TWI522335B - 用於藉由氫化１，１－二氟－２－硝基乙烷製備２，２－二氟乙基胺之方法 - Google Patents
用於藉由氫化１，１－二氟－２－硝基乙烷製備２，２－二氟乙基胺之方法 Download PDFInfo
- Publication number
- TWI522335B TWI522335B TW099133783A TW99133783A TWI522335B TW I522335 B TWI522335 B TW I522335B TW 099133783 A TW099133783 A TW 099133783A TW 99133783 A TW99133783 A TW 99133783A TW I522335 B TWI522335 B TW I522335B
- Authority
- TW
- Taiwan
- Prior art keywords
- difluoroethylamine
- nitroethane
- catalyst
- difluoro
- acid
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
- C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
- C07C209/34—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
- B01J35/391—Physical properties of the active metal ingredient
- B01J35/392—Metal surface area
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
- C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
- C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
- C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
- C01B3/38—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents using catalysts
- C01B3/40—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents using catalysts characterised by the catalyst
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/10—Catalysts for performing the hydrogen forming reactions
- C01B2203/1041—Composition of the catalyst
- C01B2203/1047—Group VIII metal catalysts
- C01B2203/1052—Nickel or cobalt catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09172271 | 2009-10-06 | ||
| US24981509P | 2009-10-08 | 2009-10-08 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW201130785A TW201130785A (en) | 2011-09-16 |
| TWI522335B true TWI522335B (zh) | 2016-02-21 |
Family
ID=41683260
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW099133783A TWI522335B (zh) | 2009-10-06 | 2010-10-05 | 用於藉由氫化１，１－二氟－２－硝基乙烷製備２，２－二氟乙基胺之方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8754262B2 (enExample) |
| EP (1) | EP2486001B1 (enExample) |
| JP (1) | JP5675826B2 (enExample) |
| KR (1) | KR20120081993A (enExample) |
| CN (1) | CN102548954B (enExample) |
| BR (1) | BR112012006839A2 (enExample) |
| IL (1) | IL218725A (enExample) |
| IN (1) | IN2012DN02643A (enExample) |
| TW (1) | TWI522335B (enExample) |
| WO (1) | WO2011042376A2 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IL305145A (en) | 2021-02-17 | 2023-10-01 | Bayer Ag | A process for the preparation of polyfluoroalkylamines from polyfluoroalkylalcohols |
| CN114682288A (zh) * | 2022-04-11 | 2022-07-01 | 西安凯立新材料股份有限公司 | 芳香硝基化合物氢化用负载型催化剂及其制备方法 |
| CN114835586B (zh) * | 2022-07-04 | 2022-09-13 | 泽升科技(广州)有限公司 | 一种用于n,n-二乙基乙二胺的高效制备方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4030994A (en) | 1971-06-18 | 1977-06-21 | Merck & Co., Inc. | Substitutive fluorination of organic compounds |
| DE3018020A1 (de) * | 1980-05-10 | 1981-11-19 | Bayer Ag, 5090 Leverkusen | Fluorierte azomethine, verfahren zu ihrer herstellung und ihre verwendung als zwischenprodukte |
| FR2497797A1 (fr) * | 1981-01-13 | 1982-07-16 | Synthelabo | Procede de preparation de l'amino-4 butyramide |
| DE3305201A1 (de) | 1983-02-16 | 1984-08-16 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von fluorierten nitroalkanen |
| JPH0931036A (ja) * | 1995-07-19 | 1997-02-04 | Kawaken Fine Chem Co Ltd | ２，７−ジアミノフルオレノンの製造方法 |
| GB0227086D0 (en) * | 2002-11-20 | 2002-12-24 | Exxonmobil Res & Eng Co | Hydrogenation processes |
| US7595400B2 (en) * | 2003-02-21 | 2009-09-29 | Chugai Seiyaku Kabushiki Kaisha | Process for the preparation of hexacyclic compounds |
-
2010
- 2010-10-04 IN IN2643DEN2012 patent/IN2012DN02643A/en unknown
- 2010-10-04 KR KR1020127008032A patent/KR20120081993A/ko not_active Abandoned
- 2010-10-04 CN CN201080042971.2A patent/CN102548954B/zh not_active Expired - Fee Related
- 2010-10-04 WO PCT/EP2010/064700 patent/WO2011042376A2/de not_active Ceased
- 2010-10-04 BR BR112012006839A patent/BR112012006839A2/pt not_active Application Discontinuation
- 2010-10-04 JP JP2012532554A patent/JP5675826B2/ja not_active Expired - Fee Related
- 2010-10-04 EP EP10765776.9A patent/EP2486001B1/de not_active Not-in-force
- 2010-10-05 TW TW099133783A patent/TWI522335B/zh not_active IP Right Cessation
- 2010-10-06 US US12/899,028 patent/US8754262B2/en not_active Expired - Fee Related
-
2012
- 2012-03-19 IL IL218725A patent/IL218725A/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| WO2011042376A3 (de) | 2011-06-30 |
| EP2486001B1 (de) | 2017-03-08 |
| IN2012DN02643A (enExample) | 2015-09-11 |
| CN102548954B (zh) | 2014-04-16 |
| CN102548954A (zh) | 2012-07-04 |
| EP2486001A2 (de) | 2012-08-15 |
| IL218725A0 (en) | 2012-06-28 |
| BR112012006839A2 (pt) | 2016-06-07 |
| WO2011042376A2 (de) | 2011-04-14 |
| JP2013506700A (ja) | 2013-02-28 |
| JP5675826B2 (ja) | 2015-02-25 |
| KR20120081993A (ko) | 2012-07-20 |
| US20110082318A1 (en) | 2011-04-07 |
| TW201130785A (en) | 2011-09-16 |
| IL218725A (en) | 2015-04-30 |
| US8754262B2 (en) | 2014-06-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Annulment or lapse of patent due to non-payment of fees |