TH17836C3 - Process of producing glycerin from rubber oil - Google Patents

Abstract

Summary of the invention which will appear on the advertisement page ReadFile:------29/12/2020------(OCR)The process of producing glycerin from rubber oil is to prepare oil. The sap that has been filtered, cleaned and stratified until a pure oil is obtained. It is heated again and a solution containing sodium hydroxide and methanol is added to separate it. It is seen as a solution that appears to be 3 layers by observing the top layer is oil, the middle layer is glycerin, and the bottom layer is not yet clear. Then separate each layer of oil by pouring to separate the solution layer. Again, to obtain glycerin, the top and bottom layers of oil are added to hydrochloric to adjust the pH, hexane is added to dissolve the oil and methanol to bind to the glycerin. and collect the methanol layer. Repeat this 3 times separately, one layer at a time, then combine the 3 layers of solution together and adjust the pH to neutral by adding sodium hydroxide, then adding activated carbon and Bring to a boil and then filter through filter paper and evaporate the solvent, then add methanol to dissolve the white precipitate of the salt, wait until the salt settles and filter again with filter paper, the final layer is The solution is to evaporate the solvent. It is removed with a rotary evaporator under vacuum until it is glycerin------------------07/08/2561------( OCR) Page 1 of 1 page Summary of the invention of glycerin production process from rubber oil is to prepare rubber oil that has been filtered, cleaned and stratified until the oil is pure. It was reheated and the solution containing sodium hydroxide and methanol was initially separated to reveal a solution that appeared in three layers, observing the top layer being oil, the middle layer being glycemic. The serine and the bottom layer are not yet clear, then separate each oil layer by pouring to separate the solution layer again to get the glycerin. Take the top oil and the bottom layer. Originally hydrochloric to adjust pH, added hexane to dissolve oil and methanol to bind to glycerin and store the methanol layer. Repeat this 3 times separately. Then the three layers of solution were brought together and adjusted the pH to neutral by adding sodium hydroxide, then adding charcoal powder and bringing it to a boil and filtering through filter paper and evaporating the solvent. Then add methanol to dissolve the white precipitate of the salt, wait until the salt precipitates and filter with Remove the filter paper again. The last step is to evaporate the solvent with a rotary evaporator under vacuum until it is glycerin. --------------- ---30/10/2017------(OCR) Page 1 of 1 page number invention summary The process of producing glycerin from rubber oil is to prepare the rubber oil that has been filtered, cleaned and stratified until the oil is pure, then heated again and added the solution. containing sodium hydroxide and methanol to form a solution that appears to be three-layered by observation: the top layer is oil, the middle layer is glycerin, and the bottom layer is unknown. Then remove the top layer of oil and put it in the separator funnel as much as possible to separate the solution layer again to obtain glycerin by adding hydrochloric to adjust the pH, adding hexane. To dissolve oil and methanol to bind to glycerin and to bring the lowest layer of wax that is not known exactly to add the same solution as the top layer and collect the methanol layer. Repeat this way3 Then, the three layers of the solution were brought to neutralize the pH by adding sodium hydroxide, then adding charcoal powder and bringing it to a boil and filtering through filter paper and evaporating the solvent, then adding. methanol to dissolve the white precipitate of the salt, wait until the salt settles and filter again with filter paper, the final step is to evaporate the solvent with a rotary evaporator under vacuum. Prof until the glycerin came out-------edited 01/02/2017 The process of preparing rubber oil for glycerin extraction. The heated rubber oil is used to bring the sodium hydroxide solution mixed with methanol (methanol) to pour into the heated rubber oil and then pour it. Put the separation funnel and leave it for a while to allow the solution to separate until it can be observed as 3 layers: the top layer is oil, the middle layer is glycerin, and the bottom layer is not clear, then pour out the oil as much as possible, adjust pH was 1 with hydrochloric and hexane and methanol were added to the separation funnel. Hexane will react to dissolve oil and methanol will bind to glycerin and mix the base wax with hexane to collect methanol (acid) layer and adjust pH again to neutral. With the addition of sodium hydroxide solution, add charcoal powder, boil until boiling, then filter through filter paper and evaporate the solvent, then a white precipitate of the salt will be observed, dissolve it with methanol to make precipitated salt and filtered through filter paper to remove the salt. After that, the solution was evaporated by a rotary evaporator under vacuum until the glycerin came out.------ Glycerin extraction and Products and produce products extracted from the rubber trees by taking the rubber oil obtained from the rubber tree drilling and burning for 2-3 minutes and covering the fire with leaves. Filter the oil and clean the oil by adding water. Mix and heat at 100°C for 15 minutes, then set aside for about 1 day to allow the oil to separate clearly. Glycerin extraction process for use in the production of glycerin bar soap by approximately 400 mL of oil obtained at 60°C. Then prepare 5 g of sodium hydroxide solution in 200 mL of methanol. The sodium hydroxide solution is added to the heated oil and poured into the separation funnel. The solution is divided into 3 layers: the top layer is oil, the middle layer is glycerin, and the bottom layer is unknown. Then pour out the oil as much as possible, adjust the pH to 1 with hydrochloric, add 200mL Haxane and 100mL methanol. The lower wax serine was mixed with Haxen to collect the methanol (acid) layer, made 3 times, then neutralized the pH with sodium hydroxide, added the charcoal powder, boiled and filtered through the evaporative filter paper. Dissolved (found white precipitate of salt) Dissolved with methanol to make the salt precipitate Filtered through filter paper to remove the salt Remove the solution to evaporate the solvent with a rotary evaporator under vacuum and get glycerin. come out Glycerin obtained as an ingredient in bar soap production by means of bringing soap shards into a pot and heating it through water in a heated pan, then adding rubber oil mixed with glycerin rubber and adding Into the pot where the soap flakes have melted and stir in the same direction, lift it up and pour it into a tray to cool. Prepare the extract from the leaves of Na Yang Na by bringing the fresh leaves to dry, then grind them finely, add alcohol to it, then stir well and leave it for 24 hours to allow the extract to fully come out. Filtered with filter paper to get extracts from the leaves. The process of producing liquid soap from the extract from the leaves of the rubber field. Prepare the ingredients are SodiumlauryletherSulfate, KOH, Preservative, perfume essence, leaf extract No.1 and water. The process is as follows. Add water and mix SodiumlauryletherSulfate into it, add KOH and Preservative. Go into the mixing bowl, stir well, add the extract obtained from the extraction of the leaves, add to the mix, then add the perfume and stir thoroughly. The production process of massage oil from Na rubber oil with the production process is as follows: Prepare the ingredients are navaline rubber oil, camphor and menthol by Vaseline at 60°C. Add the camphor and menthol to the lowest amount and add it little by little. The oil must be cool because if it is hot, the menthol and camphor will evaporate, causing the menthol and camphor to be ineffective. Stir well. The production process of herbal spray from Na Yang oil with the production process is as follows: Prepare all ingredients, namely Na ethanol rubber oil, menthol mint 20 leaf extract and perfume. Then add ethanol and leaf extract, stir well, then add menthol and tween 20 to make the oil and leaf extract together, stir until homogeneous.

Claims (9)

Claims (all) which will not appear on the advertisement page:------29/12/2020------(OCR) 1. Process of producing glycerin from rubber oil. The rice field has the following steps: a. Drill the rubber tree and burn the fire inside the hole that has been drilled for 2-3 minutes, then cover the fire with leaves, scoop out the oil from the fire and put it in the prepared container. b. Take the oil from A. A. to filter and clean the oil by adding water to mix and heat it at 100 degrees Celsius for 15 minutes, then leave it for about 1 day until you can notice the oil separation. The clear layer is then taken only the part of the oil layer that is separated and poured into a container. C. The oil obtained from the latex preparation process of 400 ml is heated to a temperature of 60 ° C. Prepare the solution. Sodium hydroxide (NaOH) 5 grams in methanol (Methanol) 200 ml, then put the solution into the oil that has been heated from the connector. Pour into a separate funnel, set aside for a while. Rest until you can notice that the solution is separated into 3 layers, the top layer is oil, the middle layer is glycerin, and the bottom layer is still not clear information. separated by pouring by top layer of oil The lowest and lowest levels were adjusted to pH 1 with hydrochloric and added 200 ml of Hexane and 100 ml of methanol by layer by layer. The ethanol binds to the glycerin and retains the binding layer of the methanol to the glycerin. Repeat this 3 times, then combine the three layers of the solution and neutralize the pH as well. Sodium hydroxide is added to charcoal powder, boiled until boiling, filtered through filter paper and evaporated oxychlorinated solvent, then found white precipitate of salt dissolved with metabolites, so that the salt precipitates and filtered through filter paper to remove Ox salt. After that, the solution is evaporated by a rotary evaporator under vacuum until it is glycerin. 2. Using glycerin from rubber oil obtained from the process according to claim 1 to produce bar soap by a. Bring the soap flakes into a pot and heat it by passing water in a pan at a temperature of 60 degrees Celsius. .Mix the rubber oil and the rubber glycerin and add it to the pot that dissolves the soap flakes from A. Then put all the ingredients in the same direction until they are mixed together. C. Bring the ingredients from the B. Lift up. Pour into prepared trays or molds, wait for it to cool, then cut into the desired size or shape and put into the package------------------07/08/2561 ------(OCR)Page 1 of the number 2 claims page 1. The process of producing glycerin from Na rubber oil is as follows: A. Drill the rubber tree and burn the fire inside the hole that has been drilled for 2-3 minutes, then cover the fire with the oil scoop. From burning out, put it in a container that has been prepared. B. Bring the oil from Clause A. to filter and clean the oil by adding water to the mix and at a temperature of 100 degrees Celsius, using a period of 15 minutes, then brought. Leave it for about 1 day until the oil can be clearly separated. Then bring only the part of the oil layer that is separated and pour it into a container. C. Bring the oil obtained from the latex preparation process in the amount of 400 ml. Heat at 60 degrees Celsius. Prepare a solution of sodium hydroxide (NaOH) 5 grams in methanol (Methanol) 200 ml. Then put the solution into the heated oil from Note. Pour into a separate funnel and leave it for a while until you can notice that the solution is separated into 3 layers, the top layer is oil, the middle layer is glycerin, and the bottom layer is not clear information. From the section. Let's separate the 3 layers of oil from each other by pouring the top and bottom oils to adjust the pH to 1 with Hydrochloric and add Hexane (Hexane). xane) 200 ml and methanol 100 ml in separate layers in which hexane dissolves oil, methanol binds to glycerin and methanol binds to glycerin. Repeat this 3 times f. Then bring all 3 steps of the solution together and neutralize the pH with sodium hydroxide, add charcoal powder, boil until boiling, filter through filter paper and evaporate the solvent. Then a white precipitate of methanol dissolved salt is found to allow the salt to precipitate and filter through filter paper to remove the salt. After that, the solution is evaporated by a rotary evaporator under vacuum until Got a glycerin out of the 2nd page of the number 2 pages. 2. Using glycerin from rubber oil obtained from the process according to claim 1 to produce bar soap by a. Bring the soap flakes into a pot and heat it by passing water in a pan at a temperature of 60 degrees Celsius. Mix Na rubber oil and Na rubber glycerin and add it to the pot to dissolve the soap flakes from A. Then stir all the ingredients in the same direction until combined. C. Bring the ingredients from B. Lift up. Pour into prepared trays or tins, wait for it to cool, then cut into desired size or shape and put into packaging------------------30/10/2017 ------(OCR)Page 1 of the number 2 claims page 1. The process of producing glycerin from Na rubber oil is as follows: A. Drill the rubber tree and burn the fire inside the hole that has been drilled for 2-3 minutes, then cover the fire with the oil scoop. From burning out, put it in a prepared container. B. Bring the oil from A. to filter and clean the oil by adding water to the mix and at a temperature of 100 degrees Celsius, using a period of 15 minutes, then set it aside. Leave for about 1 day until the oil can be clearly distinguished. Then bring only the part of the oil layer that is separated and pour it into a container. C. Bring the oil obtained from the latex preparation process in the amount of 400 ml to be heated to a temperature. 60 degrees Celsius. Prepare a solution of sodium hydroxide (NaOH) 5 g in methanol (Methanol) 200 ml. Then put the solution into the heated oil from A. Pour. Put a separate funnel and leave it for a while until you can notice that the solution is separated into 3 layers: the top layer is oil, the middle layer is glycerin and the bottom layer is not clear information. E. Take the oil from the joint. Pour the oil layer. top out in the separator funnel as much as possible to separate the solution layer again to obtain glycerin by adjusting the pH to 1 with Hydrochloric and Add 200 ml of hexane and 100 ml of methanol. Hexane will dissolve the oil, methanol will bind to glycerin and add the lowest layer of wax that is still unknown. The same solution as the top layer and collect the methanol layer. Repeat this 3 times f. Then bring the 3 layers of solution to neutralize the pH with sodium hydroxide, add charcoal powder, boil until boiling, filter through filter paper and Solvent was evaporated. Then a white precipitate of salt dissolved with methanol was found to allow the salt to precipitate and filter through filter paper to remove the salt. After that, the solution was evaporated with a machine. Rotary evaporation under vacuum until it is glycerin, 2 pages of 2 cm. After that, take the solution to evaporate the solvent with a rotary evaporator under vacuum until it is glycerin. come out 2. The use of glycerin from rubber oil obtained from the process according to claim 1 to produce bar soap by a. Bring the soap flakes into a pot and heat it by passing water in a pan at a temperature of 60 degrees Celsius. Mix Na rubber oil and Na rubber glycerin and add it to the pot to dissolve the soap flakes from A. Then stir all the ingredients in the same direction until combined. C. Bring the ingredients from B. Lift up. Pour into prepared trays or tins, wait for it to cool, then cut into desired size or shape and pack into packages.--------------Edit 01/02/2017 1. The process of preparing rubber oil for glycerin extraction. Bring the oil obtained from the latex preparation process in the amount of 400 ml and heat it to a temperature of 60 degrees Celsius. B. Prepare a solution of sodium hydroxide ( NaOH) 5 g in methanol (methanol) 200 ml, then put the solution into the oil that has been heated from Clause A. Pour into a separate funnel, set aside for a while until a separate solution can be observed. It is 3 layers: the top layer is oil, the middle layer is glycerin, and the bottom layer is not yet clear. c. Take the oil from item B. Pour out the oil as much as possible, adjust the pH to 1 with hydrochloric and Add 200 ml of hexane and 100 ml of methanol in a separate funnel where hexane will dissolve the oil and the methanol will bind to the glycerin and the lower wax is mixed with the hexane to collect. The methanol layer (acid) is made 3 times. D. Then neutralize the pH with sodium hydroxide, add charcoal powder, boil it to boil, filter through filter paper and evaporate the solvent out of the province. Then sediment will be found. The white content of the salt was dissolved with methanol to precipitate the salt and filtered through filter paper to remove the salt. After that, the solution was evaporated by a rotary evaporator under vacuum until glycemic was obtained. Aren came out 2. Process of bringing glycerin rubber to produce glycerin bar soap. Bird. Bring soap shards to a pot and heat by passing water in a pan at a temperature of 60 degrees Celsius. B. Mixing rubber oil with glycerin. Serine Yang Na and added to the pot to dissolve the soap shards from A. Then stir all the ingredients in the same direction until combined. C. Bring the ingredients from B. Lift up and pour into the prepared tray or mold. Then wait for it to cool, then cut into pieces of the desired size and put into the package -----1. The process of extracting glycerin and products from the rubber trees which are divided into a. Drill the rubber tree and burn it for 2-3 minutes and cover the fire with leaves. Bring the oil to the second. B. Clean the oil by Add water to mix and heat at 100°C for 15 minutes. Set aside for about 1 day to allow the oil to separate layers clearly. C. Bring the oil approximately 400 mL. to a temperature of 60°C, then prepare a solution of sodium hydroxide 5. g in 200mL methanol, sodium hydroxide solution is added to heated oil. Then pour it into a separate funnel. D. The solution is made into 3 layers: the top layer is oil, the middle layer is glycerin, and the bottom layer is still unknown. E. Pour out the oil as much as possible, adjust the pH to 1 with Hi. Drochloric f. Add 200mL. Haxane and 100mL. Methanol in a funnel separated by Haxen to dissolve oil and methanol. Will bind with glycerin g. The lower wax is mixed with Haxen to collect the methanol (acid) layer, do 3 times, then neutralize the pH as well. Sodium hydroxide H. Add charcoal powder to boil and then filter through paper to evaporate the solvent (found white precipitate of salt) at. Dissolved with methanol to allow the sediment salt to filter through filter paper to remove Desalination J. Remove the solution to evaporate the solvent with a rotary evaporator under vacuum and get glycerin. 1.2 Extraction process for leaf extracts with the following steps: a. Bring the fresh leaves to dry. b. Add alcohol to it, then stir well, set aside for 24 hours, filter by filter paper, extracted from rubber fibers. 1.3 Process of producing glycerin bar soap from rubber oil which has The steps are as follows: a. Put the soap shards into the pot and heat it through the water in the pan at 60 °C. b. Add the Na rubber oil mixed with the glycerin rubber and add it to the pot where the soap shards have dissolved. c. Pour into a tray size 30x30c. m. Wait for it to cool. Cut the size 8x6c. m. get glycerin bar soap from rubber oil 1.4 The process of producing massage oil from Na rubber oil, which has the following steps: a. Dissolve Vaseline at 60 °C. b. Add Na rubber oil, stir well, wait for it to cool. c. Add camphor and menthol that are pounded and put down. Little by little while the oil cools. D. Stir well to form a homogeneous mass to get massage oil from rubber oil. 1.5 The production process for liquid soap extracted from rice leaves is as follows: a. Add water and mix with SodiumlauryletherSulfate b. Add KOH and Preservative, stir well. 2nd place, stir well. D. Add perfume and stir until thoroughly. Liquid soap extracted from Na rubber oil 1.6 The process of producing rubber mitt spray, which has the following steps: a. Put the rice rubber oil into a mixing bowl, add ethanol and extract from the leaves according to claim 2 b. Add menthol to dissolve c. Add 20 tween to make a homogeneous spray. Yang Na herb 2. Glycerin extraction for cleaning must be mixed with water and heated at 100°C for 15 minutes according to claim 1. 3. Haxane layer dissolves contaminated oil and methanol binds to glycerin according to claim 1. 4. 400 ml of oil. It can get 1.8338 grams of pure glycerin for the new rubber oil and for the old rubber oil. Glycerin that does not completely remove contaminants is 2.7414 grams according to claim 1. 5. Soaking the extract from the leaves must be soaked for a period of 24-48 hours in order for the extract in the rubber leaves to come out fully according to claim 2. 6. Stirring the glycerin soap so that it doesn't foam and makes the soap mix well because it makes the molecules of the substance align. Regulations according to Article 3 7. The addition of camphor and menthol should be added small at a time while the oil is warm because if the oil is hot it will do. Let camphor and menthol evaporate, if evaporated, will reduce the effectiveness of camphor and menthol. less according to claim No. 4 8. Leaf extracts should be kept in total darkness because the chlorophyll in the leaves will fade when exposed to sunlight and will evaporates when left open according to claim 5 9. To dissolve the oil into the rubber oil extract by using Tween 20 as an aid to dissolve both substances. Types together according to claim No. 6