TR201801232T1 - Söndürme kolonunda pH kontrolü. - Google Patents

Söndürme kolonunda pH kontrolü. Download PDF

Info

Publication number
TR201801232T1
TR201801232T1 TR2018/01232T TR201801232T TR201801232T1 TR 201801232 T1 TR201801232 T1 TR 201801232T1 TR 2018/01232 T TR2018/01232 T TR 2018/01232T TR 201801232 T TR201801232 T TR 201801232T TR 201801232 T1 TR201801232 T1 TR 201801232T1
Authority
TR
Turkey
Prior art keywords
column
quench
control
condensate
quenching column
Prior art date
Application number
TR2018/01232T
Other languages
English (en)
Inventor
Robert Mcdonel Timothy
Robert Couch Jay
George Travers Thomas
Rudolph Wagner David
Trigg Wachtendorf Paul
Original Assignee
Ineos Europe Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ineos Europe Ag filed Critical Ineos Europe Ag
Publication of TR201801232T1 publication Critical patent/TR201801232T1/tr

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
    • G—PHYSICS
    • G05—CONTROLLING; REGULATING
    • G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D21/00—Control of chemical or physico-chemical variables, e.g. pH value
    • G05D21/02—Control of chemical or physico-chemical variables, e.g. pH value characterised by the use of electric means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42—Regulation; Control
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
    • B01D5/003—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium within column(s)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0033—Other features
    • B01D5/0051—Regulation processes; Control systems, e.g. valves
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/06—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms of an acyclic and unsaturated carbon skeleton
    • C07C255/07—Mononitriles
    • C07C255/08—Acrylonitrile; Methacrylonitrile

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Control Of Non-Electrical Variables (AREA)
  • Treating Waste Gases (AREA)

Abstract

Söndürme kolonu pH?ının kontrol altına alınması için bir işlem bir veya daha fazla söndürme kolonuna ait bir söndürme kolonu atığında pH?ın kontrol altına alınması için söndürme kolonuna asit eklenmesini içerir. Bir yönü itibarıyla işlem söndürme kolonu kondensatına ait bir pH?ın ölçülmesini ve kondensatta yaklaşık 3.5 ila yaklaşık 7 pH?ın sağlanması için söndürme kolonuna eklenecek bir asit miktarının ayarlanmasını içerir. Kondensat pH?ının ölçülmesi söndürme kolonuna asit ilavesinin kontrol altına alınması için tutarlı ve hatasız bir usul sağlar.
TR2018/01232T 2015-08-03 2016-07-28 Söndürme kolonunda pH kontrolü. TR201801232T1 (tr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN201510467179.6A CN105425849B (zh) 2015-08-03 2015-08-03 急冷塔pH控制
PCT/US2016/044374 WO2017023663A1 (en) 2015-08-03 2016-07-28 Quench column ph control

Publications (1)

Publication Number Publication Date
TR201801232T1 true TR201801232T1 (tr) 2018-03-21

Family

ID=55504116

Family Applications (1)

Application Number Title Priority Date Filing Date
TR2018/01232T TR201801232T1 (tr) 2015-08-03 2016-07-28 Söndürme kolonunda pH kontrolü.

Country Status (5)

Country Link
CN (1) CN105425849B (tr)
RU (1) RU2720311C2 (tr)
SA (1) SA518390859B1 (tr)
TR (1) TR201801232T1 (tr)
WO (1) WO2017023663A1 (tr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107941039B (zh) * 2016-10-12 2020-03-03 英尼奥斯欧洲股份公司 骤冷塔后冷却器
CN112439308A (zh) * 2019-09-05 2021-03-05 中石油吉林化工工程有限公司 去除丙烯腈装置急冷塔塔顶气相中酸性液体的方法

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1020088A (en) * 1964-01-22 1966-02-16 Electro Chimie Metal Improvements in or relating to the recovery and purification of acrylonitrile
US4503001A (en) 1970-10-30 1985-03-05 Standard Oil Company (Indiana) Process for the manufacture of acrylonitrile and methacrylonitrile
US4767878A (en) 1971-02-04 1988-08-30 The Standard Oil Company Process for the manufacture of acrylonitrile and methacrylonitrile
US4863891A (en) 1971-02-04 1989-09-05 The Standard Oil Company Catalyst for the manufacture of acrylonitrile and methacrylonitrile
US5093299A (en) 1990-01-09 1992-03-03 The Standard Oil Company Catalyst for process for the manufacture of acrylonitrile and methacrylonitrile
JP3809188B2 (ja) * 1995-01-31 2006-08-16 旭化成ケミカルズ株式会社 アクリロニトリルの製造方法
CN1055918C (zh) * 1997-11-13 2000-08-30 中国石油化工总公司 烯腈急冷工艺
RU2210566C2 (ru) * 1998-06-15 2003-08-20 Солютиа Инк. Способ выделения олефинненасыщенных нитрилов
CN2386046Y (zh) * 1998-12-31 2000-07-05 中国石化集团齐鲁石油化工公司 丙烯腈工艺中急冷塔进酸量的自动控制装置
CN1112352C (zh) * 2000-06-15 2003-06-25 中国石油化工集团公司 丙烯腈急冷方法
US6777585B2 (en) * 2002-11-27 2004-08-17 Exxonmobil Chemical Patents Inc. Catalyst fines handling and disposal process
US7741528B2 (en) * 2007-02-05 2010-06-22 Exxonmobil Chemical Patents Inc. Method of separating condensed liquid from an olefin stream
US7893310B2 (en) * 2007-02-05 2011-02-22 Exxonmobil Chemical Patents Inc. Method of separating condensed liquid from an olefin stream
CN102657946B (zh) * 2012-04-20 2014-11-05 中国天辰工程有限公司 一种从丙烯腈装置回收制备硫酸铵的方法
CN103896806B (zh) * 2014-04-02 2015-07-22 中国石油集团东北炼化工程有限公司吉林设计院 丙烯腈分离提纯系统
CN204233802U (zh) * 2014-06-11 2015-04-01 英尼奥斯欧洲股份公司 用于在丙烯腈回收中减轻乙腈分馏塔中的污染的设备
CN104107559A (zh) * 2014-06-11 2014-10-22 英尼奥斯欧洲股份公司 丙烯腈回收的乙腈移除步骤中的污染减轻
CN104028172B (zh) * 2014-06-27 2018-05-25 英尼奥斯欧洲股份公司 用于氨氧化反应器的氨进料的控制
CN104587818B (zh) * 2014-09-30 2017-01-04 英尼奥斯欧洲股份公司 骤冷塔操作和底物处理
CN205229846U (zh) * 2015-08-03 2016-05-11 英尼奥斯欧洲股份公司 用于控制急冷塔pH的系统

Also Published As

Publication number Publication date
WO2017023663A1 (en) 2017-02-09
RU2720311C2 (ru) 2020-04-28
RU2018106541A3 (tr) 2019-12-06
RU2018106541A (ru) 2019-09-05
SA518390859B1 (ar) 2022-01-13
CN105425849A (zh) 2016-03-23
CN105425849B (zh) 2020-06-26

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