TW201612149A - Process for preparing terephthalic diesters with circulation of the reaction mixture - Google Patents

Process for preparing terephthalic diesters with circulation of the reaction mixture

Info

Publication number
TW201612149A
TW201612149A TW104131412A TW104131412A TW201612149A TW 201612149 A TW201612149 A TW 201612149A TW 104131412 A TW104131412 A TW 104131412A TW 104131412 A TW104131412 A TW 104131412A TW 201612149 A TW201612149 A TW 201612149A
Authority
TW
Taiwan
Prior art keywords
reactor
stream
reaction
alcohol
suspension
Prior art date
Application number
TW104131412A
Other languages
English (en)
Inventor
Armin Schraut
Martin Kaller
Rob Bronneberg
Jasmin Stammer
Martin Das
Gerrit Harnischmacher
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of TW201612149A publication Critical patent/TW201612149A/zh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80—Phthalic acid esters
    • C07C69/82—Terephthalic acid esters
TW104131412A 2014-09-24 2015-09-23 Process for preparing terephthalic diesters with circulation of the reaction mixture TW201612149A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP14186141 2014-09-24

Publications (1)

Publication Number Publication Date
TW201612149A true TW201612149A (en) 2016-04-01

Family

ID=51660313

Family Applications (1)

Application Number Title Priority Date Filing Date
TW104131412A TW201612149A (en) 2014-09-24 2015-09-23 Process for preparing terephthalic diesters with circulation of the reaction mixture

Country Status (12)

Country Link
US (1) US10239818B2 (zh)
EP (1) EP3197858B1 (zh)
CN (1) CN107074720B (zh)
BR (1) BR112017005858A2 (zh)
CA (1) CA2962162A1 (zh)
ES (1) ES2724981T3 (zh)
MX (1) MX2017003925A (zh)
PL (1) PL3197858T3 (zh)
RU (1) RU2668964C1 (zh)
TR (1) TR201905052T4 (zh)
TW (1) TW201612149A (zh)
WO (1) WO2016046117A1 (zh)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6813562B6 (ja) 2015-07-09 2021-02-10 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ 硬化性組成物
KR20210033857A (ko) 2019-09-19 2021-03-29 주식회사 엘지화학 에스터화 생성물의 중화/수분리 장치 및 에스터화 생성물의 중화/수분리 방법

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB798439A (en) 1954-10-26 1958-07-23 Bayer Ag Process for the manufacture of terephthalic acid dimethyl ester
US3927982A (en) * 1970-03-18 1975-12-23 Du Pont Recirculating apparatus for continuous esterification reactions
BR8103970A (pt) 1980-10-20 1982-08-24 Ad Ind Inc Processo para remocao de vapor de agua de etanol gasoso
GB2088739B (en) 1980-11-28 1983-11-30 Coal Industry Patents Ltd Drying organic solvents
US4372857A (en) 1981-03-05 1983-02-08 Union Carbide Corporation Liquid adsorption process and apparatus
US4465875A (en) 1982-09-27 1984-08-14 Calgon Carbon Corporation Process for dehydrating ethanol
US4487614A (en) 1983-11-16 1984-12-11 Union Carbide Corporation Adsorption separation cycle
GB2151501A (en) 1983-12-22 1985-07-24 Coal Ind Continuous sorption process
US4726818A (en) 1984-12-20 1988-02-23 Union Carbide Corporation Bulk removal of water from organic liquids
GB8601082D0 (en) 1986-01-17 1986-02-19 Distillers Co Carbon Dioxide Potable spirit production
DE69012682T2 (de) 1989-06-12 1995-04-06 Merck & Co Inc Verfahren zur Entfernung von bakteriellen Endotoxinen aus gram-negativen Polysacchariden.
JPH04308543A (ja) 1991-04-06 1992-10-30 Kobe Steel Ltd 含水エタノールの精製方法
AU684134B2 (en) 1994-02-07 1997-12-04 Qiagen Gmbh Nucleic acid transfection efficiency increase by use of isopropanol in aqueous solutions
FR2719039B1 (fr) 1994-04-22 1996-06-21 Interis Nouveau procédé de déshydratation d'alcool par adsorption/regénération sur tamis moléculaire, et installation pour sa mise en Óoeuvre.
WO1999063076A1 (en) 1998-06-01 1999-12-09 The Immune Response Corporation Novel method of large scale plasmid purification
DE10043545A1 (de) * 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10056179A1 (de) 2000-11-13 2002-05-29 Basf Ag Verfahren zur Herstellung von Estern mehrbasiger Säuren
JP4996791B2 (ja) 2001-03-14 2012-08-08 Ｊｎｃ株式会社 エンドトキシン吸着体、及びそれを用いたエンドトキシンの除去方法
WO2005003152A1 (en) 2003-06-24 2005-01-13 Akzo Nobel N.V. Removal of lipopolysacchrarides from protein- lipopolysaccharide complexes by nonflammable solvents
US7531308B2 (en) 2004-04-23 2009-05-12 Sigma-Aldrich Co. Process for the reduction of endotoxins in a plasmid preparation using a carbohydrate non-ionic detergent with silica chromatography
US7276621B2 (en) 2005-08-12 2007-10-02 Eastman Chemical Company Production of di-(2-ethylhexyl) terephthalate
US7799942B2 (en) * 2005-08-12 2010-09-21 Eastman Chemical Company Production of terephthalic acid di-esters
JP4956945B2 (ja) * 2005-09-12 2012-06-20 三菱化学株式会社 テレフタル酸ジエステルの製造方法
WO2007115046A1 (en) 2006-03-31 2007-10-11 Invitrogen Corporation Low-endotoxin nucleic acid preparations
CL2007002615A1 (es) 2006-09-08 2008-04-18 Wyeth Corp Metodos para aislar o purificar un producto que comprende poner el producto enlazado en contacto con al menos una solucion de lavado que comprende arginina y luego eluir el producto; y dicho producto.
US7943094B2 (en) * 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
US8034970B2 (en) * 2007-06-27 2011-10-11 H R D Corporation Method of making phthalic acid diesters
CA2746599A1 (en) 2008-12-16 2010-07-08 Basf Se Process for the preparation of esters with recirculation of alcohol
KR101346396B1 (ko) 2008-12-16 2014-01-02 바스프 에스이 조 에스테르의 재생 방법
CN102958898B (zh) 2010-08-25 2015-05-20 埃克森美孚化学专利公司 酯的制备方法
TWI654177B (zh) 2013-10-31 2019-03-21 德商巴斯夫歐洲公司 製備羧酸酯的方法及其作爲塑化劑的用途
JP2017517496A (ja) 2014-04-22 2017-06-29 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ イオン液体及び酸性エステル化触媒の存在下でのカルボン酸エステルの製造方法並びにその可塑剤としての使用

Also Published As

Publication number Publication date
MX2017003925A (es) 2017-06-30
PL3197858T3 (pl) 2019-08-30
ES2724981T3 (es) 2019-09-18
RU2668964C1 (ru) 2018-10-05
TR201905052T4 (tr) 2019-05-21
EP3197858B1 (de) 2019-02-06
CN107074720B (zh) 2021-01-08
CN107074720A (zh) 2017-08-18
US20170297996A1 (en) 2017-10-19
US10239818B2 (en) 2019-03-26
BR112017005858A2 (pt) 2018-02-06
CA2962162A1 (en) 2016-03-31
EP3197858A1 (de) 2017-08-02
WO2016046117A1 (de) 2016-03-31

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