UA81221C2 - Process and plant for the heterogeneous synthesis of chemical compounds - Google Patents

Process and plant for the heterogeneous synthesis of chemical compounds Download PDF

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Publication number
UA81221C2
UA81221C2 UA2003098878A UA2003098878A UA81221C2 UA 81221 C2 UA81221 C2 UA 81221C2 UA 2003098878 A UA2003098878 A UA 2003098878A UA 2003098878 A UA2003098878 A UA 2003098878A UA 81221 C2 UA81221 C2 UA 81221C2
Authority
UA
Ukraine
Prior art keywords
reaction zone
reaction
heat exchange
fed
differs
Prior art date
Application number
UA2003098878A
Other languages
English (en)
Ukrainian (uk)
Inventor
Ermanno Philippi
Enrico Rizzi
Mirko Tarozzo
Original Assignee
Methanol Casale Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Methanol Casale Sa filed Critical Methanol Casale Sa
Publication of UA81221C2 publication Critical patent/UA81221C2/uk

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C01C1/0417Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
    • C01C1/0423Cold wall reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0207Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal
    • B01J8/0214Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal in a cylindrical annular shaped bed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0285Heating or cooling the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0403Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
    • B01J8/0407Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds
    • B01J8/0415Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C07C29/151Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
    • C07C29/152Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the reactor used
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D9/00Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D9/0006Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the plate-like or laminated conduits being enclosed within a pressure vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00115Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015Plates; Cylinders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00309Controlling the temperature by indirect heat exchange with two or more reactions in heat exchange with each other, such as an endothermic reaction in heat exchange with an exothermic reaction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19Details relating to the geometry of the reactor
    • B01J2219/194Details relating to the geometry of the reactor round
    • B01J2219/1941Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1943Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
UA2003098878A 2001-11-11 2002-02-10 Process and plant for the heterogeneous synthesis of chemical compounds UA81221C2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP01126840A EP1310475A1 (en) 2001-11-11 2001-11-11 Process and plant for the heterogeneous synthesis of chemical compounds
PCT/EP2002/011027 WO2003042143A1 (en) 2001-11-11 2002-10-02 Process and plant for the heterogeneous synthesis of chemical compounds

Publications (1)

Publication Number Publication Date
UA81221C2 true UA81221C2 (en) 2007-12-25

Family

ID=8179218

Family Applications (1)

Application Number Title Priority Date Filing Date
UA2003098878A UA81221C2 (en) 2001-11-11 2002-02-10 Process and plant for the heterogeneous synthesis of chemical compounds

Country Status (15)

Country Link
US (1) US6946494B2 (pt)
EP (2) EP1310475A1 (pt)
CN (1) CN1305822C (pt)
AR (1) AR037344A1 (pt)
AT (1) ATE468312T1 (pt)
AU (1) AU2002363759B2 (pt)
BR (2) BR0209799A (pt)
CA (1) CA2433846C (pt)
DE (1) DE60236448D1 (pt)
EG (1) EG23247A (pt)
MX (1) MXPA03006821A (pt)
MY (1) MY131898A (pt)
RU (1) RU2310641C2 (pt)
UA (1) UA81221C2 (pt)
WO (1) WO2003042143A1 (pt)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1153653A1 (en) * 2000-05-11 2001-11-14 Methanol Casale S.A. Reactor for exothermic or endothermic heterogeneous reactions
EP1221339A1 (en) * 2001-01-05 2002-07-10 Methanol Casale S.A. Catalytic reactor with heat exchanger for exothermic and endothermic heterogeneous chemical reactions
EP1236505A1 (en) * 2001-02-27 2002-09-04 Methanol Casale S.A. Method for carrying out chemical reactions in pseudo-isothermal conditions
MX2007001173A (es) * 2004-01-15 2007-09-25 Methanol Casale Sa Reactor catalitico de lecho fijo.
CN102247792A (zh) * 2011-04-30 2011-11-23 甘肃银光聚银化工有限公司 一种新型多相搅拌反应器
JP2017536229A (ja) * 2014-10-30 2017-12-07 サビック グローバル テクノロジーズ ベスローテン フエンノートシャップ 径方向に設置された冷却板を備えた反応器、及びそれを使用した方法
EP3050849A1 (en) 2015-01-27 2016-08-03 Casale SA A process for the synthesis of ammonia
NZ748600A (en) 2016-06-21 2023-06-30 Haldor Topsoe As Axial/radial flow converter
EP3401006A1 (en) * 2017-05-11 2018-11-14 Casale Sa Multi-bed catalytic converter with inter-bed cooling
AR113649A1 (es) * 2017-12-20 2020-05-27 Haldor Topsoe As Convertidor de flujo axial enfriado
AR113648A1 (es) 2017-12-20 2020-05-27 Haldor Topsoe As Convertidor de flujo axial adiabático
CN113226536A (zh) * 2019-02-01 2021-08-06 托普索公司 板式换热器与放热反应器的结合使用
CN109999749A (zh) * 2019-03-15 2019-07-12 中国煤层气集团有限公司 两相或多相反应容器

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2153437B2 (de) 1971-10-27 1974-11-21 Metallgesellschaft Ag, 6000 Frankfurt Reaktor zur Herstellung von Methanol
DE3201776A1 (de) * 1982-01-21 1983-09-08 Krupp-Koppers Gmbh, 4300 Essen Verfahren zur gleichzeitigen erzeugung von methanol- und ammoniak-synthesegas.
DE3790376T1 (pt) 1986-07-24 1988-06-23
DE19605572A1 (de) * 1996-02-15 1997-08-21 Metallgesellschaft Ag Verfahren zum Erzeugen von Methanol

Also Published As

Publication number Publication date
BRPI0209799B1 (pt) 2019-07-02
US20040204507A1 (en) 2004-10-14
AU2002363759B2 (en) 2008-06-05
RU2310641C2 (ru) 2007-11-20
WO2003042143A1 (en) 2003-05-22
AR037344A1 (es) 2004-11-03
CA2433846C (en) 2010-08-17
MXPA03006821A (es) 2003-12-04
CA2433846A1 (en) 2003-05-22
EP1444186A1 (en) 2004-08-11
MY131898A (en) 2007-09-28
BR0209799A (pt) 2004-06-01
CN1498199A (zh) 2004-05-19
ATE468312T1 (de) 2010-06-15
CN1305822C (zh) 2007-03-21
EP1444186B1 (en) 2010-05-19
EP1310475A1 (en) 2003-05-14
RU2003128885A (ru) 2005-04-10
EG23247A (en) 2004-09-29
DE60236448D1 (de) 2010-07-01
US6946494B2 (en) 2005-09-20

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