US20040030004A1 - Intumescent electrical installation systems and processes for their production - Google Patents
Intumescent electrical installation systems and processes for their production Download PDFInfo
- Publication number
- US20040030004A1 US20040030004A1 US10/389,777 US38977703A US2004030004A1 US 20040030004 A1 US20040030004 A1 US 20040030004A1 US 38977703 A US38977703 A US 38977703A US 2004030004 A1 US2004030004 A1 US 2004030004A1
- Authority
- US
- United States
- Prior art keywords
- intumescent
- electrical installation
- installation system
- injection molding
- ethylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
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Classifications
-
- H—ELECTRICITY
- H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
- H02G—INSTALLATION OF ELECTRIC CABLES OR LINES, OR OF COMBINED OPTICAL AND ELECTRIC CABLES OR LINES
- H02G3/00—Installations of electric cables or lines or protective tubing therefor in or on buildings, equivalent structures or vehicles
- H02G3/02—Details
- H02G3/04—Protective tubing or conduits, e.g. cable ladders or cable troughs
- H02G3/0406—Details thereof
- H02G3/0412—Heat or fire protective means
Definitions
- Electrical installation systems such as, for example, conduit boxes, junction boxes, switch boxes, armored boxes, conduits, etc.
- materials are produced from a very wide range of materials, depending on the intended use.
- Materials used to date are steel sheet, aluminum, cast iron, (polyvinyl chloride (PVC), polyphenylene ether/polyphenylene oxide (PPE/PPO), polycarbonate (PC), polystyrene (PS), polypropylene (PP), polyethylene (PE), ABS or polyamide (PA).
- PVC polyvinyl chloride
- PPE/PPO polyphenylene ether/polyphenylene oxide
- PC polycarbonate
- PS polystyrene
- PP polypropylene
- PE polyethylene
- ABS or polyamide PA
- flame retardance for electrical installation systems according to VDE 0471/DIN IEC 695 Part 2-1 are applicable: flame retardance for electrical installation systems for flush mounting and in concrete construction must be 650°, that for covers and lids must be 750° C., that for installation systems for mounting cavity walls must be 850° C. and that for terminals and semiflush-mounted conduit boxes for riser cables having 1.5 and 2.5 mm 2 copper conductors must be 960° C.
- the installation systems protected in this manner may not exceed the temperature of 181° C. in a fire test according to ASTM E-119.
- this object can be achieved by intumescent, electrical installation systems which are produced by the injection molding process from polyolefins or polyimides in combination with intumescent additives.
- the invention accordingly relates to intumescent, electrical installation systems which comprise an injection molding material of polyolefins or polyimides in combination with intumescent additives, the melting points of the polyolefins and of the polyimides being lower than the intumescence temperature of the intumescent additives.
- Electrical installation systems are to be understood as meaning, surface-mounted sockets and boxes, such as, for example, conduit boxes and armored boxes, flush-mounted sockets and boxes, such as, for example, equipment boxes or switch boxes and conduit boxes, and junction boxes, cavity wall sockets and boxes and installation systems for concrete construction.
- the abovementioned installation systems may be in the form of conduits, angle boxes, branch-Ts, cross boxes, a combination conduit box/switch box, a double conduit box/switch box, a semiflush-mounted conduit box, a ceiling light connection box, a wall light connection box, a dome box, a double equipment or switch box, a triple equipment box, an equipment conduit box, a junction box/switch box, a transition box, a universal box, etc.
- the intumescent, electrical installation systems according to the invention comprise an injection molding material of polyolefins or polyimides in combination with intumescent additives.
- Polyolefins used may be thermoplastic polyolefins, such as polyethylene (PE) having a low density (LDPE) to high density (HDPE), preferably HDPE, ethylene-vinyl acetate (EVA) copolymers, ethylene-butyl acrylate copolymers, polypropylene, poly-1-butene poly(methyl-pentene), copolymers of ethylene and octene, ethylene/propylene-diene terpolymers (EPDM) or blends thereof.
- PE polyethylene
- LDPE low density
- HDPE high density
- EVA ethylene-vinyl acetate copolymers
- EVA ethylene-butyl acrylate copolymers
- polypropylene poly-1-butene poly(methyl-pentene)
- EPDM ethylene/propylene-diene terpolymers
- HDPE, EVA copolymers or copolymers of ethylene and octene or blends of HDPE and EVA copolymer are preferably used.
- Suitable polyimides are those which are present as a low-melting precursor and form highly crosslinked products, such as, for example, bismaleimides by addition reaction under the action of heat.
- Bismaleimides which consist of diphenylmethane 4 , 4 ′-bismaleimide and methylenedianiline or other aromatic diamines are preferably used.
- the bismaleimides used should have a melting point below about 200° C.
- Suitable intumescent additives are ammonium or amino compounds, such as, for example, ammonium polyphosphate, ammonium dihydrogen phosphate, ethylenediamine phosphate, ammonium pentaborate, melamine, dicyandiamide, full phosphoric esters with polyols, dipentaerythritol, pentaerythritol, sugar, dextran, starch, vermicular graphite, waterglass, expanded mica, vermiculite, perlite and mixtures thereof.
- Preferred intumescent additives are ammonium polyphosphate, ethylenediamine phosphate, melamine, dipentaerythritol, pentaerythritol, sodium silicate or vermicular graphite or mixtures thereof.
- Vermicular graphite is particularly preferably used as an intumescent additive in the case of polyimides, and ethylenediamine phosphate and/or ammonium polyphosphate and/or melamine and/or dipentaerythritol and/or vermicular graphite in the case of polyolefins.
- the melting points of the polyolefins and of the polyimides are lower than the intumescence temperature of the intumescent additives.
- the injection molding material according to the invention contains from 20 to 50% by weight, preferably from 30 to 40% by weight, of polyolefin or polyimide and from 50 to 80% by weight, preferably from 60 to 70% by weight, of intumescent additives.
- the injection molding material according to the invention can optionally also contain inorganic fillers, such as, for example, kaolin, clays, mica, wollastonite, calcium silicates, titanium dioxide, zinc borate, quartz, zinc oxide, apatite, talc, aluminum phosphates, ATH, Mg(OH) 2 , chalk, glass fibers, mineral fibers, etc.
- inorganic fillers such as, for example, kaolin, clays, mica, wollastonite, calcium silicates, titanium dioxide, zinc borate, quartz, zinc oxide, apatite, talc, aluminum phosphates, ATH, Mg(OH) 2 , chalk, glass fibers, mineral fibers, etc.
- Preferred inorganic fillers are clays, mica and glass fibers.
- clays or mica are used as inorganic fillers, it is preferable for them to be present as nanoparticles in the mixture of polymer, intumescent additive and filler.
- the amount of added filler may be from 0 to 20% by weight, based on the total injection molding material.
- the injection molding materials according to the invention may also contain conventional dispersants, such as, for example, zinc stearate or calcium stearate, glyceryl stearate, pentaerythrityl tetrastearate, cetyl palmitate, ethylenedistearoyldiamide C 14 -C 18 fatty alcohols, dicarboxylic esters, fatty amines, paraffins, etc., in an amount of from 0 to 5% by weight.
- conventional dispersants such as, for example, zinc stearate or calcium stearate, glyceryl stearate, pentaerythrityl tetrastearate, cetyl palmitate, ethylenedistearoyldiamide C 14 -C 18 fatty alcohols, dicarboxylic esters, fatty amines, paraffins, etc.
- a powder mixture or granules of the desired components is or are prepared by simple mixing together or by extrusion.
- the intumescent electrical installation system according to the invention is shaped in only one operation in the injection molding process and optionally postcured.
- the parameters such as, for example, temperature, injection pressure and locking force, depend on the respective starting mixture.
- the material thickness is such that it corresponds to the box volume divided by the product of twice the lateral surface area and the maximum expansion factor, so that the installation system is completely filled with foam by intumescence.
- This condition can be represented as a formula as follows:
- V . . . Volume of the installation system (socket, distributor box, etc.)
- Kf . . . Compression factor ratio of max. expansion factor to actual expansion factor
- a compression factor of 2 should preferably be present.
- the intumescent electrical installation systems according to the invention have several advantages over installation systems available to date.
- the injection molding material contains no halogens, so that no corrosive gases can form in the event of a fire.
- the installation systems according to the invention provide a fume-tight seal owing to the intumescent additives, so that additional fire protection measures, such as intumescent inlays or cements, are no longer required.
- connection box 100 having the dimensions 107 ⁇ 107 ⁇ 57 mm and comprising high-impact polystyrene was mounted in a corresponding recess in a 100 mm Ytong wall so that the cover of the connection box is flush with the Ytong surface.
- a thermocouple was fastened centrally on the back.
- the box had melted after 30 minutes and a temperature of 700° C. was measured at the thermocouple after 2 hours.
- [0046] having the dimensions of 4 mm diameter and 4 mm length were produced on a K 30 twin-screw extruder from Werner & Pfleiderer.
- the extrusion temperature was 150° C. and the throughput was 10 kg/h.
- connection box 100 having the dimensions 107 ⁇ 107 ⁇ 57 mm was injection molded on an FM 60 injection molding machine from Klöckner Ferromatik.
- the temperature in the heating zone was 150-160° C. and that in the mold was 40-60° C.
- the injection pressure was 10 bar.
- connection box having a mean material thickness of 2.5 mm was closed by means of a steel sheet cover. This arrangement was mounted in a corresponding Ytong wall recess. The side with the steel sheet cover was installed facing the fire in the furnace.
- thermocouple for temperature measurement was mounted on the back of the connection box. In the course of the fire test, the connection box became completely filled with foam. The temperature on the back panel after 2 hours was 300° C.
- Test specimens were produced from another connection box and the mechanical properties in the tensile strength test according to DIN 53 455 and the expansion factor at 300° C. and in the course of 30 minutes were determined. The values are shown in table 1.
- a round connection socket having the dimensions 70 mm diameter and 36 mm height were injection molded from the same granules and likewise mounted in a 100 mm thick Ytong wall in a corresponding circular recess, closed with a steel sheet cover and tested in the furnace. After 2 hours, the back panel reached a temperature of 320° C.
- a powder mixture comprising
- connection box was injection molded on a conventional injection molding machine for heat-curable plastics, having an L/D ratio of 15 and a compressionless screw with a pitch of 0.8, at a screw speed of 40 rpm.
- the temperatures were 50-60° C. in the feed zone, 50-60° C. in the compression zone, 100-110° C. in the discharge zone and 230° C. in the mold.
- the injection pressure was 600 bar.
- a US distributor box having the dimensions 100 ⁇ 100 ⁇ 50 mm was likewise injection molded in order to be able to subject it to the UL test according to the setup of FIGS. 1 and 2. 180° C. was not exceeded in the course of 2 hours. To ensure that the material intumesces only in an inward direction, a glass fabric tape is placed around the box.
- a powder mixture comprising
- a powder mixture comprising
- the wall thickness was once again 2.5 mm. In the fire test of tab. 2, once again complete foam-filling of the box was observed. The back panel temperature after 2 hours was 280° C.
- Granules were produced from a mixture of
- Granules having the following composition were produced by means of extrusion:
- the extrusion temperature was 200° C.
- round connection sockets having a diameter of 70 mm and a height of 35 mm were injection molded at 90° C.
Landscapes
- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Injection Moulding Of Plastics Or The Like (AREA)
- Organic Insulating Materials (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/312,372 US7521495B2 (en) | 2002-03-19 | 2005-12-21 | Intumescent electrical installation systems and processes for their production |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ATA410/2002 | 2002-03-19 | ||
AT0041002A AT411261B (de) | 2002-03-19 | 2002-03-19 | Intumeszierende elektrische installationssysteme enthaltend eine kombination aus polyimiden und vermikulargraphit und zu deren herstellung |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US11/312,372 Division US7521495B2 (en) | 2002-03-19 | 2005-12-21 | Intumescent electrical installation systems and processes for their production |
Publications (1)
Publication Number | Publication Date |
---|---|
US20040030004A1 true US20040030004A1 (en) | 2004-02-12 |
Family
ID=3673736
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/389,777 Abandoned US20040030004A1 (en) | 2002-03-19 | 2003-03-18 | Intumescent electrical installation systems and processes for their production |
US11/312,372 Expired - Lifetime US7521495B2 (en) | 2002-03-19 | 2005-12-21 | Intumescent electrical installation systems and processes for their production |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US11/312,372 Expired - Lifetime US7521495B2 (en) | 2002-03-19 | 2005-12-21 | Intumescent electrical installation systems and processes for their production |
Country Status (5)
Country | Link |
---|---|
US (2) | US20040030004A1 (de) |
EP (1) | EP1347549B1 (de) |
AT (1) | AT411261B (de) |
AU (1) | AU2003201367B2 (de) |
CA (1) | CA2419759C (de) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20060019102A1 (en) * | 2004-07-26 | 2006-01-26 | Kuppsuamy Kanakarajan | Flame-retardant halogen-free polyimide films useful as thermal insulation in aircraft applications and methods relating thereto |
US20100029826A1 (en) * | 2008-07-30 | 2010-02-04 | Krizan Timothy D | Polyimide resins for high temperature wear applications |
US20130068487A1 (en) * | 2011-09-19 | 2013-03-21 | Hilti Aktiengesellschaft | Fire protection element |
US10415725B2 (en) | 2015-04-27 | 2019-09-17 | Hilti Aktiengesellschaft | Fire protection sleeve |
GB2588670A (en) * | 2019-11-01 | 2021-05-05 | Fire And Sound Solutions Group Ltd | Electrical back box |
GB2584442B (en) * | 2019-06-03 | 2022-03-02 | Vexbox Ltd | A fire-proof extension for an electrical back box |
Families Citing this family (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT500875A1 (de) * | 2004-07-23 | 2006-04-15 | Intumex Gmbh | Intumeszierende klippprofile für brandschutzeinrichtungen |
DE202010017200U1 (de) | 2009-07-09 | 2011-04-21 | Kaiser Gmbh & Co. Kommanditgesellschaft | Anordnung zur rauchgasdichten Durchführung eines Langformteils durch eine Wand |
DE102009032460A1 (de) | 2009-07-09 | 2011-01-13 | Kaiser Gmbh & Co. Kommanditgesellschaft | Anordnung zur rauchgasdichten Durchführung eines Langformteils durch eine Brandschutzwand |
US8648256B1 (en) * | 2010-06-07 | 2014-02-11 | Intumescent Technologies, Llc | Intumescent swell devices |
CN103154139B (zh) * | 2010-09-29 | 2016-09-07 | 纳幕尔杜邦公司 | 用于高温应用的聚酰亚胺树脂 |
CN103124772A (zh) * | 2010-09-29 | 2013-05-29 | 纳幕尔杜邦公司 | 高温应用的聚酰亚胺树脂 |
DE102011004575A1 (de) | 2011-02-23 | 2012-08-23 | Hilti Aktiengesellschaft | Leitungselementdurchführung |
DE102011007654B4 (de) * | 2011-04-19 | 2012-12-06 | Hilti Aktiengesellschaft | Komprimierbares Weichschott, Verfahren zu seiner Herstellung und seine Verwendung |
DE102011089531A1 (de) | 2011-12-22 | 2013-06-27 | Hilti Aktiengesellschaft | Brandschutzmanschette |
WO2014005880A1 (de) | 2012-07-03 | 2014-01-09 | Hilti Aktiengesellschaft | Form und verfahren zur herstellung eines formteils sowie formteil |
DE102012218540A1 (de) | 2012-10-11 | 2014-06-12 | Hilti Aktiengesellschaft | Brandschutzmanschette |
DE102013200546A1 (de) | 2013-01-16 | 2014-07-17 | Hilti Aktiengesellschaft | Akkumulator für eine Handwerkzeugmaschine und Verfahren zum Herstellen eines Akkumulators für eine Handwerkzeugmaschine |
EP2821207A1 (de) | 2013-07-03 | 2015-01-07 | HILTI Aktiengesellschaft | Verfahren und Spritzgiessanlage zur Herstellung von intumeszierenden Reaktionskunststoffformteilen und Reaktionskunststoffformteil |
EP2821108A1 (de) | 2013-07-03 | 2015-01-07 | HILTI Aktiengesellschaft | Intumeszierende Brandschutzeinlage und Baugruppe mit intumeszierender Brandschutzeinlage |
EP2827465A1 (de) | 2013-07-17 | 2015-01-21 | HILTI Aktiengesellschaft | Leitungsdurchführung, Verfahren zur Herstellung einer Leitungsdurchführung und Verfahren zur Montage einer Leitungsdurchführung |
EP2826612A1 (de) | 2013-07-17 | 2015-01-21 | HILTI Aktiengesellschaft | Schäumwerkzeug zur Herstellung eines Profilstranges, Verfahren zur Herstellung eines Profilstranges sowie Profilstrang |
EP2826611A1 (de) | 2013-07-18 | 2015-01-21 | HILTI Aktiengesellschaft | Verfahren zur Herstellung von Schaumformteilen in einer Verpackungshülle und Verkaufseinheit |
EP2827041A1 (de) | 2013-07-18 | 2015-01-21 | HILTI Aktiengesellschaft | Isoliermaterial sowie Isolierung für ein Rohr im Bereich einer Wand- oder Deckendurchführung |
DE102013214499A1 (de) * | 2013-07-24 | 2014-07-17 | E.G.O. Elektro-Gerätebau GmbH | Gehäusevorrichtung, Anordnung einer Gehäusevorrichtung und Verfahren zur Montage einer Gehäusevorrichtung |
US20150218403A1 (en) * | 2014-02-03 | 2015-08-06 | 3M Innovative Properties Company | Intumescent caulking compositions and methods |
EP3088785A1 (de) | 2015-04-27 | 2016-11-02 | Hilti Aktiengesellschaft | Brandschutzmanschette |
EP3088784A1 (de) | 2015-04-27 | 2016-11-02 | Hilti Aktiengesellschaft | Brandschutzmanschette |
US20170030490A1 (en) | 2015-07-28 | 2017-02-02 | Hilti Aktiengesellschaft | Air, acoustic and/or fire sealing sleeve insert and air, acoustic and/or fire sealing device |
US10145494B2 (en) | 2016-11-18 | 2018-12-04 | Hilti Aktiengesellschaft | Air, acoustic and/or fire sealing device |
DE102020212619A1 (de) | 2020-10-06 | 2022-04-07 | Siemens Aktiengesellschaft | Faser-Matrix-Halbzeug für die Herstellung von Gehäuseteilen von Leistungsschutzschaltern |
Citations (6)
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US5998503A (en) * | 1996-08-29 | 1999-12-07 | E. I. Du Pont De Nemours And Company | Polymer flame retardant |
US6031040A (en) * | 1997-05-21 | 2000-02-29 | Dsm Fine Chemicals Austria Gmbh | Intumescent sealing and cover profiles |
US6521834B1 (en) * | 2000-08-25 | 2003-02-18 | 3M Innovative Properties Company | Fire stopping cover plate for fire stopping electrical outlets and switches |
US6706793B2 (en) * | 2002-01-23 | 2004-03-16 | Delphi Technologies, Inc. | Intumescent fire retardant composition and method of manufacture thereof |
US6747074B1 (en) * | 1999-03-26 | 2004-06-08 | 3M Innovative Properties Company | Intumescent fire sealing composition |
US6809129B2 (en) * | 2002-01-23 | 2004-10-26 | Delphi Technologies, Inc. | Elastomeric intumescent material |
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US4543281A (en) * | 1982-05-07 | 1985-09-24 | A/S Norsk Kabelfabrik | Fire or flame barrier material |
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DE19603424A1 (de) * | 1996-01-31 | 1997-08-07 | Friedhelm Schneider | Formteile aus intumeszierenden Mischungen und Verfahren zur Herstellung derselben |
JPH11217508A (ja) * | 1998-02-02 | 1999-08-10 | Mitsui Chem Inc | 難燃性熱可塑性樹脂組成物 |
DE19844772A1 (de) * | 1998-09-30 | 2000-04-06 | Friedhelm Schneider | Formteile aus intumeszierenden Mischungen und Verfahren zur Herstellung derselben |
AT409045B (de) * | 1999-02-03 | 2002-05-27 | Dsm Fine Chem Austria Gmbh | Halogenfreie intumeszierende ummantelung von drähten und lichtkabeln |
CN1091296C (zh) * | 1999-12-24 | 2002-09-18 | 中国科学院上海原子核研究所 | 辐射交联低烟无卤阻燃热收缩电力电缆附件 |
-
2002
- 2002-03-19 AT AT0041002A patent/AT411261B/de not_active IP Right Cessation
-
2003
- 2003-02-24 CA CA2419759A patent/CA2419759C/en not_active Expired - Lifetime
- 2003-02-24 EP EP03004010.9A patent/EP1347549B1/de not_active Expired - Lifetime
- 2003-03-18 US US10/389,777 patent/US20040030004A1/en not_active Abandoned
- 2003-03-19 AU AU2003201367A patent/AU2003201367B2/en not_active Ceased
-
2005
- 2005-12-21 US US11/312,372 patent/US7521495B2/en not_active Expired - Lifetime
Patent Citations (6)
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US5998503A (en) * | 1996-08-29 | 1999-12-07 | E. I. Du Pont De Nemours And Company | Polymer flame retardant |
US6031040A (en) * | 1997-05-21 | 2000-02-29 | Dsm Fine Chemicals Austria Gmbh | Intumescent sealing and cover profiles |
US6747074B1 (en) * | 1999-03-26 | 2004-06-08 | 3M Innovative Properties Company | Intumescent fire sealing composition |
US6521834B1 (en) * | 2000-08-25 | 2003-02-18 | 3M Innovative Properties Company | Fire stopping cover plate for fire stopping electrical outlets and switches |
US6706793B2 (en) * | 2002-01-23 | 2004-03-16 | Delphi Technologies, Inc. | Intumescent fire retardant composition and method of manufacture thereof |
US6809129B2 (en) * | 2002-01-23 | 2004-10-26 | Delphi Technologies, Inc. | Elastomeric intumescent material |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20060019102A1 (en) * | 2004-07-26 | 2006-01-26 | Kuppsuamy Kanakarajan | Flame-retardant halogen-free polyimide films useful as thermal insulation in aircraft applications and methods relating thereto |
US20100029826A1 (en) * | 2008-07-30 | 2010-02-04 | Krizan Timothy D | Polyimide resins for high temperature wear applications |
US7858687B2 (en) | 2008-07-30 | 2010-12-28 | E.I. Du Pont De Nemours And Company | Polyimide resins for high temperature wear applications |
US20130068487A1 (en) * | 2011-09-19 | 2013-03-21 | Hilti Aktiengesellschaft | Fire protection element |
US10415725B2 (en) | 2015-04-27 | 2019-09-17 | Hilti Aktiengesellschaft | Fire protection sleeve |
US10641417B2 (en) | 2015-04-27 | 2020-05-05 | Hilti Aktiengesellschaft | Fire protection sleeve |
US11137091B2 (en) | 2015-04-27 | 2021-10-05 | Hilti Aktiengesellschaft | Fire protection sleeve |
US11655919B2 (en) | 2015-04-27 | 2023-05-23 | Hilti Aktiengesellschaft | Fire protection sleeve |
GB2584442B (en) * | 2019-06-03 | 2022-03-02 | Vexbox Ltd | A fire-proof extension for an electrical back box |
GB2588670A (en) * | 2019-11-01 | 2021-05-05 | Fire And Sound Solutions Group Ltd | Electrical back box |
GB2588670B (en) * | 2019-11-01 | 2024-05-15 | Fire And Sound Solutions Group Ltd | Electrical back box |
Also Published As
Publication number | Publication date |
---|---|
US7521495B2 (en) | 2009-04-21 |
ATA4102002A (de) | 2003-04-15 |
CA2419759A1 (en) | 2003-09-19 |
EP1347549A1 (de) | 2003-09-24 |
AU2003201367A1 (en) | 2003-10-09 |
AT411261B (de) | 2003-11-25 |
AU2003201367B2 (en) | 2009-01-08 |
US20060160926A1 (en) | 2006-07-20 |
CA2419759C (en) | 2012-04-17 |
EP1347549B1 (de) | 2017-03-29 |
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