TWI331989B - Separation of triethanolamine from a mixture obtained by reaction of ammonia with ethylene oxide - Google Patents

Separation of triethanolamine from a mixture obtained by reaction of ammonia with ethylene oxide Download PDF

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Publication number
TWI331989B
TWI331989B TW093129661A TW93129661A TWI331989B TW I331989 B TWI331989 B TW I331989B TW 093129661 A TW093129661 A TW 093129661A TW 93129661 A TW93129661 A TW 93129661A TW I331989 B TWI331989 B TW I331989B
Authority
TW
Taiwan
Prior art keywords
mixture
column
triethanolamine
tea
ethanolamine
Prior art date
Application number
TW093129661A
Other languages
English (en)
Chinese (zh)
Other versions
TW200523233A (en
Inventor
Wolfgang Reif
Hans Hammer
Guenther Ruider
Anton Meier
Philip Buskens
Matthias Frauenkron
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of TW200523233A publication Critical patent/TW200523233A/zh
Application granted granted Critical
Publication of TWI331989B publication Critical patent/TWI331989B/zh

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/12Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic the nitrogen atom of the amino group being further bound to hydrocarbon groups substituted by hydroxy groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
TW093129661A 2003-10-08 2004-09-30 Separation of triethanolamine from a mixture obtained by reaction of ammonia with ethylene oxide TWI331989B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10346779A DE10346779A1 (de) 2003-10-08 2003-10-08 Verfahren zur Abtrennung von Triethanolamin aus einem durch die Umsetzung von Ammoniak mit Ethylenoxid erhaltenen Stoffgemisch

Publications (2)

Publication Number Publication Date
TW200523233A TW200523233A (en) 2005-07-16
TWI331989B true TWI331989B (en) 2010-10-21

Family

ID=34428244

Family Applications (1)

Application Number Title Priority Date Filing Date
TW093129661A TWI331989B (en) 2003-10-08 2004-09-30 Separation of triethanolamine from a mixture obtained by reaction of ammonia with ethylene oxide

Country Status (13)

Country Link
US (1) US7279602B2 (de)
EP (1) EP1675816B1 (de)
JP (1) JP4471976B2 (de)
KR (1) KR101036382B1 (de)
CN (1) CN100364960C (de)
AT (1) ATE365153T1 (de)
CA (1) CA2540246C (de)
DE (2) DE10346779A1 (de)
ES (1) ES2286669T3 (de)
MX (1) MXPA06003484A (de)
MY (1) MY138351A (de)
TW (1) TWI331989B (de)
WO (1) WO2005035481A2 (de)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101139296B (zh) * 2007-09-29 2010-05-26 吴兆立 增设气提拔头段的乙醇胺蒸馏的方法
JP5528454B2 (ja) 2008-09-17 2014-06-25 ビーエーエスエフ ソシエタス・ヨーロピア 1つまたはそれより多くのアルカノールアミンを含有する混合物を連続的に蒸留分離するための装置および方法
JP2012512826A (ja) * 2008-12-19 2012-06-07 ビーエーエスエフ ソシエタス・ヨーロピア 純粋なトリエタノールアミン(teoa)の製造法
WO2013095810A1 (en) 2011-12-22 2013-06-27 Dow Global Technologies Llc Reductive amination of diethanolamine and resulting product mixture
CN103271238B (zh) * 2013-05-10 2014-04-02 中国科学院亚热带农业生态研究所 一种饲料添加剂一乙醇胺的制备方法及应用
EP3126323B1 (de) * 2014-04-04 2021-12-15 SABIC Global Technologies B.V. Minimierung des wassergehalts in ethanolaminproduktströmen
WO2015155667A1 (en) * 2014-04-08 2015-10-15 Sabic Global Technologies B.V. Minimizing water content in ethanolamine product streams
CN106458848A (zh) 2014-05-27 2017-02-22 沙特基础工业全球技术有限公司 不存在与纯剪切的dea 99%混合的情况下直接生产tea 85%
EP3148964A1 (de) 2014-05-30 2017-04-05 SABIC Global Technologies B.V. Verbesserte qualität und farbe von ethanolaminproduktströmen mit reduzierter temperatur an der triethanolaminsäule
US10662144B2 (en) 2015-12-11 2020-05-26 Sabic Global Technologies B.V. Method of reducing color in alkanolamine compositions and compositions produced thereby
US11203568B2 (en) 2015-12-29 2021-12-21 Sabic Global Technologies B.V. Methods of reducing color in alkanolamine compositions and compositions produced thereby
CN114276255A (zh) * 2021-12-17 2022-04-05 湖北仙粼化工有限公司 一种乙醇胺多段管式反应节能生产系统及生产工艺

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1968512A (en) * 1931-12-07 1934-07-31 Carbide & Carbon Chem Corp Process for purifying liquids
US3453183A (en) * 1964-12-29 1969-07-01 Nippon Catalytic Chem Ind Method of purifying ethanolamines
US3742059A (en) * 1971-05-24 1973-06-26 Dow Chemical Co Color-stabilized alkanolamines
IT967651B (it) * 1972-09-20 1974-03-11 Sir Soc Italiana Resine Spa Perfezionamenti nei procedimenti per la preparazione di etanolam mine
US4381223A (en) * 1981-09-30 1983-04-26 Union Carbide Corporation Process for the treatment of organic amine compositions
JPS6219558A (ja) 1985-07-19 1987-01-28 Mitsui Toatsu Chem Inc 安定化高品質トリエタノ−ルアミンの製造方法
US4673762A (en) * 1986-05-27 1987-06-16 Texaco Inc. Decolorizing ethanolamines with alkylene oxides
FR2804109B1 (fr) * 2000-01-24 2002-08-16 Bp Chemicals Snc Procede de fabrication en continu de triethanolamine, et produit obtenu
DE10011942A1 (de) * 2000-03-11 2001-09-13 Basf Ag Verfahren zur Herstellung von Alkanolaminen mit verbesserter Farbqualität
TWI303242B (en) * 2003-02-03 2008-11-21 Nippon Catalytic Chem Ind Process for producing high purity trialkanolamine

Also Published As

Publication number Publication date
KR20060120026A (ko) 2006-11-24
WO2005035481A3 (de) 2005-06-02
ATE365153T1 (de) 2007-07-15
TW200523233A (en) 2005-07-16
ES2286669T3 (es) 2007-12-01
CA2540246A1 (en) 2005-04-21
WO2005035481A2 (de) 2005-04-21
US7279602B2 (en) 2007-10-09
MXPA06003484A (es) 2006-06-08
US20060293541A1 (en) 2006-12-28
JP2007508257A (ja) 2007-04-05
EP1675816B1 (de) 2007-06-20
MY138351A (en) 2009-05-29
KR101036382B1 (ko) 2011-05-23
CN100364960C (zh) 2008-01-30
CA2540246C (en) 2011-06-07
DE10346779A1 (de) 2005-05-12
DE502004004156D1 (de) 2007-08-02
EP1675816A2 (de) 2006-07-05
CN1863761A (zh) 2006-11-15
JP4471976B2 (ja) 2010-06-02

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TWI331989B (en) Separation of triethanolamine from a mixture obtained by reaction of ammonia with ethylene oxide
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MM4A Annulment or lapse of patent due to non-payment of fees