US2229077A - Iron plating for shafting - Google Patents
Iron plating for shafting Download PDFInfo
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- US2229077A US2229077A US246644A US24664438A US2229077A US 2229077 A US2229077 A US 2229077A US 246644 A US246644 A US 246644A US 24664438 A US24664438 A US 24664438A US 2229077 A US2229077 A US 2229077A
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- shaft
- plating
- tank
- solution
- shafting
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
- C25D5/34—Pretreatment of metallic surfaces to be electroplated
- C25D5/36—Pretreatment of metallic surfaces to be electroplated of iron or steel
Definitions
- a further object of this invention is to pro- 5 vicle a method of building up worn steel shafting by a practical sufficiently cold process that it cannot develop any heating strains or warping in the shafts, as compared with attempting to accomplish the same result either by weldingor to by hot metal spraying.
- a further object of this invention is to pro vide a method and apparatus for iron plating of shafts which is of general application but is especially useful for plating shafting wherein the 1s shalt may be of substantial size, as for instance, the shaft of a motor.
- armature and which may be applied without the necessity of disassembling the armature from the shaft, even though the assembled armature and shaft may weigh several further object of this invention is to prowide a method and apparatus for plating an iron shaiting wherein the resulting plate will have qualities desirable tor the purpose intended.
- it still further object of this invention is to provide a method and apparatus for keeping the plating solution in proper control and oi a proper purity and for keeping the plE-l (hydrogen ion concentration) of the plating solution under proper control within the maximum and minimum limits necessary to provide a plate having the desired uality.
- the invention consists in the construction, com- 35 blnation and arrangement of parts hereinaiter described and illustrated in the drawing, in which:
- l is a trout elevational, partly lt-ray view oi the plating tank of this invention, with the electrical leads shown diagrammatically.
- liig. 2 is a top plan view ol the. i.
- Fig. 3 is a side elevational view of Fig. 1.
- Fig. i is an edge view of a lalse bottom.
- Fig. 5 is a plan view of the false bottom oi l 'ig. t.
- M d is a'dlagrammatlc elevatlonal view oi the ping tank.
- l is a fragmentary enlarged view of a portion oi the gas outlet ring.
- the plating tank oi this so invention supported on legs it and provided with a removable talse steel bottom it to shield two so watt immersion heaters It placed immedl ately below the false bottom l2, the immersion heaters it being provided with leads N connected m thereto through the side or the tank and leading to a switch control panel l5, through a thermostat control box IE 'on the side of the tank, and through the leads H to a suitable source of electrical current, preferably of 230 volts.
- a tap I8 for draining off the solution when necessary.
- an air pipe l9 leading to a pair of cross pipes 2
- These apertures 22 are graduated in size, being smallest adjacent the points where the cross pipes are joined to the ring 2] and largest at the points furthest from 15 such junction so that the stream of air or other gas used escaping therefrom may be equalized throughout the circumference of the ring.
- a solution level control box On one side of the tank near the top thereof is located a solution level control box it provided so with an overflow pipe it having a control valve it and provided with an inlet pipe it having control valves ll and it.
- a 230 volt motor it may operate a 12 volt direct current generator it for supplying a plating current, a lead ti be- 25 ing connected to the tank lll through its leg it to act as the anode, while another lead it is connected to the Work it whereby the shaft to I being replated acts as the cathode.
- picklingtank it which so is connected to a suitable source of the direct current of 12 volts by means of a lead it to the lead lined wooden pickling tank lit, using the lead lining oi the tank it as the anode,-whi1e.the other lead til is connected to the work it, making the shaft it again the cathode.
- an armmonia dropping tunnel lll consisting of a glass bottle ll suitably supported by a bracket it and having a rubber stopper lli through which exw is then blanked 0d with paper, the windings of the armature are protected with rubber sheet and paper, and the lower part oi the shaft which will necessarily be immersed in the plating solution, but is not to be plated, is sprayed with a prime coat of insulating compound which is not efiected 5 by the plating solution.
- a commercial insulating compound which works very well is on the market as General Electric Glyptal. Cotton tape is wrapped around the primed surface while it is still soft.
- a heavy cellulose lacquer such as Dupont Mt. Ash Scarlet
- a rusting solution composed of 10% hydrochloric acid, 10% alcohol and 80% water is lightly swabbed on and allowed to act over-night.
- the plating is begun by dipping therusted shaft 35 into .the pickling tank 36, making the work the cathode with a minimum current density of about 600 amperes per square foot of area to be plated.
- the area to be plated should come from this pickling with a slightly matted, silvery surface, as left by the rusting solution.
- the pickling solution in the pickling tank 36 consists of sulphuric acid, technical grade. Any carbon deposit on the area to be plated must be scratch-brushed off.
- the shaft is then rinsed and immediately lowered into the plating bath in tank Hi, the work 34 being connected as the cathode to the lead 33, while the the tank i0 is connected as the anode to the lead 32 to the generator 3
- the plating solution consists of technical, crystal, ferrous sulphate in the proportion of 2 to 2 /2 pounds per gallon of water, and ammonium sulphate in the proportion of one pound per gallon when the solution is new, tap water being added to fill the tank to the level 41.
- the preferred current densityused is amperes per square foot of plating area, while the temperature of the solution is kept around Fah. by means of the heaters l3 and the thermostat control box IS. A higher current rate or too low a temperature tends to produce rough metal or whiskers. A lower current area can be used to advantage in slow building up of a film, unusually thick, such as one of 0.100 inch or cover;
- the work 34 is suspended in position by means of a chainfall or crane so that it may be rotated a quarter turn every half hour or so by the operator to equalize any discrepancies in plating rate on different sides. Before the current is turned on the shaft is centered and the air supply from the pipe I9 through the perforated ring 2
- the chemical control of the plating solution is maintained by thirty minute tests of pH, as well as daily analyses of the ferrous sulphate.
- the pH must be kept above 6, preferably from 6 to 6.4, equivalent to a greenish yellow in brom thymol blue, as tested in any standard block comparomoter. may be used.
- the pH can be raised by increasing the rate of addition of ammonia from the dipping funnel 40, the normal rate being one pound of ammonium hydroxide per hour, the stop-cock 46 being adjusted to control the rate as desired.
- the pH- can be lowered by increasing the air flow from the ring 2
- the operator must Watch the temperature to maintain it around 150 Fah., as too low a temperature tends to embrittle the metal. He mus-t also watch the water level, plating current, and adjust the ammonia intake to maintain a steady pH.
- excess over the finished size of at least 0.010 inch should be allowed for machining and the plating should be continued without stopping until the job is finished, except that the shaft can be lifted a few inches near the conclusion of the mm long enough for calipers to be applied to the top of the wet, newly plated surface, allowance being made; of course, for contraction upon cooling.
- the plated metal thus provided on a shaft is suitable for taking ball-bearing assemblies.
- the plated metal has ductility and hardness resembling that of freshly cast unannealed soft steel, and because of its purity resists rust better than soft steel. It has a radial grain at right angles to the plane of wear in the shaft, thereby increasing its resistance to wear in the same way that wooden paving blocks set upright in a floor resist wear better than the same blocks set side ways.
- a tool cut in the lathe removes fine shavings with a tendency to curl, and considerable hammering is required in order to knock the plating loose from the shaft, much more than the shaft would be likely to receive in service.
- a method of restoring full diameter to a shaft comprising thesteps of cutting the worn shaft to an even surface'gof good metal, applying a rusting solution to the shaft and allowing it to remain over night, pickling the shaft in a solution of approximately 30% sulphuric acid with the shaft as the cathode at a minimum current density of about 600 amperes per square foot for from two to four minutes, rinsing the shaft, then making the shaft the cathode in a plating bath of ferrous sulphate and ammonium sulphate with a current density of about 80 amperes per square foot of plating area and a temperature of about 150 Fah., and maintaining the pH at above 6 and not over 6.4, the maintaining of the pH being controlled by adding ammonia and stirring the plating bath by a gas fiow therethrough,the pH being increased by increasing the rate of am monia addition, the pH being decreased by incr'easing the rate of gas flow.
- a method of restoring full diameter to a shaft comprising the steps of cutting the worn iii shaft to an even surface of good metal, applying a rusting solution of one part hydrochloric acid, one part of alcohol and eight parts water and allowing it to remain over night to provide a slightly matted surface, pickling the shaft in a solution of approximately sulphuric acid with the shaft as the cathode at a minimum current density of about 600 amperes per square foot for from two to four minutes, scratch brushing oil.”
- any carbon deposit, rinsing the shaft immediately making the shaft the cathode ina plating bath of ferrous sulphate and ammonium sulphate with a current density of about amperes per square foot of area and a maintained temperature oi not less than Fah., adding ferrous sulphate periodically as needed'to maintain the solution, adding ammonium hydroxide continuously to maintain the ammonium sulphate in the solution, stirring the plating bath by a continuous gas flow therethrough, maintaining the pH
- an apparatus for plating a heavy sha/fting comprising an open tank, a false bottomin said tank, immersion heaters in said tank below said i'alse bottom, a gas outlet ring in said tank above said false bottom, said gas outlet ring having gas outlet openings graduated in size in proportion to their distance from the gas supply, whereby to supply-an evenly dispersed quantity of gas, thermostat control means for maintaining a desired temperature of the solution within said tank, and means for maintaining the solution at'a desired level.
- an apparatus for plating a heavy'shafting comprising an open tank, a false bottom in said tank, immersion heaters in said tank below said false bottom, a gas outlet ring in said tank above said false bottom, said gas outlet ring comprising a hollow gas ring supporting spider, a .gas
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating Methods And Accessories (AREA)
- Electroplating And Plating Baths Therefor (AREA)
Description
atented Jan. 21, 1941 PATENT OFFICE IRON PLATING FOR SHAFTIN G Wesley H. Hammond, Edwin I. Adolphson, and Wai Yun Young, Honolulu, Territory of Hawaii Application December 19, 1938, Serial No. 246,644
Claims. (Cl. 204-25) (Granted under the act of March 3, 1883, as amended April 30, 1928; 370 o. G. 757) This invention relates to a method and apparatus for building up worn steel shafts by electrodeposition of iron.
I A further object of this invention is to pro- 5 vicle a method of building up worn steel shafting by a practical sufficiently cold process that it cannot develop any heating strains or warping in the shafts, as compared with attempting to accomplish the same result either by weldingor to by hot metal spraying.
a further object of this invention is to pro vide a method and apparatus for iron plating of shafts which is of general application but is especially useful for plating shafting wherein the 1s shalt may be of substantial size, as for instance, the shaft of a motor. armature, and which may be applied without the necessity of disassembling the armature from the shaft, even though the assembled armature and shaft may weigh several further object of this invention is to prowide a method and apparatus for plating an iron shaiting wherein the resulting plate will have qualities desirable tor the purpose intended.
25 it still further object of this invention is to provide a method and apparatus for keeping the plating solution in proper control and oi a proper purity and for keeping the plE-l (hydrogen ion concentration) of the plating solution under proper control within the maximum and minimum limits necessary to provide a plate having the desired uality.
With the foregoing and other objects in view, the invention consists in the construction, com- 35 blnation and arrangement of parts hereinaiter described and illustrated in the drawing, in which:
l is a trout elevational, partly lt-ray view oi the plating tank of this invention, with the electrical leads shown diagrammatically.
liig. 2 is a top plan view ol the. i.
Fig. 3 is a side elevational view of Fig. 1.
Fig. i is an edge view of a lalse bottom.
Fig. 5 is a plan view of the false bottom oi l 'ig. t.
M d is a'dlagrammatlc elevatlonal view oi the ping tank.- I
l is a fragmentary enlarged view of a portion oi the gas outlet ring. A
There is shown at it the plating tank oi this so invention supported on legs it and provided with a removable talse steel bottom it to shield two so watt immersion heaters It placed immedl ately below the false bottom l2, the immersion heaters it being provided with leads N connected m thereto through the side or the tank and leading to a switch control panel l5, through a thermostat control box IE 'on the side of the tank, and through the leads H to a suitable source of electrical current, preferably of 230 volts.
Likewise extending through the side of the tank 5 Ill is a tap I8 for draining off the solution when necessary. Also extending through the side'of the tank is an air pipe l9 leading to a pair of cross pipes 2|] at the end of which is supported a perforated preferably non-metallic ring 2i provided with a plurality of air or gas outlet apertures 22 on the top thereof. These apertures 22 are graduated in size, being smallest adjacent the points where the cross pipes are joined to the ring 2] and largest at the points furthest from 15 such junction so that the stream of air or other gas used escaping therefrom may be equalized throughout the circumference of the ring.
On one side of the tank near the top thereof is located a solution level control box it provided so with an overflow pipe it having a control valve it and provided with an inlet pipe it having control valves ll and it. A 230 volt motor it may operate a 12 volt direct current generator it for supplying a plating current, a lead ti be- 25 ing connected to the tank lll through its leg it to act as the anode, while another lead it is connected to the Work it whereby the shaft to I being replated acts as the cathode.
There is also provided a picklingtank it which so is connected to a suitable source of the direct current of 12 volts by means of a lead it to the lead lined wooden pickling tank lit, using the lead lining oi the tank it as the anode,-whi1e.the other lead til is connected to the work it, making the shaft it again the cathode.
.llnother piece of apparatus provided is an armmonia dropping tunnel lll, consisting of a glass bottle ll suitably supported by a bracket it and having a rubber stopper lli through which exw is then blanked 0d with paper, the windings of the armature are protected with rubber sheet and paper, and the lower part oi the shaft which will necessarily be immersed in the plating solution, but is not to be plated, is sprayed with a prime coat of insulating compound which is not efiected 5 by the plating solution. A commercial insulating compound which works very well is on the market as General Electric Glyptal. Cotton tape is wrapped around the primed surface while it is still soft. As soon as the primed surface is dry, a heavy cellulose lacquer, such as Dupont Mt. Ash Scarlet," is then sprayed on, extreme care being taken that all corners and projections are properly covered. After the lacquer is dry the paper is removed from the area to be plated and a rusting solution composed of 10% hydrochloric acid, 10% alcohol and 80% water is lightly swabbed on and allowed to act over-night.
In the morning the plating is begun by dipping therusted shaft 35 into .the pickling tank 36, making the work the cathode with a minimum current density of about 600 amperes per square foot of area to be plated. The area to be plated should come from this pickling with a slightly matted, silvery surface, as left by the rusting solution. The pickling solution in the pickling tank 36 consists of sulphuric acid, technical grade. Any carbon deposit on the area to be plated must be scratch-brushed off. The shaft is then rinsed and immediately lowered into the plating bath in tank Hi, the work 34 being connected as the cathode to the lead 33, while the the tank i0 is connected as the anode to the lead 32 to the generator 3| supplying 12 volt direct current.
The plating solution consists of technical, crystal, ferrous sulphate in the proportion of 2 to 2 /2 pounds per gallon of water, and ammonium sulphate in the proportion of one pound per gallon when the solution is new, tap water being added to fill the tank to the level 41. The preferred current densityused is amperes per square foot of plating area, while the temperature of the solution is kept around Fah. by means of the heaters l3 and the thermostat control box IS. A higher current rate or too low a temperature tends to produce rough metal or whiskers. A lower current area can be used to advantage in slow building up of a film, unusually thick, such as one of 0.100 inch or cover;
The work 34 is suspended in position by means of a chainfall or crane so that it may be rotated a quarter turn every half hour or so by the operator to equalize any discrepancies in plating rate on different sides. Before the current is turned on the shaft is centered and the air supply from the pipe I9 through the perforated ring 2| is adjusted to give a turbulent flow over the entire surface of the area to be plated.
The chemical control of the plating solution is maintained by thirty minute tests of pH, as well as daily analyses of the ferrous sulphate. The pH must be kept above 6, preferably from 6 to 6.4, equivalent to a greenish yellow in brom thymol blue, as tested in any standard block comparomoter. may be used. The pH can be raised by increasing the rate of addition of ammonia from the dipping funnel 40, the normal rate being one pound of ammonium hydroxide per hour, the stop-cock 46 being adjusted to control the rate as desired. The pH- can be lowered by increasing the air flow from the ring 2|.
The operator must Watch the temperature to maintain it around 150 Fah., as too low a temperature tends to embrittle the metal. He mus-t also watch the water level, plating current, and adjust the ammonia intake to maintain a steady pH.
The build-up of metalon the shaft 34 will ap- Any other means of measuring pH proximate 0.002 to 0.003 inch per hour on the radius or twice that on the diameter. A 12 hour run should build up 0.060 inch on the diameter of the thinnest spot, making full allowances. An
excess over the finished size of at least 0.010 inch should be allowed for machining and the plating should be continued without stopping until the job is finished, except that the shaft can be lifted a few inches near the conclusion of the mm long enough for calipers to be applied to the top of the wet, newly plated surface, allowance being made; of course, for contraction upon cooling.
After one end of the shaft is finished in this way the other end of the shaft may be similarly treated. The finished shaft is then placed into a lathe and turned to exact size. The plated metal thus provided on a shaft is suitable for taking ball-bearing assemblies. The plated metal has ductility and hardness resembling that of freshly cast unannealed soft steel, and because of its purity resists rust better than soft steel. It has a radial grain at right angles to the plane of wear in the shaft, thereby increasing its resistance to wear in the same way that wooden paving blocks set upright in a floor resist wear better than the same blocks set side ways. A tool cut in the lathe removes fine shavings with a tendency to curl, and considerable hammering is required in order to knock the plating loose from the shaft, much more than the shaft would be likely to receive in service.
As the plating is carried on the ammonium sulphate concentration gradually increases, while the ferrous sulphate content gradually decreases by loss to the cathode and by oxidation by air and must be renewed at the approximate rate of 40 pounds for every 12 hour run. The sludge thus created drops through the solution through the holes 29 in the false bottom l2 to the bottom of tank l0, whence it may be removed from time to time.
Other modifications and changes in the proportions and arrangements of the parts may be made by those skilled in the art without departing from the nature of the invention, within the scope of what is hereinafter claimed.
The invention described herein may be manufactured and/or used by or for the Government of the United States of .America for governmental purposes without the payment of any royalties thereon or therefor.
Having thus set forth and disclosed the nature of this invention, what is claimed is:
l. A method of restoring full diameter to a shaft comprising thesteps of cutting the worn shaft to an even surface'gof good metal, applying a rusting solution to the shaft and allowing it to remain over night, pickling the shaft in a solution of approximately 30% sulphuric acid with the shaft as the cathode at a minimum current density of about 600 amperes per square foot for from two to four minutes, rinsing the shaft, then making the shaft the cathode in a plating bath of ferrous sulphate and ammonium sulphate with a current density of about 80 amperes per square foot of plating area and a temperature of about 150 Fah., and maintaining the pH at above 6 and not over 6.4, the maintaining of the pH being controlled by adding ammonia and stirring the plating bath by a gas fiow therethrough,the pH being increased by increasing the rate of am monia addition, the pH being decreased by incr'easing the rate of gas flow.
2. A method of restoring full diameter to a shaft comprising the steps of cutting the worn iii shaft to an even surface of good metal, applying a rusting solution of one part hydrochloric acid, one part of alcohol and eight parts water and allowing it to remain over night to provide a slightly matted surface, pickling the shaft in a solution of approximately sulphuric acid with the shaft as the cathode at a minimum current density of about 600 amperes per square foot for from two to four minutes, scratch brushing oil." any carbon deposit, rinsing the shaft, immediately making the shaft the cathode ina plating bath of ferrous sulphate and ammonium sulphate with a current density of about amperes per square foot of area and a maintained temperature oi not less than Fah., adding ferrous sulphate periodically as needed'to maintain the solution, adding ammonium hydroxide continuously to maintain the ammonium sulphate in the solution, stirring the plating bath by a continuous gas flow therethrough, maintaining the pH at above 6 and not over 6.4 by increasing the rate of ammonium hydroxide addition to increase the pH, and increasing the rate of gas flow to decrease the pH. 2d
3. in a method of restoring full diameter to a shaft comprising the steps of preparing the worm shaft for the plating operation which comprises making the shaft the cathode in aplating bath of ferrous sulphate and ammonium sulphate with a current density of about 80 amperes per square foot oi area and a maintained temperature of not less than 150 Fair, adding ferrous sulphate periodically as needed to maintain the solution,
adding ammonium hydroxide continuously to maintain the ammonium sulphate in the solution, stirring the plating bath by a continuous gas flow therethrough, maintaining the pH at above 6 and not over 6.4 by increasing the rate of ammonium hydroxide additionto increase the'pH, andincreasing the rate of gas flow to decrease the pH.
4. In an apparatus for plating a heavy sha/fting comprising an open tank, a false bottomin said tank, immersion heaters in said tank below said i'alse bottom, a gas outlet ring in said tank above said false bottom, said gas outlet ring having gas outlet openings graduated in size in proportion to their distance from the gas supply, whereby to supply-an evenly dispersed quantity of gas, thermostat control means for maintaining a desired temperature of the solution within said tank, and means for maintaining the solution at'a desired level.
5. In an apparatus for plating a heavy'shafting comprising an open tank, a false bottom in said tank, immersion heaters in said tank below said false bottom, a gas outlet ring in said tank above said false bottom, said gas outlet ring comprising a hollow gas ring supporting spider, a .gas
- feeding arm supporting said spider, and a gas dis- WESLEY n. HAMMOND. EDWIN r. ADOLPHSON. WAI YUN YOUNG.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US246644A US2229077A (en) | 1938-12-19 | 1938-12-19 | Iron plating for shafting |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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US246644A US2229077A (en) | 1938-12-19 | 1938-12-19 | Iron plating for shafting |
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US2229077A true US2229077A (en) | 1941-01-21 |
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US246644A Expired - Lifetime US2229077A (en) | 1938-12-19 | 1938-12-19 | Iron plating for shafting |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2465747A (en) * | 1945-04-30 | 1949-03-29 | Rca Corp | Apparatus for electroplating metal |
US2626895A (en) * | 1944-11-17 | 1953-01-27 | Fansteel Metallurgical Corp | Electrolytic production of iron |
US3051632A (en) * | 1959-07-27 | 1962-08-28 | William D Kraemer | Method of electroplating copper elbows |
-
1938
- 1938-12-19 US US246644A patent/US2229077A/en not_active Expired - Lifetime
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2626895A (en) * | 1944-11-17 | 1953-01-27 | Fansteel Metallurgical Corp | Electrolytic production of iron |
US2465747A (en) * | 1945-04-30 | 1949-03-29 | Rca Corp | Apparatus for electroplating metal |
US3051632A (en) * | 1959-07-27 | 1962-08-28 | William D Kraemer | Method of electroplating copper elbows |
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