TR201903360T4 - Bir polikarbodiimid polimer hazırlama yöntemi ve bu şekilde hazırlanan polikarbodiimid polimer. - Google Patents

Bir polikarbodiimid polimer hazırlama yöntemi ve bu şekilde hazırlanan polikarbodiimid polimer. Download PDF

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Publication number
TR201903360T4
TR201903360T4 TR2019/03360T TR201903360T TR201903360T4 TR 201903360 T4 TR201903360 T4 TR 201903360T4 TR 2019/03360 T TR2019/03360 T TR 2019/03360T TR 201903360 T TR201903360 T TR 201903360T TR 201903360 T4 TR201903360 T4 TR 201903360T4
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TR
Turkey
Prior art keywords
polycarbodiimide polymer
compound
polycarbodiimide
precursor compound
temperature
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TR2019/03360T
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English (en)
Inventor
Williams-Harry Michele
Kumar Rajesh
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Basf Se
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Publication of TR201903360T4 publication Critical patent/TR201903360T4/tr

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
    • C08G18/025—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only the polymeric products containing carbodiimide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C267/00—Carbodiimides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C271/00—Derivatives of carbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
    • C07C271/06—Esters of carbamic acids
    • C07C271/08—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms
    • C07C271/26—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atom of at least one of the carbamate groups bound to a carbon atom of a six-membered aromatic ring
    • C07C271/28—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atom of at least one of the carbamate groups bound to a carbon atom of a six-membered aromatic ring to a carbon atom of a non-condensed six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
    • C08G18/095—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture oligomerisation to carbodiimide or uretone-imine groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/285—Nitrogen containing compounds
    • C08G18/2865—Compounds having only one primary or secondary amino group; Ammonia
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3855—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur
    • C08G18/3876—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur containing mercapto groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/71—Monoisocyanates or monoisothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
    • C08G18/7621—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring being toluene diisocyanate including isomer mixtures
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/13—Phenols; Phenolates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/51—Phosphorus bound to oxygen
    • C08K5/53—Phosphorus bound to oxygen bound to oxygen and to carbon only
    • C08K5/5313—Phosphinic compounds, e.g. R2=P(:O)OR'

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyurethanes Or Polyureas (AREA)

Abstract

Buluş, bir polikarbodiimid polimer üretmeye ilişkin bir yöntem ve daha spesifik olarak moleküler ağırlık dağılımında düşük bir varyasyona sahip olan ve daha az yan ürün ile sonuçlanan bir polikarbodiimid polimer üretmeye ilişkin bir yöntem ile ilgilidir. Bir karbodiimid bileşiği içeren bir prekürsör bileşiğin istenen bir sıcaklığa ısıtılması; prekürsör bileşiğinin, bir diizosiyanat bileşiğinin ve bir karbodiimidizasyon katalizörünün bir reaksiyon karışımı oluşturmak için kombine edilmesi; ve reaksiyon karışımının 0'dan fazla ila 18 saat aralığındaki bir birinci zaman periyodu boyunca bir birinci sıcaklığa ısıtılması, böylelikle prekürsör bileşiğin ve diizosiyanat bileşiğinin polikarbodiimid polimer üretmek için karbodiimidizasyon katalizörünün mevcudiyetinde reaksiyona sokulması işlem adımlarının yer aldığı bu yöntemde istenen sıcaklık ve birinci sıcaklığın her biri bağımsız olarak 70 ve 150 °C arasındadır ve prekürsör bileşik tekli karbodiimid bağına sahip olan bir karbodiimid bileşiğidir.
TR2019/03360T 2014-02-14 2015-05-12 Bir polikarbodiimid polimer hazırlama yöntemi ve bu şekilde hazırlanan polikarbodiimid polimer. TR201903360T4 (tr)

Applications Claiming Priority (1)

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US201461940049P 2014-02-14 2014-02-14

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TR201903360T4 true TR201903360T4 (tr) 2019-04-22

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TR2019/03360T TR201903360T4 (tr) 2014-02-14 2015-05-12 Bir polikarbodiimid polimer hazırlama yöntemi ve bu şekilde hazırlanan polikarbodiimid polimer.

Country Status (11)

Country Link
US (1) US10457767B2 (tr)
EP (1) EP3105275B1 (tr)
JP (1) JP6676533B2 (tr)
KR (1) KR102333130B1 (tr)
CN (1) CN106164123B (tr)
CA (1) CA2939503A1 (tr)
ES (1) ES2719411T3 (tr)
PL (1) PL3105275T3 (tr)
TR (1) TR201903360T4 (tr)
TW (1) TWI659049B (tr)
WO (1) WO2015123416A1 (tr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
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WO2017119443A1 (ja) * 2016-01-05 2017-07-13 三井化学株式会社 ポリカルボジイミド組成物、ポリカルボジイミド組成物の製造方法、水分散組成物、溶液組成物、樹脂組成物および樹脂硬化物
CN113544231A (zh) 2019-03-07 2021-10-22 巴斯夫欧洲公司 基于碳二亚胺化学的胶粘剂
CN111662328B (zh) * 2020-06-12 2021-10-15 万华节能科技集团股份有限公司 阻燃环保甲苯二异氰酸酯的衍生物及其合成方法
KR20240058934A (ko) 2021-09-17 2024-05-03 바스프 에스이 폴리카보디이미드 경화 중합체의 제조를 위한 원-팟 방법
KR102656558B1 (ko) * 2023-02-06 2024-04-09 동우 화인켐 주식회사 퍼플루오로폴리에테르기 함유 아크릴 화합물 및 이를 포함하는 조성물

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Also Published As

Publication number Publication date
EP3105275A1 (en) 2016-12-21
ES2719411T3 (es) 2019-07-10
TWI659049B (zh) 2019-05-11
EP3105275B1 (en) 2019-01-09
US20170166678A1 (en) 2017-06-15
JP6676533B2 (ja) 2020-04-08
JP2017507212A (ja) 2017-03-16
CN106164123A (zh) 2016-11-23
US10457767B2 (en) 2019-10-29
KR20160122201A (ko) 2016-10-21
KR102333130B1 (ko) 2021-12-01
WO2015123416A1 (en) 2015-08-20
TW201538555A (zh) 2015-10-16
PL3105275T3 (pl) 2019-07-31
CA2939503A1 (en) 2015-08-20
CN106164123B (zh) 2019-04-16

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