TWI480041B - 用於製備吡唑羧醯胺之方法 - Google Patents

用於製備吡唑羧醯胺之方法 Download PDF

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Publication number
TWI480041B
TWI480041B TW100113508A TW100113508A TWI480041B TW I480041 B TWI480041 B TW I480041B TW 100113508 A TW100113508 A TW 100113508A TW 100113508 A TW100113508 A TW 100113508A TW I480041 B TWI480041 B TW I480041B
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TW
Taiwan
Prior art keywords
formula
compound
palladium
ligand
chloro
Prior art date
Application number
TW100113508A
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English (en)
Chinese (zh)
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TW201210590A (en
Inventor
浮羅倫 史雷斯
湯瑪斯 凡特吉
麥可 羅摩
漢斯 托比勒
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先正達合夥公司
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Publication of TW201210590A publication Critical patent/TW201210590A/zh
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Publication of TWI480041B publication Critical patent/TWI480041B/zh

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/26Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/2635Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions involving a phosphorus compound, e.g. Wittig synthesis
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/26Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/30Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by a Diels-Alder synthesis
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/35Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction
    • C07C17/354Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction by hydrogenation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C25/00Compounds containing at least one halogen atom bound to a six-membered aromatic ring
    • C07C25/24Halogenated aromatic hydrocarbons with unsaturated side chains

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Catalysts (AREA)
TW100113508A 2010-04-20 2011-04-19 用於製備吡唑羧醯胺之方法 TWI480041B (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP10160439 2010-04-20

Publications (2)

Publication Number Publication Date
TW201210590A TW201210590A (en) 2012-03-16
TWI480041B true TWI480041B (zh) 2015-04-11

Family

ID=43984050

Family Applications (1)

Application Number Title Priority Date Filing Date
TW100113508A TWI480041B (zh) 2010-04-20 2011-04-19 用於製備吡唑羧醯胺之方法

Country Status (13)

Country Link
US (1) US8524915B2 (https=)
EP (1) EP2560960B1 (https=)
JP (1) JP6153864B2 (https=)
CN (1) CN102858749B (https=)
AR (1) AR080923A1 (https=)
BR (1) BR112012026456B1 (https=)
ES (1) ES2458935T3 (https=)
IL (1) IL222400A (https=)
MX (1) MX2012012009A (https=)
PY (1) PY1115669A (https=)
TW (1) TWI480041B (https=)
UY (1) UY33341A (https=)
WO (1) WO2011131544A1 (https=)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI534126B (zh) * 2011-01-25 2016-05-21 先正達合夥公司 用於製備吡唑羧酸醯胺之方法
CN103483407B (zh) * 2013-10-10 2015-11-18 宁夏启元药业有限公司 一种硫氰酸红霉素萃取结晶用复合溶媒及萃取结晶方法
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
CN105985254B (zh) * 2015-02-17 2018-03-16 上海中科绿碳化工科技有限公司 一种制备甲酰胺类化合物的方法
CN106588745B (zh) * 2016-12-02 2019-06-14 杭州百昂锐地科技有限公司 一种苯并烯氟菌唑的中间体及其制备方法和应用
KR20250036910A (ko) 2022-07-22 2025-03-14 신젠타 크롭 프로텍션 아게 이종환식 아미드 유도체의 고체 형태
PY2503719A (es) 2024-01-26 2025-08-05 Syngenta Crop Protection Ag Proceso químico

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007048556A1 (en) * 2005-10-25 2007-05-03 Syngenta Participations Ag Heterocyclic amide derivatives useful as microbiocides
WO2007068417A2 (en) * 2005-12-12 2007-06-21 Syngenta Participations Ag Process for the preparation of amines
TWI428325B (zh) * 2010-04-20 2014-03-01 先正達合夥公司 製備吡唑羧醯胺之方法

Family Cites Families (9)

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Publication number Priority date Publication date Assignee Title
JPH075487B2 (ja) 1985-11-14 1995-01-25 住友化学工業株式会社 1―ブロモ―2―クロロ―4―フルオロベンゼンの製造法
US5093347A (en) 1991-01-28 1992-03-03 Monsanto Company 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use
US7223879B2 (en) 1998-07-10 2007-05-29 Massachusetts Institute Of Technology Ligands for metals and improved metal-catalyzed processes based thereon
CN101528034B (zh) 2006-10-25 2011-11-09 辛根塔有限公司 生产经取代的溴苯的方法
MX2010011790A (es) * 2008-05-14 2010-11-25 Syngenta Ltd Proceso para la preparacion de amidas.
BRPI0923527A2 (pt) * 2008-12-24 2016-08-09 Syngenta Ltd métodos de preparo de fungicidas
BR112012024705A2 (pt) * 2010-03-31 2016-06-07 Actelion Pharmaceuticals Ltd derivados antibacterianos de isoquinolin-3-ilureia
WO2011131546A1 (en) * 2010-04-20 2011-10-27 Syngenta Participations Ag Process for the preparation of pyrazole carboxylic acid amides
JP5684895B2 (ja) * 2010-04-20 2015-03-18 シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト ピラゾールカルボン酸アミドの調製方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007048556A1 (en) * 2005-10-25 2007-05-03 Syngenta Participations Ag Heterocyclic amide derivatives useful as microbiocides
WO2007068417A2 (en) * 2005-12-12 2007-06-21 Syngenta Participations Ag Process for the preparation of amines
TWI428325B (zh) * 2010-04-20 2014-03-01 先正達合夥公司 製備吡唑羧醯胺之方法

Also Published As

Publication number Publication date
US8524915B2 (en) 2013-09-03
AR080923A1 (es) 2012-05-16
PY1115669A (es) 2014-09-01
BR112012026456A2 (pt) 2015-09-08
BR112012026456B1 (pt) 2017-06-27
US20130041160A1 (en) 2013-02-14
WO2011131544A1 (en) 2011-10-27
UY33341A (es) 2011-12-01
EP2560960A1 (en) 2013-02-27
EP2560960B1 (en) 2014-02-26
CN102858749A (zh) 2013-01-02
IL222400A (en) 2015-04-30
MX2012012009A (es) 2012-12-17
JP2013527840A (ja) 2013-07-04
ES2458935T3 (es) 2014-05-07
TW201210590A (en) 2012-03-16
CN102858749B (zh) 2014-07-02
JP6153864B2 (ja) 2017-06-28

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