US1881745A - Process of bleaching, dyeing, and printing vegetable and animal fiber material, fabrics, or felt - Google Patents
Process of bleaching, dyeing, and printing vegetable and animal fiber material, fabrics, or felt Download PDFInfo
- Publication number
- US1881745A US1881745A US81311A US8131126A US1881745A US 1881745 A US1881745 A US 1881745A US 81311 A US81311 A US 81311A US 8131126 A US8131126 A US 8131126A US 1881745 A US1881745 A US 1881745A
- Authority
- US
- United States
- Prior art keywords
- bleaching
- dyeing
- fiber material
- felt
- fabrics
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004061 bleaching Methods 0.000 title description 35
- 239000002657 fibrous material Substances 0.000 title description 23
- 238000000034 method Methods 0.000 title description 20
- 238000004043 dyeing Methods 0.000 title description 14
- 239000004744 fabric Substances 0.000 title description 4
- 235000013311 vegetables Nutrition 0.000 title description 3
- 241001465754 Metazoa Species 0.000 title description 2
- 238000007639 printing Methods 0.000 title description 2
- 150000003839 salts Chemical class 0.000 description 12
- 239000002253 acid Substances 0.000 description 11
- 239000000243 solution Substances 0.000 description 9
- 239000000344 soap Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- 239000004571 lime Substances 0.000 description 6
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 5
- 235000011941 Tilia x europaea Nutrition 0.000 description 5
- 150000007513 acids Chemical class 0.000 description 5
- 238000007792 addition Methods 0.000 description 5
- 238000009835 boiling Methods 0.000 description 5
- 235000019441 ethanol Nutrition 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 239000000080 wetting agent Substances 0.000 description 5
- RGCKGOZRHPZPFP-UHFFFAOYSA-N alizarin Chemical compound C1=CC=C2C(=O)C3=C(O)C(O)=CC=C3C(=O)C2=C1 RGCKGOZRHPZPFP-UHFFFAOYSA-N 0.000 description 4
- 229910052783 alkali metal Inorganic materials 0.000 description 4
- -1 aromatic sulpho acids Chemical class 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 4
- 239000000975 dye Substances 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 150000001340 alkali metals Chemical class 0.000 description 3
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000007844 bleaching agent Substances 0.000 description 3
- 150000001805 chlorine compounds Chemical class 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000002184 metal Chemical class 0.000 description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 3
- 238000009736 wetting Methods 0.000 description 3
- XOBRDIKDYBKVKH-UHFFFAOYSA-N 2-cyclohexylnaphthalene-1-sulfonic acid Chemical compound C1=CC2=CC=CC=C2C(S(=O)(=O)O)=C1C1CCCCC1 XOBRDIKDYBKVKH-UHFFFAOYSA-N 0.000 description 2
- ZTFYJIXFKGPCHV-UHFFFAOYSA-N 2-propan-2-ylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C(C)C)=CC=C21 ZTFYJIXFKGPCHV-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 150000001339 alkali metal compounds Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229960004756 ethanol Drugs 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910052751 metal Chemical class 0.000 description 2
- 239000001814 pectin Substances 0.000 description 2
- 229920001277 pectin Polymers 0.000 description 2
- 235000010987 pectin Nutrition 0.000 description 2
- 159000000000 sodium salts Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000001117 sulphuric acid Substances 0.000 description 2
- 235000011149 sulphuric acid Nutrition 0.000 description 2
- 210000002268 wool Anatomy 0.000 description 2
- YRJSLCBKZMMEPB-UHFFFAOYSA-N 2-(2-methylpropyl)naphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(CC(C)C)=CC=C21 YRJSLCBKZMMEPB-UHFFFAOYSA-N 0.000 description 1
- 102000009027 Albumins Human genes 0.000 description 1
- 108010088751 Albumins Proteins 0.000 description 1
- 229910000906 Bronze Inorganic materials 0.000 description 1
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical class [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 235000000177 Indigofera tinctoria Nutrition 0.000 description 1
- 239000005569 Iron sulphate Substances 0.000 description 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000005708 Sodium hypochlorite Substances 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 241001584775 Tunga penetrans Species 0.000 description 1
- 241000219422 Urtica Species 0.000 description 1
- 235000009108 Urtica dioica Nutrition 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 229940037003 alum Drugs 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000012550 audit Methods 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000010974 bronze Substances 0.000 description 1
- 229940043430 calcium compound Drugs 0.000 description 1
- 150000001674 calcium compounds Chemical class 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- SURLGNKAQXKNSP-DBLYXWCISA-N chlorin Chemical compound C\1=C/2\N/C(=C\C3=N/C(=C\C=4NC(/C=C\5/C=CC/1=N/5)=CC=4)/C=C3)/CC\2 SURLGNKAQXKNSP-DBLYXWCISA-N 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 229910021563 chromium fluoride Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 description 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 229940097275 indigo Drugs 0.000 description 1
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 description 1
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
- 229960004592 isopropanol Drugs 0.000 description 1
- 239000010721 machine oil Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000010446 mirabilite Substances 0.000 description 1
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical class C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 1
- 150000007530 organic bases Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 description 1
- 229960003656 ricinoleic acid Drugs 0.000 description 1
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 1
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 1
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- FTBATIJJKIIOTP-UHFFFAOYSA-K trifluorochromium Chemical compound F[Cr](F)F FTBATIJJKIIOTP-UHFFFAOYSA-K 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/12—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen combined with specific additives
Definitions
- the fiber be wet: ted
- Monopol-soap is a name sometimes applied to the sodium salt of ricinoleic acid.
- These additions are objectionable for various reasons, the additions having a low efliciency and being uneconomical.
- most of thesaid ingredients are not appropriate for dyeing wool in acetic or sulphuric acid baths, because in caseof organic bases, inactive salts are formed, and in case of soaps, Turkey-red oils, and the like, decompositions take place with the production of fatty acids which are insoluble in water. Also in case of oils which are stable in acids the dispersing property is reduced, so that the favorable action is largely lost.
- the solutions of the said compounds are suitable for forming the dye-stuff into a paste, and they improve the dispersion of the dye-stuff, and thereby they prevent too rapid. and non-uniform absorption of the dye-stuff they improve the tints and the rubbing property, and they prevent the formation of bronze.
- the property of improving the suspension and emulsion is particularly important when dyeing matter containing oily impurities, which by reason of the said impurities are not easily uniformly dyed. For example, oily cotton obtained as a waste roduct from spinning mills and weaving actories, or carpet yarns containing residues of oils which cannot be saponified can be uniformly dyed without having the residue of the fat removed.
- the aliphatically substituted aromatic sulpho acids or the salts thereof are distinguished from the known subsidiary ingredients used in dyeing, in that they may be universally used and that they have the aforesaid technical advantages.
- the inorganic mordants such as potassium-bichromate, chromium-fluoride,
- alum, copper-sulphate, iron-sulphate, chloride of tin, etc, may be completely or in part substituted in mordant dyeing by the
- the moistcning and permeating action of i the said sulpho-acids and their salts can be further improved by adding thereto alcohols of one and higher valencies and soluble in water, such as methyl-alcohol, ethyl-alcohol, isopropyl-alcohol, mayl-alcohol, glycol-glycerine.
- the said sulphonic-acids may be added to the aforesaid bath heretofore used preparatory to bleaching.
- Example 1 bleaching of piece go0tls.-100 kilogrammes of nettle fabric are bleached from 3 to 4 hours in a bleaching jigger by means of 500 liters of a chloride of lime bleaching'liquor of 0.7 B. (1 Twaddell) containing 0.4 gramme of sodium salt of isobutyl naphthalene sulphonic acid per liter, whereupon it is further treated in the usual way.
- Example 2 dyeing 100 kilogrammes 0 f cotton g am.-Five kilogrammes of powdered indigo and kilogramme of potassium salt of cyclo-hexyl-naphthalene sulphonic acid are formed with three liters of water into a homogeneous paste, and the said paste is brought into a bath of about 3000 liters of water, 2.5 liters of soda solution of 30 B. (52.13 Twaddell and 1.8 kilogrammes of anhydrous sodium-hydro-sulfite at a'temperature of 40 C. (104 F.). Thereafter dyeing is carried on in the usual way.
- Example 3 dyeing of 100 kilogram/mes of wool felt (hat felt).-1 kilogram of a suitable acid dye-stuif is formed into a paste with a solution of 0.8 kilogramme of isopropyl-naphthalene-sulphonic-acid and two liters of water, which paste is gradually added to the dyers bath of about 3000 liters together with two kilogrammes of concentrated sulphuric acid and 8 kilogrammes of calcined Glauber salt.
- the felt material is dyed in the usual way at boiling temperature to extraction of the bath.
- raw fibrous material is meant a material which contains the natural constituents of the fiber such as starches, gums, pectins and the like, and also contains contaminating material such as machine oil, grease and the like.
- the process of bleaching raw fibrous material which comprises introducing the raw fibrous material into a cold bath containing an alkali metal compound yielding hydroxyl ions in aqueous solution and then introducing the fibrous material into a cold bleaching liquor containing a salt of an aliphatically substituted aromatic sulphonic acid and an unstable chlorine compound and then completing the bleaching process in known manner.
- the process of bleaching raw fibrous material which comprises introducing the said raw fibrous material into a cold bath containing an alkali metal compound yield- I ing hydroxyl ions in aqueous solution and then introducing the fibrous material into a cold bleaching liquor containing a salt of an alkyl substituted naphthalene sulphonic acid and bleaching powder and completing the bleaching process in known manner.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Detergent Compositions (AREA)
- Paper (AREA)
- Coloring (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE246155X | 1925-01-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1881745A true US1881745A (en) | 1932-10-11 |
Family
ID=5934637
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US81311A Expired - Lifetime US1881745A (en) | 1925-01-14 | 1926-01-14 | Process of bleaching, dyeing, and printing vegetable and animal fiber material, fabrics, or felt |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US1881745A (enrdf_load_stackoverflow) |
| BE (1) | BE331503A (enrdf_load_stackoverflow) |
| GB (1) | GB246155A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2893913A (en) * | 1955-08-29 | 1959-07-07 | Monsanto Chemicals | Wetting and dispersing agents containing a water-soluble lignosulfonic acid salt |
| US3027223A (en) * | 1957-12-11 | 1962-03-27 | Dow Chemical Co | Caustic mercerizing solutions |
| US3950277A (en) * | 1973-07-25 | 1976-04-13 | The Procter & Gamble Company | Laundry pre-soak compositions |
| US4285695A (en) * | 1977-12-14 | 1981-08-25 | Olin Corporation | Process for inhibiting crust formation in reduced dye baths |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE753848C (de) * | 1938-08-03 | 1951-12-20 | Holtmann & Co Komm Ges A | Stabilisieren alkalischer Peroxydbleichbaeder |
| US2606094A (en) * | 1949-08-22 | 1952-08-05 | Byrne Mazy | Process of degumming bast fibers |
-
0
- BE BE331503D patent/BE331503A/xx unknown
-
1926
- 1926-01-14 GB GB1143/26A patent/GB246155A/en not_active Expired
- 1926-01-14 US US81311A patent/US1881745A/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2893913A (en) * | 1955-08-29 | 1959-07-07 | Monsanto Chemicals | Wetting and dispersing agents containing a water-soluble lignosulfonic acid salt |
| US3027223A (en) * | 1957-12-11 | 1962-03-27 | Dow Chemical Co | Caustic mercerizing solutions |
| US3950277A (en) * | 1973-07-25 | 1976-04-13 | The Procter & Gamble Company | Laundry pre-soak compositions |
| US4285695A (en) * | 1977-12-14 | 1981-08-25 | Olin Corporation | Process for inhibiting crust formation in reduced dye baths |
Also Published As
| Publication number | Publication date |
|---|---|
| BE331503A (enrdf_load_stackoverflow) | |
| GB246155A (en) | 1926-08-12 |
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