US12606515B2 - Method for producing compound - Google Patents

Method for producing compound

Info

Publication number
US12606515B2
US12606515B2 US18/025,576 US202118025576A US12606515B2 US 12606515 B2 US12606515 B2 US 12606515B2 US 202118025576 A US202118025576 A US 202118025576A US 12606515 B2 US12606515 B2 US 12606515B2
Authority
US
United States
Prior art keywords
wash column
slurry
hydraulic wash
crystals
compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active, expires
Application number
US18/025,576
Other languages
English (en)
Other versions
US20240025835A1 (en
Inventor
Hiroki Wada
Masashi MUKAE
Yasutaka TAKEMOTO
Toyofumi Sakai
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Shokubai Co Ltd
Original Assignee
Nippon Shokubai Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd
Publication of US20240025835A1 publication Critical patent/US20240025835A1/en
Application granted granted Critical
Publication of US12606515B2 publication Critical patent/US12606515B2/en
Active legal-status Critical Current
Adjusted expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
    • B01D9/0045—Washing of crystals, e.g. in wash columns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D2009/0086—Processes or apparatus therefor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
US18/025,576 2020-09-11 2021-09-08 Method for producing compound Active 2043-01-29 US12606515B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2020-153287 2020-09-11
JP2020153287 2020-09-11
PCT/JP2021/033037 WO2022054841A1 (ja) 2020-09-11 2021-09-08 化合物の製造方法

Publications (2)

Publication Number Publication Date
US20240025835A1 US20240025835A1 (en) 2024-01-25
US12606515B2 true US12606515B2 (en) 2026-04-21

Family

ID=80631857

Family Applications (1)

Application Number Title Priority Date Filing Date
US18/025,576 Active 2043-01-29 US12606515B2 (en) 2020-09-11 2021-09-08 Method for producing compound

Country Status (7)

Country Link
US (1) US12606515B2 (https=)
EP (1) EP4212504A4 (https=)
JP (1) JP7574306B2 (https=)
KR (1) KR102869324B1 (https=)
CN (1) CN116057034B (https=)
TW (1) TWI883258B (https=)
WO (1) WO2022054841A1 (https=)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2024128153A1 (ja) * 2022-12-16 2024-06-20 株式会社日本触媒 結晶粒を含むスラリーを容器から排出する方法

Citations (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4286101A (en) * 1978-10-19 1981-08-25 Mitsubishi Chemical Industries Ltd. Process for preparing terephthalic acid
JPH11123302A (ja) 1997-10-22 1999-05-11 Tsukishima Kikai Co Ltd 結晶の溶融精製方法および装置
US6018077A (en) * 1997-04-17 2000-01-25 Mitsubishi Gas Chemical Company, Inc. Process for producing 2,6-naphthalenedicarboxylic acid
US20020008064A1 (en) 2000-06-19 2002-01-24 Kei Hamamoto Solid substance removing device
US20030060661A1 (en) 2000-04-11 2003-03-27 Bernd Eck Method for the purification of a crude acrylic acid melt
US20030175159A1 (en) 2000-07-28 2003-09-18 Jorg Heilek Regulation of a wash column in a melt crystallization process
US20040256319A1 (en) 2001-11-15 2004-12-23 Ulrich Hammon Method for performing the purifying separation of crystals out their suspension in a mother liquor
JP2005509009A (ja) 2001-11-15 2005-04-07 ビーエーエスエフ アクチェンゲゼルシャフト 結晶を母液中の結晶の懸濁液から精製分離する方法
JP2006069959A (ja) 2004-09-02 2006-03-16 Kureha Engineering Co Ltd 結晶精製方法及びそのための装置
US20070129572A1 (en) 2005-12-06 2007-06-07 Fumio Shibusawa Method for producing acrylic acid
JP2007182437A (ja) 2005-12-06 2007-07-19 Nippon Shokubai Co Ltd アクリル酸の製造方法
WO2007108875A1 (en) 2006-03-21 2007-09-27 Bp Corporation North America Inc. Apparatus and process for the separation of solids and liquids
WO2009095111A1 (en) 2008-01-30 2009-08-06 Evonik Röhm Gmbh Process for preparation of high purity methacrylic acid
JP2010059107A (ja) 2008-09-04 2010-03-18 Mitsubishi Rayon Co Ltd 原料粗結晶の精製方法
WO2011045356A1 (de) 2009-10-16 2011-04-21 Basf Se Verfahren der inbetriebnahme eines trennverfahrens zur reinigenden abtrennung von acrylsäurekristallen aus einer suspension s ihrer kristalle in mutterlauge
US8232425B2 (en) * 2005-12-22 2012-07-31 Basf Aktiengesellschaft Process for heterogeneously catalyzed partial gas phase oxidation of propylene to acrylic acid
WO2018216699A1 (ja) 2017-05-25 2018-11-29 株式会社日本触媒 （メタ）アクリル酸の製造方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10017903A1 (de) * 2000-04-11 2001-10-18 Basf Ag Verfahren zur Reinigung einer Rohacrylsäureschmelze
NL1019862C2 (nl) 2002-01-30 2003-07-31 Tno Werkwijze en inrichting voor het verwerken van een suspensie.
US8673245B2 (en) 2008-09-22 2014-03-18 Nippon Shokubai Co., Ltd. Fixed-bed reactor and process for producing acrylic acid using the reactor

Patent Citations (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4286101A (en) * 1978-10-19 1981-08-25 Mitsubishi Chemical Industries Ltd. Process for preparing terephthalic acid
US6018077A (en) * 1997-04-17 2000-01-25 Mitsubishi Gas Chemical Company, Inc. Process for producing 2,6-naphthalenedicarboxylic acid
JPH11123302A (ja) 1997-10-22 1999-05-11 Tsukishima Kikai Co Ltd 結晶の溶融精製方法および装置
JP2003530376A (ja) 2000-04-11 2003-10-14 ビーエーエスエフ アクチェンゲゼルシャフト 粗製アクリル酸溶融物の精製法
US20030060661A1 (en) 2000-04-11 2003-03-27 Bernd Eck Method for the purification of a crude acrylic acid melt
US20020008064A1 (en) 2000-06-19 2002-01-24 Kei Hamamoto Solid substance removing device
US20030175159A1 (en) 2000-07-28 2003-09-18 Jorg Heilek Regulation of a wash column in a melt crystallization process
US20040256319A1 (en) 2001-11-15 2004-12-23 Ulrich Hammon Method for performing the purifying separation of crystals out their suspension in a mother liquor
US20050006299A1 (en) 2001-11-15 2005-01-13 Jorg Heilek Device for performing the purifying separation of crystals out of their suspension in a contaminated crystal melt
JP2005509010A (ja) 2001-11-15 2005-04-07 ビーエーエスエフ アクチェンゲゼルシャフト 不純化された結晶溶融液中の結晶の懸濁液から結晶を精製分離するための装置
JP2005509009A (ja) 2001-11-15 2005-04-07 ビーエーエスエフ アクチェンゲゼルシャフト 結晶を母液中の結晶の懸濁液から精製分離する方法
JP2006069959A (ja) 2004-09-02 2006-03-16 Kureha Engineering Co Ltd 結晶精製方法及びそのための装置
US20070129572A1 (en) 2005-12-06 2007-06-07 Fumio Shibusawa Method for producing acrylic acid
JP2007182437A (ja) 2005-12-06 2007-07-19 Nippon Shokubai Co Ltd アクリル酸の製造方法
US8232425B2 (en) * 2005-12-22 2012-07-31 Basf Aktiengesellschaft Process for heterogeneously catalyzed partial gas phase oxidation of propylene to acrylic acid
WO2007108875A1 (en) 2006-03-21 2007-09-27 Bp Corporation North America Inc. Apparatus and process for the separation of solids and liquids
JP2009530103A (ja) 2006-03-21 2009-08-27 ビーピー・コーポレーション・ノース・アメリカ・インコーポレーテッド 固体と液体を分離するための装置及び方法
US7812206B2 (en) * 2006-03-21 2010-10-12 Bp Corporation North America Inc. Apparatus and process for the separation of solids and liquids
US20070225539A1 (en) 2006-03-21 2007-09-27 Wilsak Richard A Apparatus and Process for the Separation of Solids and Liquids
WO2009095111A1 (en) 2008-01-30 2009-08-06 Evonik Röhm Gmbh Process for preparation of high purity methacrylic acid
US20100273970A1 (en) 2008-01-30 2010-10-28 Evonik Roehm Gmbh Process for preparation of high purity methacrylic acid
JP2011514311A (ja) 2008-01-30 2011-05-06 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツング 高純度メタクリル酸の製造方法
JP2010059107A (ja) 2008-09-04 2010-03-18 Mitsubishi Rayon Co Ltd 原料粗結晶の精製方法
WO2011045356A1 (de) 2009-10-16 2011-04-21 Basf Se Verfahren der inbetriebnahme eines trennverfahrens zur reinigenden abtrennung von acrylsäurekristallen aus einer suspension s ihrer kristalle in mutterlauge
US20110124834A1 (en) 2009-10-16 2011-05-26 Basf Se Process for starting up a separating process for purifying removal of acrylic acid crystals from a suspension s of crystals thereof in mother liquor
WO2018216699A1 (ja) 2017-05-25 2018-11-29 株式会社日本触媒 （メタ）アクリル酸の製造方法
US20200181056A1 (en) 2017-05-25 2020-06-11 Nippon Shokubai Co., Ltd. Method for producing (meth)acrylic acid
US10919834B2 (en) * 2017-05-25 2021-02-16 Nippon Shokubai Co., Ltd. Method for producing (meth)acrylic acid

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
International Search Report dated Dec. 7, 2021, which issued in the corresponding PCT Patent Application No. PCT/JP2021/033037, including English translation.
Verdoes et al., Speciality Chemicals Magazine, 2009.

Also Published As

Publication number Publication date
EP4212504A1 (en) 2023-07-19
JP7574306B2 (ja) 2024-10-28
CN116057034B (zh) 2025-05-09
TW202219026A (zh) 2022-05-16
EP4212504A4 (en) 2025-02-12
KR20230051586A (ko) 2023-04-18
BR112023004298A2 (pt) 2023-04-04
CN116057034A (zh) 2023-05-02
WO2022054841A1 (ja) 2022-03-17
TWI883258B (zh) 2025-05-11
JPWO2022054841A1 (https=) 2022-03-17
KR102869324B1 (ko) 2025-10-14
US20240025835A1 (en) 2024-01-25

Similar Documents

Publication Publication Date Title
JPH1045667A (ja) 分散媒置換装置を用いた高純度テレフタル酸の製造方法
US12606515B2 (en) Method for producing compound
CN101981018B (zh) 在马来酸酐的生产期间分离出富马酸和其它次要组分的方法
US20230373897A1 (en) Purification device
US12600693B2 (en) Method for producing compound
EP4349444A1 (en) Purification apparatus
EP4635590A1 (en) Method for discharging crystal grain-containing slurry from container
TWI913474B (zh) 純化裝置、化合物之製造方法及其純化方法
BR112023004298B1 (pt) Método para produzir um composto
EP4349807A1 (en) Method for producing easily polymerizable compound
BR112023004299B1 (pt) Aparelho de purificação que purifica cristais, método para produzir um composto e método para purificar um composto

Legal Events

Date Code Title Description
AS Assignment

Owner name: NIPPON SHOKUBAI CO., LTD., JAPAN

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:WADA, HIROKI;MUKAE, MASASHI;TAKEMOTO, YASUTAKA;AND OTHERS;REEL/FRAME:062991/0468

Effective date: 20230303

STPP Information on status: patent application and granting procedure in general

Free format text: DOCKETED NEW CASE - READY FOR EXAMINATION

STPP Information on status: patent application and granting procedure in general

Free format text: NON FINAL ACTION COUNTED, NOT YET MAILED

STPP Information on status: patent application and granting procedure in general

Free format text: NON FINAL ACTION MAILED

STPP Information on status: patent application and granting procedure in general

Free format text: NON FINAL ACTION MAILED

STPP Information on status: patent application and granting procedure in general

Free format text: ALLOWED -- NOTICE OF ALLOWANCE NOT YET MAILED

STPP Information on status: patent application and granting procedure in general

Free format text: NOTICE OF ALLOWANCE MAILED -- APPLICATION RECEIVED IN OFFICE OF PUBLICATIONS

STPP Information on status: patent application and granting procedure in general

Free format text: PUBLICATIONS -- ISSUE FEE PAYMENT RECEIVED

Free format text: PUBLICATIONS -- ISSUE FEE PAYMENT VERIFIED

STCF Information on status: patent grant

Free format text: PATENTED CASE