 6 the spinneret.
- the heating medium for the jacket of the spinning shaft enters the heating jacket at 3 and leaves it at 4.
- the heating gas enters the top part of the 2,876,494 @Patented Mar. 10, 1959 2 spinning shaft through an annular tube with holes 7 and reaches the remaining part of the shaft through gauze 8, so-called electrolytic nickel gauze 40 mesh.
- the heating gas is supplied to the shaft by means of the annular slot 9, the gas being guided to this slot 9 through the supply tube 10, the annular channel 11 and the openings 12.
- Conical guide member 14 is connected to channel member 13.
- the invention is elucidated by the following comparative examples.
- Example I (a) A 20% solution of polyacrylonitrile in dimethyl formamide was pressed through a spinneret with 40 holes into a spinning shaft according to Fig. 2, in which air of 200 C. was supplied only through the annular tube 7, the wall of the spinning shaft being maintained at 200 C. The gauze 8 and the guide member 14 were absent. While proceeding in this manner regular spinning appeared to be entirely impossible. Owing to strong fluttering of the thread, thread ruptures occurred repeatedly.
- a dry-spinning process for the conversion of a spinning solution into filaments by extruding the solution through a spinneret into a heated cell having a wall and passing a gaseous evaporative medium through the cell comprising the steps of heating the cell wall, supplying the gaseous medium to the cell from above the spinneret and in an annular stream from the cell wall below the spinneret, the gaseous medium being supplied at a temperature 10 to C. higher than the temperature of the cell wall in the vicinity of the spinneret, and deflecting the annular stream downwardly and away from the spinneret to'merge therebelow with the gaseous medium supplied from above the spinneret.
- a dry-spinning apparatus comprising a spinning cell having a wall, a heating jacket surrounding the wall, a spinneret mounted near one end of the cell, a conduit means for supplying a gaseous evaporative medium to the cell, said conduit means being mounted in the cell between the spinneret and said one end, a bafile member having the form of a truncated cone arranged in the cell between the spinneret and the cell wall, the bafile member and the cell wall defining an annular space therebetween, and second conduit means for supplying gaseous evaporative meduim to the cell, said latter means discharging into the annular space through an annular slot in the cell wall.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Magnetically Actuated Valves (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL331800X | 1954-07-31 |
Publications (1)
Publication Number | Publication Date |
---|---|
US2876494A true US2876494A (en) | 1959-03-10 |
Family
ID=19784397
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US520329A Expired - Lifetime US2876494A (en) | 1954-07-31 | 1955-07-06 | Process and device for dry spinning |
Country Status (7)
Country | Link |
---|---|
US (1) | US2876494A (enrdf_load_stackoverflow) |
BE (1) | BE539482A (enrdf_load_stackoverflow) |
CH (1) | CH331800A (enrdf_load_stackoverflow) |
DE (1) | DE1082001B (enrdf_load_stackoverflow) |
FR (1) | FR1127186A (enrdf_load_stackoverflow) |
GB (1) | GB778194A (enrdf_load_stackoverflow) |
NL (1) | NL96514C (enrdf_load_stackoverflow) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4224269A (en) * | 1977-03-26 | 1980-09-23 | Bayer Aktiengesellschaft | Process for spinning hygroscopic filaments and fibers |
US4257999A (en) * | 1977-08-10 | 1981-03-24 | Bayer Aktiengesellschaft | Process for the production of hydrophilic filaments and fibres by the dry jet wet-spinning method |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB855023A (en) * | 1958-08-09 | 1960-11-30 | British Nylon Spinners Ltd | Improvements in or relating to thread guides for spinning man-made filament yarns |
DE1168725B (de) * | 1960-07-21 | 1964-04-23 | Erich Herion | Durchgangsmagnetventil mit elektromagnetischer Hilfsventilausloesung |
US3462116A (en) * | 1964-02-06 | 1969-08-19 | Wright Components Inc | Solenoid valve and method for making the same |
IT1256966B (it) * | 1992-10-12 | 1995-12-27 | Claudio Margaria | Elettrovalvola perfezionata. |
US5667194A (en) * | 1995-12-11 | 1997-09-16 | Siemens Automotive Corporation | Armature needle valve assembly having plastic connecting means |
CN115747987A (zh) * | 2022-12-24 | 2023-03-07 | 浙江联颖科技有限公司 | 一种全消光异形异收缩涤纶fdy的制备工艺 |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1592006A (en) * | 1925-09-18 | 1926-07-13 | Rhodiaseta | Method of and apparatus for manufacturing artificial filaments |
DE474043C (de) * | 1927-03-03 | 1929-03-25 | Aceta G M B H | Verfahren und Vorrichtung zur Herstellung von Kunstseidenfaeden nach dem Trockenspinnverfahren, bei dem die Trockenluft von unten dem Faserbuendel entgegengefuehrt wird |
US2404714A (en) * | 1942-06-17 | 1946-07-23 | Du Pont | Polymer products |
US2615198A (en) * | 1949-04-06 | 1952-10-28 | Du Pont | Spinning apparatus and method |
US2697251A (en) * | 1951-02-07 | 1954-12-21 | American Viscose Corp | Method and apparatus for manufacturing artificial filaments |
GB731478A (en) * | 1952-04-16 | 1955-06-08 | Celanese Corp | Improvements in the dry-spinning of artificial filamentary materials |
US2763891A (en) * | 1951-11-21 | 1956-09-25 | Celanese Corp | Spinning apparatus |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE508113C (de) * | 1927-06-25 | 1930-09-24 | Aceta G M B H | Vorrichtung zum Spinnen von Kunstfaeden |
BE354193A (enrdf_load_stackoverflow) * | 1927-09-14 | |||
DE506975C (de) * | 1928-03-25 | 1930-09-11 | Ernst Berl Dr | Verfahren zum Trockenspinnen von Kunstseide |
DE611683C (de) * | 1930-01-01 | 1935-04-04 | Aceta G M B H | Verfahren zur Herstellung von Kunstfaeden nach dem Trockenspinnverfahren |
FR741912A (enrdf_load_stackoverflow) * | 1931-09-29 | 1933-02-23 | ||
US2058527A (en) * | 1932-03-12 | 1936-10-27 | Celanese Corp | Process and apparatus for the manufacture of artificial materials |
GB541238A (en) * | 1940-04-17 | 1941-11-19 | Henry Dreyfus | Improvements in or relating to the manufacture of artificial textile materials and the like |
-
0
- BE BE539482D patent/BE539482A/xx unknown
- NL NL96514D patent/NL96514C/xx active
-
1953
- 1953-03-13 GB GB7032/53A patent/GB778194A/en not_active Expired
-
1955
- 1955-06-24 DE DEN10837A patent/DE1082001B/de active Pending
- 1955-07-04 FR FR1127186D patent/FR1127186A/fr not_active Expired
- 1955-07-06 US US520329A patent/US2876494A/en not_active Expired - Lifetime
- 1955-07-07 CH CH331800D patent/CH331800A/de unknown
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1592006A (en) * | 1925-09-18 | 1926-07-13 | Rhodiaseta | Method of and apparatus for manufacturing artificial filaments |
DE474043C (de) * | 1927-03-03 | 1929-03-25 | Aceta G M B H | Verfahren und Vorrichtung zur Herstellung von Kunstseidenfaeden nach dem Trockenspinnverfahren, bei dem die Trockenluft von unten dem Faserbuendel entgegengefuehrt wird |
US2404714A (en) * | 1942-06-17 | 1946-07-23 | Du Pont | Polymer products |
US2615198A (en) * | 1949-04-06 | 1952-10-28 | Du Pont | Spinning apparatus and method |
US2697251A (en) * | 1951-02-07 | 1954-12-21 | American Viscose Corp | Method and apparatus for manufacturing artificial filaments |
US2763891A (en) * | 1951-11-21 | 1956-09-25 | Celanese Corp | Spinning apparatus |
GB731478A (en) * | 1952-04-16 | 1955-06-08 | Celanese Corp | Improvements in the dry-spinning of artificial filamentary materials |
US2763892A (en) * | 1952-04-16 | 1956-09-25 | Celanese Corp | Spinning apparatus |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4224269A (en) * | 1977-03-26 | 1980-09-23 | Bayer Aktiengesellschaft | Process for spinning hygroscopic filaments and fibers |
US4257999A (en) * | 1977-08-10 | 1981-03-24 | Bayer Aktiengesellschaft | Process for the production of hydrophilic filaments and fibres by the dry jet wet-spinning method |
Also Published As
Publication number | Publication date |
---|---|
DE1082001B (de) | 1960-05-19 |
NL96514C (enrdf_load_stackoverflow) | |
FR1127186A (fr) | 1956-12-10 |
BE539482A (enrdf_load_stackoverflow) | |
GB778194A (en) | 1957-07-03 |
CH331800A (de) | 1958-08-15 |
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