TWI524849B - Method for the preparation of oyster meat extract using continuous centrifugal separation device - Google Patents

Method for the preparation of oyster meat extract using continuous centrifugal separation device Download PDF

Info

Publication number
TWI524849B
TWI524849B TW102117374A TW102117374A TWI524849B TW I524849 B TWI524849 B TW I524849B TW 102117374 A TW102117374 A TW 102117374A TW 102117374 A TW102117374 A TW 102117374A TW I524849 B TWI524849 B TW I524849B
Authority
TW
Taiwan
Prior art keywords
solution
oyster meat
meat extract
rotating
continuously
Prior art date
Application number
TW102117374A
Other languages
Chinese (zh)
Other versions
TW201444473A (en
Inventor
Mitsugu Watanabe
Original Assignee
Watanabe Oyster Lab Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Watanabe Oyster Lab Co Ltd filed Critical Watanabe Oyster Lab Co Ltd
Priority to TW102117374A priority Critical patent/TWI524849B/en
Publication of TW201444473A publication Critical patent/TW201444473A/en
Application granted granted Critical
Publication of TWI524849B publication Critical patent/TWI524849B/en

Links

Landscapes

  • Meat, Egg Or Seafood Products (AREA)

Description

使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法 Extraction and manufacturing method of oyster meat extract using continuous centrifugal separation device

本發明係關於能夠從例如生牡蠣等的牡蠣肉有效率地萃取出牡蠣肉萃取物,並且不會使存在牡蠣肉內的有益之有效成分的微量成分流失地加以萃取,製造牡蠣肉萃取物製品的使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法。 The present invention relates to an oyster meat extract which can be efficiently extracted from oyster meat such as raw oysters without extracting trace components which are beneficial active ingredients in the oyster meat. An extraction manufacturing method of oyster meat extract using a continuous centrifugal separator.

近年,牡蠣肉萃取物製品係作為健康輔助食品含有大量的有益物質極為優良之製品,一般對其認識度日益增高。 In recent years, oyster meat extract products are excellent products containing a large amount of beneficial substances as health supplement foods, and their awareness is generally increasing.

現今關於藉由各種萃取法所萃取的牡蠣肉萃取物之健康輔助食品被販賣著(日本特開平10-136946號公報)。 A health supplement food for oyster meat extract extracted by various extraction methods is now being sold (Japanese Patent Laid-Open No. Hei 10-136946).

在進行牡蠣肉萃取物之萃取時,期望萃取製造出在所萃取出的牡蠣肉萃取物內含有大量的肝醣、胺基乙磺酸或蛋白質、硒等的有益營養源及包含鋅等具有所謂可抑制血小板凝結的作用的物質或近年被注目的抗氧化物質等的有效成分且作業效率佳地回收者。 In the extraction of the oyster meat extract, it is desirable to extract a beneficial nutrient source containing a large amount of glycogen, amino ethanesulfonic acid or protein, selenium, etc. in the extracted oyster meat extract and contains zinc. A substance which can suppress the action of platelet aggregation or an active ingredient such as an antioxidant substance which has been attracting attention in recent years, and which is efficiently recovered.

以往,當進行牡蠣肉萃取物的萃取製造之際,採用所 謂的自然沉澱法,攪拌含有牡蠣肉萃取物的萃取溶液,在經過預定時間後,將所謂的沉澱之沉澱物與不沉澱之上澄清液自然分離,分別從各物質萃取出牡蠣肉萃取物的有效成分,但因進行此攪拌及自然沉澱法時之沉澱物的沉澱和與上澄清液之分離作業,必須等待預定時間的攪拌後之自然沉澱,在此方法,存在有必須要一定的待機時間,並且無法利用於大量生產之課題。 In the past, when extracting oyster meat extracts, In the natural precipitation method, the extraction solution containing the oyster meat extract is stirred, and after a predetermined period of time, the so-called precipitated precipitate is naturally separated from the non-precipitate supernatant, and the oyster meat extract is extracted from each substance. The active ingredient, but the sedimentation of the precipitate and the separation from the supernatant liquid during the stirring and natural precipitation method must wait for the natural precipitation after stirring for a predetermined time. In this method, there is a certain waiting time. And can not be used for mass production issues.

亦即,以往,對基於前述攪拌沉澱的沉澱物與上澄清液之分離作業不存在有可連續地進行的裝置,因此,存在有為了大量地進行牡蠣肉萃取物萃取處理作業,而還是需要長時間之進行此攪拌沉澱分離的作業時間之課題。 In other words, in the past, there was no continuous operation for the separation of the precipitate based on the agitation and the supernatant, and therefore there was a large amount of extraction operation of the oyster meat extract, but it was still necessary. Time is the subject of the operation time of the stirring and precipitation separation.

〔專利文獻1〕日本特開平10-136946號公報 [Patent Document 1] Japanese Patent Laid-Open No. Hei 10-136946

如此,本發明係有鑑於前述課題而開發完成的發明,其目的在於提供使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法,該方法係對以往所必須進行的含有牡蠣肉萃取物之溶液的攪拌作業、所謂的基於自然沉澱之沉澱物與不沉澱的上澄清液之分離作業、又從各沉澱物及上澄清液萃取出牡蠣肉萃取物的有效成分之作業,不需要依賴自然沉澱而可強制地予以分離,並且可連續地進行該分離作業,藉此,可大幅地縮短攪拌沉澱分離的作業時間,尤其是沉澱物的沉澱時間、也不需進行待機,因此能有效率地 進行牡蠣肉萃取物的萃取製造作業之劃時代的牡蠣肉萃取物的萃取製造方法。 Thus, the present invention has been made in view of the above problems, and an object thereof is to provide an extraction and production method of an oyster meat extract using a continuous centrifugal separation apparatus, which is a solution containing oyster meat extract which has been conventionally required. The stirring operation, the so-called separation of the precipitate based on natural precipitation and the supernatant without sedimentation, and the extraction of the active ingredients of the oyster meat extract from each of the precipitates and the supernatant liquid do not depend on natural precipitation. The separation can be forcibly separated, and the separation operation can be continuously performed, whereby the operation time of the agitation and sedimentation separation can be greatly shortened, in particular, the sedimentation time of the precipitate is not required to stand by, so that the separation can be performed efficiently An epoch-making method for extracting oyster meat extracts from the extraction and production of oyster meat extracts.

一種使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法,該連續離心分離裝置是具有:在內部具有收納空間部的收納體;旋轉體,該旋轉體配置在該收納體內,具有構成為能以長度方向作為軸芯方向進行旋轉的旋轉軸部,且具有從該旋轉軸部的外周隔著間隔配置之複數個旋轉葉片;使該旋轉體旋轉的旋轉手段;將欲分離的溶液連續注入到前述收納空間部的注入部;將自注入部所注入的溶液予以進行離心分離,而使從前述收納空間部的側部分離之流動物連續排出之排出部;及將從前述流動物所分離之剩餘的溶液連續地排出的溶液排出部,其特徵為:從牡蠣肉萃取出牡蠣肉萃取物,將該所萃取的牡蠣肉萃取物予以濃縮,將再對含有前述濃縮後的牡蠣肉萃取物之溶液添加乙醇溶液的攪拌分離製程作為使用前述連續離心分離裝置之離心分離製程,在前述離心分離製程,將含有前述萃取並濃縮之牡蠣肉萃取物的溶液由左側管朝送出管可調整送出量地送出,並且從右側管將乙醇溶液可調節濃度並且可調整送出量地朝前述送出管送出,前述雙方的溶液連續地送出至前述注入部,該連續地送出的雙方溶液儲存在前述收納體內,使前述旋轉體旋轉,進行將收納體內的雙方溶液攪拌並離心分離之作業,藉由前述旋轉,前述流動物 被聚集到朝前述收納體的凹陷成三角形之側壁的頂角部分側,當預定量的該流動物聚集至凹陷成前述三角形的側壁的頂角部分側時,以作動液進行開閉作動,在凹陷成前述三角形的側壁之頂角部分的圓周方向上,開口形成有隔著預定間隔所設置之複數個排出孔,藉由前述複數個排出孔將前述流動物通過前述排出部而連續地排出至外部,藉由從前述旋轉軸部外周朝外側突出成裙狀所設置之前述複數個旋轉葉片的旋轉,使從前述流動物所分離之剩餘的溶液朝收納體上方移動,由配置在收納體的上方之前述溶液排出部連續排出,前述連續排出的前述剩餘的溶液在濃縮後再次添加預定濃度的乙醇溶液,藉由第2連續離心分離裝置加以分離,再由前述溶液排出部連續排出。 An extraction and manufacturing method of an oyster meat extract using a continuous centrifugal separation apparatus, comprising: a storage body having a storage space portion therein; and a rotating body disposed in the storage body and configured to be capable of a rotating shaft portion that rotates in a longitudinal direction as a core direction, and has a plurality of rotating blades arranged at intervals from an outer circumference of the rotating shaft portion; a rotating means for rotating the rotating body; and continuously injecting the solution to be separated into An injection portion of the storage space portion; a discharge portion that centrifugally separates the solution injected from the injection portion, and continuously discharges the fluid separated from the side portion of the storage space portion; and the separation from the fluid material The solution discharge portion continuously discharged from the remaining solution is characterized in that the oyster meat extract is extracted from the oyster meat, and the extracted oyster meat extract is concentrated, and the oyster meat extract containing the concentrate is further added. A stirring separation process in which a solution is added with an ethanol solution as a centrifugal separation process using the aforementioned continuous centrifugal separation device, before a centrifugation process, the solution containing the extracted and concentrated oyster meat extract is sent from the left side tube to the delivery tube to adjust the delivery amount, and the ethanol solution is adjusted in concentration from the right side tube and the delivery amount can be adjusted to the aforementioned delivery tube. The two solutions are continuously sent to the injection unit, and the two solutions that are continuously sent are stored in the storage body, and the rotating body is rotated to perform the operation of stirring and centrifuging the both solutions in the storage body. Rotating, the aforementioned fluid When it is gathered toward the apex portion side of the side wall of the recessed portion which is formed into a triangle toward the storage body, when a predetermined amount of the flow material is collected to the side of the apex portion of the side wall of the triangular shape, the opening and closing operation is performed as a moving liquid, and the depression is performed. In the circumferential direction of the apex portion of the side wall of the triangular shape, the opening is formed with a plurality of discharge holes provided at predetermined intervals, and the flow material is continuously discharged to the outside through the discharge portion by the plurality of discharge holes The rotation of the plurality of rotating blades provided in a skirt shape from the outer circumference of the rotating shaft portion outwardly moves the remaining solution separated from the fluid to the upper side of the storage body, and is disposed above the storage body The solution discharge unit is continuously discharged, and the remaining solution continuously discharged is concentrated, and a predetermined concentration of the ethanol solution is added again, separated by a second continuous centrifugal separator, and continuously discharged from the solution discharge unit.

或者,一種牡蠣肉萃取物的萃取製造方法,係具有:將生牡蠣肉收納於儲存有溶液的萃取容器內,在該萃取容器內從前述生牡蠣肉萃取牡蠣肉萃取物之萃取製程;將在前述萃取製程所萃取出的牡蠣肉萃取物予以濃縮之製程;對已被濃縮的牡蠣肉萃取物添加乙醇溶液並加以攪拌之攪拌製程;及將在進行前述攪拌後所獲得的沉澱物予以濃縮之濃縮製程,其特徵為:前述攪拌製程是作為使用連續離心分離裝置的離心分離製程所構成,該連續離心分離裝置是具有:在內部具有收納空間部的收納體;旋轉體,該旋轉體配置在該收納體內,具有構成為能以長度方向作為軸芯方向進行旋轉的旋轉軸部,且具有從該旋轉軸部的外周隔著 間隔配置之複數個旋轉葉片;使該旋轉體旋轉的旋轉手段;將欲分離的溶液注入到前述收納空間部的注入部;將自注入部所注入的溶液予以進行離心分離,而使從前述收納空間部的側部分離之流動物連續排出之排出部;及將從前述流動物所分離之剩餘的溶液連續地排出的溶液排出部,在前述離心分離製程,將含有前述萃取並濃縮之牡蠣肉萃取物的溶液由左側管朝送出管可調整送出量地送出,並且從右側管將乙醇溶液可調整送出量地朝前述送出管送出,前述雙方的溶液連續地送出至前述注入部,該連續地送出的雙方溶液儲存在前述收納體內,使前述旋轉體旋轉,進行將收納體內的雙方溶液攪拌並離心分離之作業,藉由前述旋轉,前述流動物被聚集到朝前述收納體的凹陷成三角形之側壁的頂角部分側,當該流動物聚集至凹陷成前述三角形的側壁的頂角部分側時,以作動液進行開閉作動,在凹陷成前述三角形的側壁之頂角部分的圓周方向上,開口形成有隔著預定間隔所設置之複數個排出孔,藉由前述複數個排出孔將前述流動物通過前述排出部而連續地排出至外部,藉由從前述旋轉軸部外周朝外側突出成裙狀所設置之前述複數個旋轉葉片的旋轉,使從前述流動物所分離之剩餘的溶液朝收納體上方移動,由配置在收納體的上方之前述溶液排出部連續排出,前述連續排出的前述剩餘的溶液在濃縮後再次添加預定濃度的乙醇溶液,藉由第2連續離心分離裝置加以分離,再由前述溶液排出部連續排出。 Alternatively, the method for extracting an oyster meat extract comprises: storing the raw oyster meat in an extraction container in which the solution is stored, and extracting the oyster meat extract from the raw oyster meat in the extraction container; a process for concentrating the oyster meat extract extracted by the foregoing extraction process; a stirring process of adding an ethanol solution to the concentrated oyster meat extract and stirring; and concentrating the precipitate obtained after the agitation described above The concentrating process is characterized in that the agitation process is constituted by a centrifugal separation process using a continuous centrifugal separation device having a storage body having a housing space therein, and a rotating body disposed in the rotating body The housing body has a rotating shaft portion that is configured to be rotatable in the axial direction in the longitudinal direction, and has an outer circumference from the rotating shaft portion. a plurality of rotating blades arranged at intervals; a rotating means for rotating the rotating body; an injection portion for injecting the solution to be separated into the storage space portion; and centrifuging the solution injected from the injection portion to be stored from the housing a discharge portion in which the side separated by the side portion of the space portion is continuously discharged; and a solution discharge portion continuously discharging the remaining solution separated from the fluid material, and the oyster meat containing the extracted and concentrated portion is contained in the centrifugal separation process The solution of the extract is sent out by the left side tube to the delivery tube in an adjustable delivery amount, and the ethanol solution is sent from the right side tube to the delivery tube in an adjustable delivery amount, and the both solutions are continuously sent to the injection unit, which continuously The two solutions to be sent are stored in the storage body, the rotating body is rotated, and the two solutions in the storage body are stirred and centrifuged, and the fluid is collected in a recessed shape toward the storage body by the rotation. The apex portion side of the side wall, when the flow is concentrated to the apex angle of the side wall recessed into the aforementioned triangle When the side is divided, the opening and closing operation is performed by the movable liquid, and in the circumferential direction of the apex portion of the side wall recessed into the triangle, the opening is formed with a plurality of discharge holes provided at predetermined intervals, and the plurality of discharge holes are The fluid is continuously discharged to the outside through the discharge portion, and the remaining solution separated from the fluid is separated by the rotation of the plurality of rotating blades provided in a skirt shape from the outer circumference of the rotating shaft portion. Moving toward the upper side of the storage body, the solution discharge unit disposed above the storage body is continuously discharged, and the remaining remaining solution is continuously added, and a predetermined concentration of the ethanol solution is added again, and separated by a second continuous centrifugal separation device. Then, the solution discharge portion is continuously discharged.

或者,前述複數個旋轉葉片係從設在前述軸芯的旋轉軸部的外周朝軸芯方向隔著間隔且呈放射狀突出而形成。 Alternatively, the plurality of rotating blades are formed to protrude radially from the outer circumference of the rotating shaft portion of the shaft core at intervals in the axial direction.

或者,前述旋轉軸部係藉由筒狀構件所構成,內部的中空部作為從注入部所注入的溶液之導入路徑。 Alternatively, the rotating shaft portion is constituted by a tubular member, and the inner hollow portion serves as an introduction path of the solution injected from the injection portion.

若依據本發明之使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法,能夠達到以下的優良效果,亦即,對以往所必須進行的含有牡蠣肉萃取物之溶液的攪拌作業、所謂的基於自然沉澱之沉澱物與不沉澱的上澄清液之分離作業、又從前述各沉澱物及上澄清液萃取出牡蠣肉萃取物的有效成分之萃取作業等的製程,不需要依賴自然沉澱而可強制地予以分離,並且可連續地進行該分離作業,藉此,可大幅地縮短攪拌分離的作業時間,尤其是沉澱物的沉澱時間、也不需進行待機,因此能有效率地進行牡蠣肉萃取物的萃取製造作業。 According to the extraction production method of the oyster meat extract using the continuous centrifugal separation apparatus according to the present invention, the following excellent effects can be obtained, that is, the stirring operation of the solution containing the oyster meat extract which has been conventionally performed, so-called based on The process of separating the precipitate of the natural precipitate from the supernatant without the precipitation, and extracting the active ingredient of the oyster meat extract from each of the above-mentioned precipitates and the supernatant liquid, can be forced without relying on natural precipitation. The separation is carried out continuously, and the separation operation can be continuously performed, whereby the operation time of the stirring and separation can be greatly shortened, in particular, the sedimentation time of the precipitate, and no standby is required, so that the oyster meat extract can be efficiently performed. Extraction manufacturing operations.

1‧‧‧連續離心分離裝置 1‧‧‧Continuous centrifugal separation device

2‧‧‧收納空間部 2‧‧‧Storage Space Department

3‧‧‧收納體 3‧‧‧ 收纳

4‧‧‧旋轉葉片 4‧‧‧Rotating blades

5‧‧‧旋轉體 5‧‧‧Rotating body

6‧‧‧旋轉裝置 6‧‧‧Rotating device

7‧‧‧注入部 7‧‧‧Injection Department

8‧‧‧排出部 8‧‧‧Exporting Department

9‧‧‧剩餘溶液排出部 9‧‧‧Remaining solution discharge

10‧‧‧旋轉軸 10‧‧‧Rotary axis

11‧‧‧旋轉軸部 11‧‧‧Rotary shaft

12‧‧‧流動物 12‧‧‧Mobiles

13‧‧‧注入管 13‧‧‧Injection tube

14‧‧‧送出管 14‧‧‧Send tube

15‧‧‧導入路徑 15‧‧‧Importing path

16‧‧‧排出孔 16‧‧‧Exhaust hole

17‧‧‧送出孔 17‧‧‧Send hole

18‧‧‧作動液 18‧‧‧Working fluid

19‧‧‧剩餘的溶液 19‧‧‧Remaining solution

20‧‧‧萃取容器 20‧‧‧ extraction container

21‧‧‧生牡蠣肉 21‧‧‧ raw oyster meat

22‧‧‧溶液 22‧‧‧solution

23‧‧‧萃取混合溶液 23‧‧‧Extraction mixed solution

24‧‧‧注入管的基端側 24‧‧‧The base end of the injection tube

25‧‧‧左分歧管 25‧‧‧Left manifold

26‧‧‧右分歧管 26‧‧‧Right manifold

27‧‧‧萃取溶液 27‧‧‧ Extraction solution

28‧‧‧乙醇溶液 28‧‧‧Ethanol solution

29‧‧‧控制裝置 29‧‧‧Control device

30‧‧‧開閉構件 30‧‧‧Opening and closing components

31‧‧‧剩餘的溶液的濃縮液 31‧‧‧Concentrate of remaining solution

32‧‧‧旋轉控制部 32‧‧‧Rotation Control Department

33‧‧‧第2連續離心分離裝置 33‧‧‧2nd continuous centrifugal separator

34‧‧‧剩餘的溶液 34‧‧‧Remaining solution

35‧‧‧萃取混合溶液 35‧‧‧Extraction mixed solution

圖1係說明連續離心分離裝置的結構之構成說明圖(其1)。 Fig. 1 is a block diagram showing the structure of a continuous centrifugal separator (1).

圖2係說明連續離心分離裝置的結構之構成說明圖(其2)。 Fig. 2 is a block diagram showing the structure of a continuous centrifugal separator (2).

圖3係說明牡蠣肉萃取物的製造製程之說明圖(其1)。 Fig. 3 is an explanatory view (the 1) of the manufacturing process of the oyster meat extract.

圖4係說明第2連續離心分離裝置的結構之構成說明圖。 Fig. 4 is an explanatory view showing the configuration of the second continuous centrifugal separator.

以下,說明本發明的理想實施例。 Hereinafter, a preferred embodiment of the present invention will be described.

圖1係顯示本發明之連續離心分離裝置1的結構,該連續離心分離裝置1的結構係具有:在內部具有收納空間部2的收納體3;配置在該收納體3內的中央位置,具有以長度方向、在此是垂直方向作為軸芯方向構成為可旋轉的複數個旋轉葉片4之旋轉體5;使該旋轉體5旋轉的旋轉裝置6;將混合有從牡蠣肉進行萃取並將其予以濃縮的牡蠣肉萃取物的萃取溶液27及預定濃度的乙醇溶液28之萃取混合溶液23朝前述收納空間部2連續注入之注入部7;將從注入部7所注入的前述萃取混合溶液23予以離心分離,從前述收納空間部2的側部,將已被分離的流動物12(以往藉由自然沉澱法所獲得之自然沉澱物)連續排出之排出部8;以及將自前述流動物12所分離之剩餘的溶液19(以往藉由自然沉澱物所獲得之上澄清液)連續排出之剩餘溶液排出部9。 Fig. 1 shows a configuration of a continuous centrifugal separator 1 according to the present invention. The continuous centrifugal separator 1 has a structure in which a housing 3 having a housing space 2 therein is disposed, and a central position disposed in the housing 3 has a rotating body 5 constituting a plurality of rotatable rotating blades 4 as a core direction in a longitudinal direction, here a vertical direction; a rotating device 6 for rotating the rotating body 5; and mixing and extracting from oyster meat An extraction solution 27 of the concentrated oyster meat extract 27 and an extraction mixture solution 23 of a predetermined concentration of the ethanol solution 28 are continuously injected into the storage space portion 2; the extraction mixture solution 23 injected from the injection portion 7 is given Centrifugal separation, from the side of the storage space 2, the discharged fluid 12 (the natural sediment obtained by the natural precipitation method) is continuously discharged to the discharge portion 8; and from the fluid 12 The remaining solution 19 (the conventional supernatant obtained by the natural sediment obtained in the past) is continuously discharged to the remaining solution discharge portion 9.

在此,前述旋轉裝置6的結構係具備有:突設於較連續離心分離裝置1的底部略中央更上方的旋轉軸10;及對該旋轉軸10,以長度方向(在本實施例為垂直方向)作為旋轉方向進行旋轉之馬達等的旋轉構件(未圖示)。 Here, the structure of the rotating device 6 is provided with a rotating shaft 10 projecting slightly above the center of the continuous centrifugal separator 1 and a longitudinal direction (vertical in the present embodiment) for the rotating shaft 10 Direction) A rotating member (not shown) such as a motor that rotates in the direction of rotation.

又,在旋轉軸10的前端方向安裝著旋轉體5,此旋 轉體5構成為與旋轉軸10同樣地進行旋轉。旋轉體5係如圖1所示,具備在內部具有中空部且呈圓筒狀的旋轉軸部11,在此旋轉軸部11的外周,各自朝外側突出成裙狀的旋轉葉片4......以朝垂直方向隔著預定的間隔的方式安裝著。 Further, a rotating body 5 is attached to the distal end of the rotating shaft 10, and this rotation The swivel 5 is configured to rotate in the same manner as the rotating shaft 10. As shown in Fig. 1, the rotating body 5 includes a rotating shaft portion 11 having a hollow portion inside and having a cylindrical shape. The rotating shaft portion 11 is formed on the outer circumference of the rotating shaft portion 11 so as to protrude outward in a skirt shape... ... is mounted in a vertical direction with a predetermined interval therebetween.

又,在旋轉軸部11的前端側,插入自上方垂下而設置的管狀注入管13的前端部,在該注入管13與旋轉軸部11之間,構成為既可使旋轉軸部11旋轉又可將注入管13與旋轉軸部11之間加以密閉。 Further, a distal end portion of the tubular injection tube 13 which is provided to hang down from above is inserted into the distal end side of the rotary shaft portion 11, and the rotary shaft portion 11 is rotated between the injection tube 13 and the rotary shaft portion 11 The injection tube 13 and the rotating shaft portion 11 can be sealed.

再者如前述,如圖1所示,自前述注入管13的基端側24,對要進行離心分離的牡蠣肉萃取物的萃取液濃縮的濃縮液(萃取溶液27)添加了預定濃度的乙醇溶液28之萃取混合溶液23從送出管14朝注入管13連續地送出。 Further, as described above, as shown in Fig. 1, a concentrated concentration of ethanol is added to the concentrated liquid (extraction solution 27) from which the extract of the oyster meat extract to be centrifuged is concentrated from the proximal end side 24 of the injection tube 13 The extraction mixed solution 23 of the solution 28 is continuously sent out from the delivery pipe 14 toward the injection pipe 13.

參照圖2進行說明時,在送出管14的上方,自左右方向,左分歧管25與右分歧管26連接成與前述送出管14連通。又,從左分歧管25將前述所萃取的牡蠣肉萃取物之濃縮液(萃取溶液27)連續地送出至送出管14,又,從右分歧管26,將設定成預定濃度的乙醇溶液28連續地送出至送出管14。在此,從左分歧管25送出之所萃取的牡蠣肉萃取物之濃縮液(萃取溶液27)之送出量、和從右分歧管26所連續送出之設定成預定濃度的乙醇溶液28之送出量是藉由控制裝置29加以控制。 Referring to Fig. 2, the left branch pipe 25 and the right branch pipe 26 are connected to the feed pipe 14 from the left and right direction above the delivery pipe 14. Further, the concentrate (extraction solution 27) of the extracted oyster meat extract is continuously sent out from the left branch pipe 25 to the delivery pipe 14, and the ethanol solution 28 set to a predetermined concentration is continuously continuous from the right branch pipe 26. The ground is sent to the delivery pipe 14. Here, the amount of the concentrate of the extracted oyster meat extract (extraction solution 27) sent from the left branch pipe 25, and the amount of the ethanol solution 28 which is continuously fed from the right branch pipe 26 and set to a predetermined concentration are delivered. It is controlled by the control device 29.

亦即,在左分歧管25及右分歧管26分別設有開閉構 件30,藉由來自於控制裝置29的指示,能夠以前述開閉構件30調節從左分歧管25送出之所萃取的牡蠣肉萃取物之濃縮液(萃取溶液27)之送出量、和從右分歧管26所送出之設定成預定濃度的乙醇溶液28之送出量。 That is, the left and right branch pipes 25 and 26 are respectively provided with an opening and closing structure. The member 30 can adjust the delivery amount of the concentrated oyster meat extract (extraction solution 27) sent from the left branch tube 25 by the opening and closing member 30, and the difference from the right side, by the instruction from the control device 29. The amount of the ethanol solution 28 set to a predetermined concentration sent by the tube 26 is sent.

藉此,能夠自由地調節萃取混合溶液23之萃取溶液27與設定成預定濃度的乙醇溶液28之比例。 Thereby, the ratio of the extraction solution 27 of the extraction mixed solution 23 to the ethanol solution 28 set to a predetermined concentration can be freely adjusted.

如此,藉由不僅乙醇溶液的濃度之變更,且可控制萃取溶液27與設定成預定濃度的乙醇溶液28之量的比例,使得能夠控制進行離心分離而採取之牡蠣肉萃取物的有效成分的採取量及能夠採取的有效成分之種類。 Thus, by not only changing the concentration of the ethanol solution, but also controlling the ratio of the extraction solution 27 to the amount of the ethanol solution 28 set to a predetermined concentration, it is possible to control the adoption of the active ingredient of the oyster meat extract taken by centrifugation. The amount and type of active ingredients that can be taken.

又,如前述般,藉由連續的離心分離作業將流動物12(以往的沉澱物)從排出口8連續排出,而將自前述流動物12所分離之剩餘的溶液19(以往的上澄清液)從剩餘溶液排出部9連續排出,但,藉由控制裝置29送出調節牡蠣肉萃取物的濃縮液(萃取溶液27)的送出量和設定成預定濃度的乙醇溶液28的送出量,藉此同步於該等排出量。 Further, as described above, the fluid 12 (conventional precipitate) is continuously discharged from the discharge port 8 by a continuous centrifugal separation operation, and the remaining solution 19 separated from the fluid 12 (the conventional supernatant liquid) The continuous discharge from the remaining solution discharge unit 9 is performed, but the delivery amount of the concentrated liquid (extraction solution 27) for regulating the oyster meat extract and the delivery amount of the ethanol solution 28 set to a predetermined concentration are sent by the control device 29, thereby synchronizing The amount of such emissions.

再者,在進行該調節時,前述控制裝置29藉由感測器檢測被收納於收納體3的萃取混合溶液23的收納量,並檢測顯示此收納量少量化等的檢測訊號,依據該檢測訊號進行調節控制等。 In addition, when the adjustment is performed, the control device 29 detects the storage amount of the extraction mixed solution 23 accommodated in the storage body 3 by the sensor, and detects a detection signal indicating that the storage amount is small, etc., according to the detection. Signal adjustment control, etc.

如此,由注入管13所送來的牡蠣肉萃取物的濃縮液(萃取溶液27)與設定成預定濃度的乙醇溶液28之萃取混合溶液23通過形成在旋轉軸部11的內部之導入路徑 15,自該導入路徑15的下側導入到收納體3內。 In this way, the concentrated solution of the oyster meat extract (extraction solution 27) sent from the injection tube 13 and the extraction mixed solution 23 of the ethanol solution 28 set to a predetermined concentration pass through the introduction path formed inside the rotary shaft portion 11. 15, the lower side of the introduction path 15 is introduced into the storage body 3.

當在收納體3內儲存了預定量的前述萃取混合溶液23時,前述旋轉體5以垂直方向作為旋轉軸進行高速旋轉。在該旋轉體5,如前述般,設有複數片旋轉葉片4......進行以下作業,亦即,此複數個旋轉葉片4......一邊旋轉一邊攪拌收納體3內的萃取混合溶液23並予以離心分離。 When a predetermined amount of the extraction mixed solution 23 is stored in the storage body 3, the rotating body 5 is rotated at a high speed as a rotation axis in the vertical direction. In the rotating body 5, as described above, a plurality of rotating blades 4 are provided to perform the following operations, that is, the plurality of rotating blades 4 are rotated while stirring the inside of the storage body 3. The extraction solution 23 was extracted and centrifuged.

又,以往一般是在攪拌後,等待預定時間讓沉澱物自然沉澱,在自然沉澱結束後,分離成上方上澄清液與沉澱物並取出,但,在此連續離心分離裝置1,前述以往要沉澱之沉澱物藉由旋轉,聚集到收納體3的凹陷成三角形之側壁的頂角部分側,且藉由設在凹陷成三角形的側壁之頂角部分的排出孔16連續地排出至外部。亦即,並非如以往般藉助自然沉澱,而是在短時間內強制地分離成沉澱物與上澄清液者。 Further, in the past, after the stirring, the precipitate is naturally allowed to settle for a predetermined period of time, and after the natural precipitation is completed, the supernatant liquid and the precipitate are separated and taken out, but the centrifugal separator 1 is continuously centrifuged in the past. The precipitate is condensed, gathered to the side of the apex portion of the recessed triangular side wall of the accommodating body 3, and continuously discharged to the outside by the discharge hole 16 provided at the apex portion of the side wall of the recessed triangular shape. That is, it is not forced to separate into a precipitate and a supernatant liquid in a short time by natural precipitation as in the past.

再者,此排出孔16是以複數個的方式,於圓周方向隔著預定間隔設在收納體3的凹陷成三角形之側壁的頂角部分。 Further, the discharge holes 16 are provided in a plurality of manners at the corner portions of the side walls of the storage body 3 which are recessed into triangles at predetermined intervals in the circumferential direction.

前述排出孔16並非一開始就開放。在該排出孔16的附近位置,構成為藉由離心分離操作,使得成為以往的沉澱物之流動物12聚集預定量,當檢測到該量時,例如使作動液18作動,將前述排出孔16進行開閉,又構成為當使排出孔16開口時,前述流動物12可圓滑地排出至外部(參照圖2)。 The aforementioned discharge holes 16 are not opened at the beginning. In the vicinity of the discharge hole 16, the centrifugal separation operation is performed so that the fluid 12 which has become a conventional deposit is aggregated by a predetermined amount, and when the amount is detected, for example, the actuation liquid 18 is actuated, and the discharge hole 16 is opened. When the opening and closing are performed, the fluid 12 can be smoothly discharged to the outside (see FIG. 2).

又,在本發明的連續離心分離裝置1,構成為藉由旋轉控制部32能夠控制前述旋轉體5的旋轉數。 Further, in the continuous centrifugal separator 1 of the present invention, the rotation control unit 32 can control the number of rotations of the rotating body 5.

通常,該連續離心分離裝置1係以例如2000rpm前後的旋轉數進行運轉,但,當作成為該數值以上的旋轉數時,離心加速度急遽地增加,例如得到略8000×g左右的數值,能夠謀求在短時間大量萃取牡蠣肉萃取物的有效成分。 In general, the continuous centrifugal separator 1 is operated at a number of rotations of, for example, 2000 rpm. However, when the number of rotations is equal to or greater than the numerical value, the centrifugal acceleration is rapidly increased, and for example, a numerical value of approximately 8000 × g is obtained, which can be obtained. The active ingredient of the oyster meat extract is extracted in a large amount in a short time.

又,藉由控制前述旋轉數並變更旋轉數,亦可選擇及增減已被分離的流動物12(以往藉由自然沉澱法之自然沉澱物)內所含有之牡蠣肉萃取物的有效成分量、種類等。亦即,這是由於強制地進行離心分離,使得在以往的自然沉澱法也不沉澱之有效成分也能含於前述流動物12內。 Further, by controlling the number of rotations and changing the number of rotations, it is also possible to select and increase or decrease the amount of the active ingredient of the oyster meat extract contained in the separated fluid 12 (conventional natural sediment by natural precipitation method). , types, etc. That is, this is because the centrifugal separation is forcibly performed, so that the active component which is not precipitated by the conventional natural precipitation method can be contained in the fluid 12 as well.

且,自前述流動物12所分離之剩餘的溶液19(以往藉由自然沉澱法之上澄清液)內所含有之牡蠣肉萃取物的有效成分之量、種類等亦可加以選擇、增減變更。 Further, the amount and type of the active ingredient of the oyster meat extract contained in the remaining solution 19 separated from the fluid 12 (conventional liquid by the natural precipitation method) may be selected, increased or decreased. .

在後述的說明可得知,將以連續離心分離強制地分離之前述剩餘的溶液19(以往利用自然沉澱法之上澄清液)進一步濃縮而產生濃縮液,對該濃縮液添加預定濃度之乙醇溶液28,再次使用例如第2連續離心分離裝置33進行離心分離時,在藉由該離心分離之剩餘的溶液34(以往藉由自然沉澱法之上澄清液)內含有大量的抗氧化物質。關於此詳細說明容後再述。 As will be described later, it is understood that the remaining solution 19 (conventionally used in the conventional precipitation method) which is forcibly separated by continuous centrifugation is further concentrated to produce a concentrate, and a predetermined concentration of the ethanol solution is added to the concentrate. When the centrifugal separation is performed again using, for example, the second continuous centrifugal separator 33, a large amount of antioxidant substances are contained in the remaining solution 34 (previously a clear liquid by a natural precipitation method) by the centrifugation. This detailed description will be described later.

在此,簡單說明注入到本發明之連續離心分離裝置1 的牡蠣肉萃取物萃取溶液27之萃取方法。 Here, the injection into the continuous centrifugal separator 1 of the present invention will be briefly described. Extraction method of oyster meat extract extraction solution 27.

首先,如圖3所示,在儲存有水等的溶液22之呈例如所謂半球狀的釜型之萃取容器20內,將剝殼後的生牡蠣肉21以該狀態,亦即,不將剝殼後的生牡蠣肉21粉碎而慎重地予以收納。 First, as shown in FIG. 3, in the extraction container 20 in which a solution 22 containing water or the like is stored, for example, in a so-called hemispherical shape, the raw oyster meat 21 after peeling is in this state, that is, not peeled off. The raw oyster meat 21 after the shell is pulverized and carefully stored.

其次,在前述萃取容器20內,藉由溫熱萃取、常溫粹取,常壓萃取或加壓萃取、減壓萃取等之製程,進行牡蠣肉萃取物萃取製程。 Next, in the extraction container 20, the oyster meat extract extraction process is carried out by a process of warm extraction, normal temperature extraction, atmospheric pressure extraction or pressure extraction, and vacuum extraction.

在此,說明關於在前述萃取選擇製程中選擇加壓萃取之情況。首先,將萃取容器20予以密閉並加壓。 Here, the case where the pressure extraction is selected in the above-described extraction selection process will be described. First, the extraction container 20 is sealed and pressurized.

關於此加壓程度未特別限定,但加壓至1氣壓以上,例如,1.1氣壓至2.5氣壓左右為佳。又,加壓時間也未特別限定,但5至60分鐘左右為佳。又,此時的溫度係75度C至120度C,當被加壓時溫度會上升至常壓時的溫度以上。 Although the degree of pressurization is not particularly limited, it is preferably pressurized to 1 or more, for example, 1.1 to 2.5. Further, the pressurization time is also not particularly limited, but it is preferably about 5 to 60 minutes. Further, the temperature at this time is 75 degrees C to 120 degrees C, and when pressurized, the temperature rises to a temperature higher than the normal pressure.

再者,在進行前述加壓萃取時,為了不讓剝殼後的牡蠣肉受傷,在萃取容器20內不需要進行攪拌。這是由於若依據本發明,即使不進行攪拌亦可有效率地進行萃取。又,當進行攪拌,則會有使要萃取的有效成分受損之虞產生。 Further, in the above-described pressure extraction, in order to prevent the oyster meat after the shelling from being injured, stirring in the extraction container 20 is not required. This is because, according to the present invention, extraction can be carried out efficiently without stirring. Further, when stirring is carried out, there is a possibility that the active ingredient to be extracted is damaged.

如此,從生牡蠣肉可有效率地萃取出各種有效成分。又,前述各種有效成分可有效率地溶出至萃取容器20內的水等之溶液22內。 Thus, various active ingredients can be efficiently extracted from raw oyster meat. Further, the above various active ingredients can be efficiently eluted into the solution 22 of water or the like in the extraction container 20.

比起在一般的常壓下進行萃取之情況,確認到此萃取 量為相當大的增加量。又,比起以往,亦可大幅地縮短萃取時間而萃取到相同量。 This extraction is confirmed compared to the case of extraction under normal atmospheric pressure. The amount is a considerable increase. Moreover, the extraction time can be greatly shortened and extracted to the same amount as compared with the prior art.

其次,將從前述生牡蠣肉21萃取出牡蠣肉萃取物之萃取溶液予以濃縮。 Next, the extract solution of the oyster meat extract is extracted from the raw oyster meat 21 and concentrated.

在此,關於水溶液的濃縮方法未特別限定,能夠將已萃取出的牡蠣肉萃取物濃縮成其固態成分含有量為例如15~45(W/W)%左右。 Here, the method of concentrating the aqueous solution is not particularly limited, and the extracted oyster meat extract can be concentrated to have a solid content of, for example, about 15 to 45 (W/W)%.

又,在進行此濃縮時,通常會提高溫度,在60度至70度的範圍或該溫度以上的高溫進行作業,但若採用減壓低溫加熱濃縮方法,則可在較其低溫下進行作業。 Further, when this concentration is carried out, the temperature is usually raised, and the operation is carried out in the range of 60 to 70 degrees or higher than the temperature. However, if the pressure reduction low temperature heating concentration method is employed, the operation can be performed at a lower temperature.

再者,無論何種濃縮作業,在本發明未被限定,不限於前述減壓低溫加熱濃縮,亦可藉由例如常壓加熱之濃縮,利用膜之濃縮,利用加壓加熱之濃縮等來進行。 Further, the concentration operation is not limited in the present invention, and is not limited to the above-described decompression and low-temperature heating and concentration, and may be carried out by, for example, concentration under normal pressure heating, concentration by a membrane, concentration by pressure heating, or the like. .

對已被濃縮到前述預定濃度的濃縮液添加乙醇溶液,以往必須例如在進行攪拌後經過預定時間,等待牡蠣肉萃取物自然沉澱。但,在本發明,如前述般使用連續離心分離裝置1,強制地予以分離。 The addition of the ethanol solution to the concentrate which has been concentrated to the predetermined concentration described above has conventionally been carried out for a predetermined period of time, for example, after the stirring, and the natural precipitation of the oyster meat extract is waited for. However, in the present invention, the continuous centrifugal separation device 1 is used as described above, and is forcibly separated.

又,連續地採取進行連續離心分離而成為以往的沉澱物之流動物12,使其乾燥而產生牡蠣肉萃取物的乾燥物。 In addition, the fluid 12 which has been subjected to continuous centrifugation and is a conventional precipitate is continuously dried to produce a dried product of the oyster meat extract.

如此,若依據本發明,能夠短時間且連續地進行:胺基乙磺酸、肝醣、蛋白質或含有鋅之所謂抑制血小板的凝結之作用的物質、維他命、其他有益的物質之含有率、萃取度高的牡蠣肉萃取物之萃取、製造(參照圖3)。 Thus, according to the present invention, it is possible to carry out in a short time and continuously: amino ethanesulfonic acid, glycogen, protein or a substance containing zinc, which inhibits the coagulation of platelets, the content of vitamins, other beneficial substances, extraction Extraction and manufacture of high-quality oyster meat extract (see Figure 3).

如此,若依據本發明,藉由使用前述連續離心分離裝置1,能夠在短時間期間大量地進行:胺基乙磺酸、肝醣、蛋白質或含有鋅之所謂抑制血小板的凝結之作用的物質、維他命、其他有益的物質之含有率、萃取度高的牡蠣肉萃取物之萃取、製造。 Thus, according to the present invention, by using the above-described continuous centrifugal separation apparatus 1, it is possible to carry out a large amount of substances in a short period of time: amino ethanesulfonic acid, glycogen, protein or a substance containing zinc which inhibits the coagulation of platelets, Extraction and manufacture of oyster meat extracts with high vitamin and other beneficial substances and high extraction.

又,在本發明的連續離心分離裝置1之離心分離作業,得知在相當於以往沉澱法中的上澄清液之所謂剩餘的溶液19內含有大量的腺苷、抗氧化物質等。因此,如前述般,在本發明,對以連續離心分離裝置1所分離的此剩餘的溶液19,產生濃縮液31,將其送出至如圖4所示的第2連續離心分離裝置33。 Further, in the centrifugal separation operation of the continuous centrifugal separator 1 of the present invention, it is found that a large amount of adenosine, an antioxidant, and the like are contained in the so-called remaining solution 19 corresponding to the supernatant liquid in the conventional precipitation method. Therefore, as described above, in the present invention, the concentrated solution 31 is produced in the remaining solution 19 separated by the continuous centrifugal separator 1, and is sent to the second continuous centrifugal separator 33 shown in Fig. 4 .

參照圖4進行說明時,在此第2連續離心分離裝置33之送出管14的上方,自左右方向,左分歧管25與右分歧管26連接成與前述送出管14連通。又,從左分歧管25,關於前述被離心分離的剩餘的溶液19之濃縮液31朝送出管14連續地送出。又,從右分歧管26,設定成預定濃度例如80%的乙醇溶液28朝送出管14連續地送出。 Referring to Fig. 4, the left branch pipe 25 and the right branch pipe 26 are connected to the feed pipe 14 from the left-right direction above the feed pipe 14 of the second continuous centrifugal separator 33. Further, from the left branch pipe 25, the concentrated liquid 31 of the remaining solution 19 which has been centrifuged is continuously sent to the delivery pipe 14. Further, from the right branch pipe 26, the ethanol solution 28 set to a predetermined concentration, for example, 80%, is continuously sent to the delivery pipe 14.

再者,關於此第2連續離心分離裝置33,也在左分歧管25及右分歧管26分別設有開閉構件30,藉由來自於控制裝置29的指示,能夠送出調節從左分歧管25送出之剩餘的溶液19的濃縮液31之送出量、和從右分歧管26送出之設定成預定濃度的乙醇溶液28之送出量。 Further, in the second continuous centrifugal separator 33, the opening and closing member 30 is also provided in each of the left branch pipe 25 and the right branch pipe 26, and the feed can be sent out from the left branch pipe 25 by an instruction from the control device 29. The amount of the concentrated solution 31 remaining in the solution 19 and the amount of the ethanol solution 28 sent from the right branch pipe 26 set to a predetermined concentration are sent.

又,藉由以第2連續離心分離裝置33所進行之連續的離心分離作業,可將由被進行了離心分離的剩餘的溶液 19之濃縮液31及預定濃度的乙醇溶液28所構成的萃取混合溶液35以該第2連續離心分離裝置33進行離心分離,使得流動物12(以往的沉澱物)從排出部8連續地排出,並且從前述流動物12所離心分離的剩餘的溶液34從剩餘溶液排出部9連續地排出。 Further, the remaining solution subjected to centrifugation can be separated by a continuous centrifugation operation by the second continuous centrifugal separator 33. The extract mixed solution 35 composed of the concentrated liquid 31 of 19 and the ethanol solution 28 of a predetermined concentration is centrifugally separated by the second continuous centrifugal separator 33, so that the fluid 12 (conventional precipitate) is continuously discharged from the discharge unit 8. Further, the remaining solution 34 centrifugally separated from the fluid 12 is continuously discharged from the remaining solution discharge portion 9.

如此,如前述般,相當於以往的上澄清液之剩餘的溶液19被再次濃縮,對該濃縮液31添加預定濃度的乙醇溶液28作成萃取混合溶液34,將其進行複數次連續離心分離。 As described above, the remaining solution 19 corresponding to the conventional supernatant liquid is reconcentrated, and the ethanol solution 28 of a predetermined concentration is added to the concentrate 31 to form the extract mixed solution 34, which is subjected to a plurality of continuous centrifugation.

於是,從相當於以往的上澄清液之剩餘的溶液34,可萃取出含有大量的腺苷、抗氧化物質之牡蠣肉萃取物並加以製造。 Then, the oyster meat extract containing a large amount of adenosine and an antioxidant substance can be extracted and produced from the remaining solution 34 corresponding to the conventional supernatant liquid.

再者,在此實施例,以兩次連續離心分離為例進行了說明,但不限於兩次的離心分離作業,亦可進行兩次以上的連續離心分離作業者。 Further, in this embodiment, the description has been made by taking two continuous centrifugation as an example, but it is not limited to two centrifugation operations, and two or more continuous centrifugation operators may be performed.

1‧‧‧連續離心分離裝置 1‧‧‧Continuous centrifugal separation device

20‧‧‧萃取容器 20‧‧‧ extraction container

21‧‧‧生牡蠣肉 21‧‧‧ raw oyster meat

22‧‧‧溶液 22‧‧‧solution

Claims (4)

一種使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法,該連續離心分離裝置是具有:在內部具有收納空間部的收納體;旋轉體,該旋轉體配置在該收納體內,具有構成為能以長度方向作為軸芯方向進行旋轉的旋轉軸部,且具有從該旋轉軸部的外周隔著間隔配置之複數個旋轉葉片;使該旋轉體旋轉的旋轉手段;將欲分離的溶液連續注入到前述收納空間部的注入部;將自注入部所注入的溶液予以進行離心分離,而使從前述收納空間部的側部分離之流動物連續排出之排出部;及將從前述流動物所分離之剩餘的溶液連續地排出的溶液排出部,其特徵為:從牡蠣肉萃取出牡蠣肉萃取物,將該所萃取的牡蠣肉萃取物予以濃縮,將再對含有前述濃縮後的牡蠣肉萃取物之溶液添加乙醇溶液的攪拌分離製程作為使用前述連續離心分離裝置之離心分離製程,在前述離心分離製程,將含有萃取並濃縮之前述牡蠣肉萃取物的溶液由左側管朝送出管可調整送出量地送出,並且從右側管將乙醇溶液可調節濃度並且可調整送出量地朝前述送出管送出,雙方的溶液連續地送出至前述注入部,該連續地送出的前述雙方的溶液儲存在前述收納體內,使前述旋轉體旋轉,進行將收納體內的雙方溶液攪拌並離心分離之作業, 藉由前述旋轉,前述流動物被聚集到朝前述收納體的凹陷成三角形之側壁的頂角部分側,當預定量的該流動物聚集至凹陷成前述三角形的側壁的頂角部分側時,以作動液進行開閉作動,在凹陷成前述三角形的側壁之頂角部分的圓周方向上,開口形成有隔著預定間隔所設置之複數個排出孔,藉由前述複數個排出孔將前述流動物通過前述排出部而連續地排出至外部,藉由從前述旋轉軸部外周朝外側突出成裙狀所設置之前述複數個旋轉葉片的旋轉,使從前述流動物所分離之剩餘的溶液朝收納體上方移動,由配置在收納體的上方之前述溶液排出部連續排出,前述連續排出的前述剩餘的溶液在濃縮後再次添加預定濃度的乙醇溶液,藉由第2連續離心分離裝置加以分離,再由前述溶液排出部連續排出。 An extraction and manufacturing method of an oyster meat extract using a continuous centrifugal separation apparatus, comprising: a storage body having a storage space portion therein; and a rotating body disposed in the storage body and configured to be capable of a rotating shaft portion that rotates in a longitudinal direction as a core direction, and has a plurality of rotating blades arranged at intervals from an outer circumference of the rotating shaft portion; a rotating means for rotating the rotating body; and continuously injecting the solution to be separated into An injection portion of the storage space portion; a discharge portion that centrifugally separates the solution injected from the injection portion, and continuously discharges the fluid separated from the side portion of the storage space portion; and the separation from the fluid material The solution discharge portion continuously discharged from the remaining solution is characterized in that the oyster meat extract is extracted from the oyster meat, and the extracted oyster meat extract is concentrated, and the oyster meat extract containing the concentrate is further added. A stirring separation process in which a solution is added with an ethanol solution as a centrifugal separation process using the aforementioned continuous centrifugal separation device, before a centrifugation process, the solution containing the extracted and concentrated oyster meat extract is sent from the left side tube to the delivery tube to adjust the delivery amount, and the ethanol solution is adjusted in concentration from the right side tube and the delivery amount can be adjusted toward the aforementioned delivery tube. The two solutions are continuously sent to the injection unit, and the two solutions that are continuously fed are stored in the storage body, and the rotating body is rotated to perform the operation of stirring and centrifuging the both solutions in the storage body. By the aforementioned rotation, the fluid is collected toward the apex portion side toward the side wall of the recessed body which is triangular in shape, and when a predetermined amount of the flow is collected to the side of the apex portion of the side wall of the triangular shape, The actuating liquid is opened and closed, and in the circumferential direction of the apex portion of the side wall recessed into the triangle, the opening is formed with a plurality of discharge holes provided at predetermined intervals, and the flow is passed through the plurality of discharge holes The discharge portion is continuously discharged to the outside, and the remaining solution separated from the fluid object is moved toward the upper side of the storage body by the rotation of the plurality of rotating blades provided in a skirt shape from the outer circumference of the rotating shaft portion. The solution is discharged from the solution discharge unit disposed above the storage body, and the remaining solution continuously discharged is concentrated, and then a predetermined concentration of the ethanol solution is added again, and separated by a second continuous centrifugal separation device, and then the solution is separated. The discharge portion is continuously discharged. 一種使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法,係具有:將生牡蠣肉收納於儲存有溶液的萃取容器內,在該萃取容器內從前述生牡蠣肉萃取牡蠣肉萃取物之萃取製程;將在前述萃取製程所萃取出的牡蠣肉萃取物予以濃縮之製程;對已被濃縮的牡蠣肉萃取物添加乙醇溶液並加以攪拌之攪拌製程;及將在進行前述攪拌後所獲得的沉澱物予以濃縮之濃縮 製程,其特徵為:前述攪拌製程是作為使用連續離心分離裝置的離心分離製程所構成,該連續離心分離裝置是具有:在內部具有收納空間部的收納體;旋轉體,該旋轉體配置在該收納體內,具有構成為能以長度方向作為軸芯方向進行旋轉的旋轉軸部,且具有從該旋轉軸部的外周隔著間隔配置之複數個旋轉葉片;使該旋轉體旋轉的旋轉手段;將欲分離的溶液注入到前述收納空間部的注入部;將自注入部所注入的溶液予以進行離心分離,而使從前述收納空間部的側部分離之流動物連續排出之排出部;及將從前述流動物所分離之剩餘的溶液連續地排出的溶液排出部,在前述離心分離製程,將含有萃取並濃縮之前述牡蠣肉萃取物的溶液由左側管朝送出管可調整送出量地送出,並且從右側管將乙醇溶液可調整送出量地朝前述送出管送出,雙方的溶液連續地送出至前述注入部,該連續地送出的前述雙方的溶液儲存在前述收納體內,使前述旋轉體旋轉,進行將收納體內的雙方溶液攪拌並離心分離之作業,藉由前述旋轉,前述流動物被聚集到朝前述收納體的凹陷成三角形之側壁的頂角部分側,當該流動物聚集至凹陷成前述三角形的側壁的頂角部分側時,以作動液進行開閉作動,在凹陷成前述三角形的側壁之頂角部分的圓周方向上,開口形成有隔著預定間隔 所設置之複數個排出孔,藉由前述複數個排出孔將前述流動物通過前述排出部而連續地排出至外部,藉由從前述旋轉軸部外周朝外側突出成裙狀所設置之前述複數個旋轉葉片的旋轉,使從前述流動物所分離之剩餘的溶液朝收納體上方移動,由配置在收納體的上方之前述溶液排出部連續排出,前述連續排出的前述剩餘的溶液在濃縮後再次添加預定濃度的乙醇溶液,藉由第2連續離心分離裝置加以分離,再由前述溶液排出部連續排出。 An extraction method for extracting oyster meat extract using a continuous centrifugal separation device, comprising: storing raw oyster meat in an extraction container in which a solution is stored, and extracting the oyster meat extract from the raw oyster meat in the extraction container a process of concentrating the oyster meat extract extracted by the foregoing extraction process; a stirring process of adding an ethanol solution to the concentrated oyster meat extract and stirring; and a precipitate obtained after the agitation described above Concentrated The process of the present invention is characterized in that the agitation process is constituted by a centrifugal separation process using a continuous centrifugal separation device having a storage body having a housing space therein, and a rotating body in which the rotating body is disposed The accommodating body has a rotating shaft portion that is configured to be rotatable in the axial direction in the longitudinal direction, and has a plurality of rotating blades arranged at intervals from the outer circumference of the rotating shaft portion; and a rotating means for rotating the rotating body; The solution to be separated is injected into the injection portion of the storage space portion; the solution injected from the injection portion is centrifuged, and the discharge portion separated from the side portion of the storage space portion is continuously discharged; a solution discharge portion in which the remaining solution separated by the fluid is continuously discharged, and the solution containing the extracted and concentrated oyster meat extract is sent out from the left tube to the delivery tube in a predetermined amount by the centrifugation process, and The ethanol solution is sent to the delivery tube by adjusting the delivery amount from the right tube, and the solutions of both sides are continuously sent. In the injection portion, the two solutions that are continuously fed are stored in the storage body, the rotating body is rotated, and the both solutions in the storage body are stirred and centrifuged, and the fluid is collected by the rotation. To the side of the apex portion of the side wall of the recessed body which is formed in a triangular shape toward the storage body, when the fluid is collected to the side of the apex portion of the side wall which is recessed into the triangle, the opening and closing action is performed by the movable liquid, and the side wall of the triangle is recessed In the circumferential direction of the apex portion, the opening is formed with a predetermined interval The plurality of discharge holes are provided, and the plurality of discharge holes are continuously discharged to the outside through the discharge portion, and the plurality of the plurality of discharge holes are protruded outward from the outer circumference of the rotary shaft portion. The rotation of the rotary vane moves the remaining solution separated from the fluid to the upper side of the storage body, and is continuously discharged by the solution discharge unit disposed above the storage body, and the remaining remaining solution is continuously added after concentration. The ethanol solution having a predetermined concentration is separated by a second continuous centrifugal separator, and continuously discharged from the solution discharge portion. 如申請專利範圍第1或2項之使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法,其中,前述複數個旋轉葉片係從設在前述軸芯的旋轉軸部之外周,於軸芯方向上隔著間隔且呈放射狀突出而形成。 The method for extracting oyster meat extract using a continuous centrifugal separator according to the first or second aspect of the invention, wherein the plurality of rotating blades are disposed from the outer circumference of the rotating shaft portion of the shaft core in the axial direction It is formed by being spaced apart from each other and radially protruding. 如申請專利範圍第3項之使用連續離心分離裝置之牡蠣肉萃取物的萃取製造方法,其中,前述旋轉軸部是藉由筒狀構件所構成,內部的中空部作為從注入部所注入的溶液之導入路徑。 The method for producing an oyster meat extract using a continuous centrifugal separator according to the third aspect of the invention, wherein the rotating shaft portion is constituted by a cylindrical member, and the inner hollow portion is a solution injected from the injection portion. The import path.
TW102117374A 2013-05-16 2013-05-16 Method for the preparation of oyster meat extract using continuous centrifugal separation device TWI524849B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
TW102117374A TWI524849B (en) 2013-05-16 2013-05-16 Method for the preparation of oyster meat extract using continuous centrifugal separation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
TW102117374A TWI524849B (en) 2013-05-16 2013-05-16 Method for the preparation of oyster meat extract using continuous centrifugal separation device

Publications (2)

Publication Number Publication Date
TW201444473A TW201444473A (en) 2014-12-01
TWI524849B true TWI524849B (en) 2016-03-11

Family

ID=52706731

Family Applications (1)

Application Number Title Priority Date Filing Date
TW102117374A TWI524849B (en) 2013-05-16 2013-05-16 Method for the preparation of oyster meat extract using continuous centrifugal separation device

Country Status (1)

Country Link
TW (1) TWI524849B (en)

Also Published As

Publication number Publication date
TW201444473A (en) 2014-12-01

Similar Documents

Publication Publication Date Title
WO2007095734A1 (en) Method for increasing the rate and consistency of bioavailability of supplemental dietary ingredients
CN107998333B (en) Preparation method of donkey-hide gelatin peptide product
BR112020007891A2 (en) terpene enrichment methods and systems
JP4697978B2 (en) Method for producing oyster meat extract using continuous centrifuge
TWI524849B (en) Method for the preparation of oyster meat extract using continuous centrifugal separation device
Yang et al. Encapsulation of propolis flavonoids in a water soluble polymer using pressurized carbon dioxide anti-solvent crystallization
CN109393458A (en) A kind of preparation method of Lycium chinense glycopeptide particle electuary
TWI524850B (en) Extraction method of oyster meat extract using decompression or pressurized extraction
CN109169965B (en) Preparation method of ginseng seed oil microcapsule powder
KR20140135086A (en) Method of extracting and manufacturing oyster meat extract using depressurized or pressurized extraction method
CN104397193A (en) Technology and equipment for producing walnut milk by circulating high-micro grinding through slag storage in separate barrels
AU2013206123B2 (en) Method of extracting and manufacturing oyster meat extract using continuous centrifuge
CN209205557U (en) A kind of efficient centrifugal machine
JP4716523B2 (en) Production method of oyster meat extract with adenosine
KR20140134595A (en) Method of extracting and manufacturing oyster meat extract using continuous centrifuge
JP6341497B2 (en) Method for producing oyster meat extract jelly
CN111514112B (en) Method for preparing enteric composite microcapsule by using spray drying technology
CN206508590U (en) A kind of high speed centrifugation atomization combines the alcohol sink device of continuous alcohol precipitation
AU2013206125B2 (en) Method of extracting and manufacturing oyster meat extract using depressurized or pressurized extraction method
CN206508594U (en) A kind of alcohol sink device of pressure type mechanical atomization combination continuous alcohol precipitation
JP2006111619A (en) Food composition containing flower of arrowroot
CN207478029U (en) A kind of extractor suitable for seed material
CN104286872B (en) A kind of natural enteric maca preparation and production method thereof
CN204017679U (en) Supersonic quick firer on a kind of jet uniform filtration device
CN107596728A (en) Using supercritical CO2The method for extracting egg oil