SU988186A3 - Способ получени диметилкарбоната - Google Patents
Способ получени диметилкарбоната Download PDFInfo
- Publication number
- SU988186A3 SU988186A3 SU803261151A SU3261151A SU988186A3 SU 988186 A3 SU988186 A3 SU 988186A3 SU 803261151 A SU803261151 A SU 803261151A SU 3261151 A SU3261151 A SU 3261151A SU 988186 A3 SU988186 A3 SU 988186A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- methanol
- hydrogen
- oxygen
- dimethyl carbonate
- kgf
- Prior art date
Links
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 238000000034 method Methods 0.000 title claims description 15
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 57
- 229910002091 carbon monoxide Inorganic materials 0.000 claims abstract description 17
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims abstract description 16
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 15
- 239000001301 oxygen Substances 0.000 claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 claims abstract description 7
- 239000003054 catalyst Substances 0.000 claims abstract description 6
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 5
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract 18
- 239000001257 hydrogen Substances 0.000 claims abstract 17
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract 14
- 239000000203 mixture Substances 0.000 claims abstract 13
- 238000006243 chemical reaction Methods 0.000 claims abstract 10
- 239000007789 gas Substances 0.000 claims abstract 9
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 7
- 238000004458 analytical method Methods 0.000 claims 4
- 239000007791 liquid phase Substances 0.000 claims 4
- 150000002431 hydrogen Chemical class 0.000 claims 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
- 229910052799 carbon Inorganic materials 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 239000004215 Carbon black (E152) Substances 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- VMQMZMRVKUZKQL-UHFFFAOYSA-N Cu+ Chemical compound [Cu+] VMQMZMRVKUZKQL-UHFFFAOYSA-N 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 238000004868 gas analysis Methods 0.000 claims 1
- 229930195733 hydrocarbon Natural products 0.000 claims 1
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 239000012535 impurity Substances 0.000 claims 1
- 230000003993 interaction Effects 0.000 claims 1
- 239000002994 raw material Substances 0.000 claims 1
- 230000035484 reaction time Effects 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 abstract description 3
- 239000008246 gaseous mixture Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 230000000737 periodic effect Effects 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
- HQYCOEXWFMFWLR-UHFFFAOYSA-K vanadium(iii) chloride Chemical compound [Cl-].[Cl-].[Cl-].[V+3] HQYCOEXWFMFWLR-UHFFFAOYSA-K 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/01—Preparation of esters of carbonic or haloformic acids from carbon monoxide and oxygen
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT27816/79A IT1127270B (it) | 1979-12-04 | 1979-12-04 | Processo per la produzione di dimetilcarbonato |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU988186A3 true SU988186A3 (ru) | 1983-01-07 |
Family
ID=11222385
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU803261151A SU988186A3 (ru) | 1979-12-04 | 1980-12-04 | Способ получени диметилкарбоната |
Country Status (17)
Families Citing this family (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3265843D1 (en) | 1981-07-30 | 1985-10-03 | Shell Int Research | Process for the preparation of carbonate esters |
| US5093513A (en) * | 1983-06-20 | 1992-03-03 | Texaco Inc. | Process for oxycarbonylation of lower alkanols |
| US4761467A (en) * | 1985-10-21 | 1988-08-02 | Texaco Inc. | Pyridine ligands for preparation of organic carbonates |
| US5149839A (en) * | 1988-11-08 | 1992-09-22 | Nitto Boseki Co., Ltd. | Silane coupling agent and glass fiber product for laminates |
| DE3926709A1 (de) * | 1989-08-12 | 1991-02-14 | Basf Ag | Verfahren zur herstellung von dialkylcarbonaten |
| US5171874A (en) * | 1989-08-22 | 1992-12-15 | Quantum Chemical Corporation | Process for making dihydrocarbyl carbonate |
| DE69103445T3 (de) * | 1990-03-09 | 1998-03-19 | Enichem Spa | Verfahren zur Herstellung von organischen Carbonaten. |
| EP0463678B1 (en) * | 1990-06-29 | 1994-10-05 | ENICHEM SYNTHESIS S.p.A. | Process and catalyst for preparing organic carbonates |
| DE4123603A1 (de) * | 1991-07-17 | 1993-01-21 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| US5183920A (en) * | 1992-01-13 | 1993-02-02 | The Dow Chemical Company | Integrated process for the production of dimethyl carbonate |
| DE4203796A1 (de) * | 1992-02-10 | 1993-08-12 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| IT1254226B (it) * | 1992-02-26 | 1995-09-14 | Enichem Sintesi | Prodedimento catalitico per la preparazione di carbonati organici |
| US5221761A (en) * | 1992-04-29 | 1993-06-22 | Instituto Guido Donegani | Melt transesterification process for the production of polycarbonates |
| JPH06239807A (ja) * | 1992-07-31 | 1994-08-30 | Ube Ind Ltd | 炭酸エステルの製造法 |
| US5391803A (en) * | 1992-09-30 | 1995-02-21 | The Dow Chemical Company | Production of dimethyl carbonate using copper zeolite catalysts |
| JPH06192181A (ja) * | 1992-11-06 | 1994-07-12 | Ube Ind Ltd | 炭酸ジエステルの製造法 |
| DE4339977A1 (de) * | 1993-11-24 | 1995-06-01 | Bayer Ag | Verfahren zur Aufarbeitung der flüssigen Reaktionsprodukte aus der Cu-katalysierten Dimethylcarbonatherstellung |
| IT1269884B (it) | 1994-06-03 | 1997-04-15 | Enichem Sintesi | Metodo per la rimozione dei contaminanti acidi e salini dalla fase condensata dell'effluente di reazione in un processo per la sintesi di dimetilcarbonato |
| IT1269883B (it) | 1994-06-03 | 1997-04-15 | Enichem Sintesi | Metodo per la rimozione dei contaminanti acidi contenuti in una corrente vaporizzata composta da vapori organici e acqua |
| US5563288A (en) * | 1995-06-07 | 1996-10-08 | Osi Specialties, Inc. | Process for the preparation of tertiary aminocarbonates and aminoethers |
| US6818049B1 (en) | 1998-05-05 | 2004-11-16 | Exxonmobil Chemical Patents Inc. | Environmentally preferred fluids and fluid blends |
| US6280519B1 (en) * | 1998-05-05 | 2001-08-28 | Exxon Chemical Patents Inc. | Environmentally preferred fluids and fluid blends |
| US6008399A (en) * | 1999-03-11 | 1999-12-28 | Mobil Oil Corporation | Process for preparing organic carbonates |
| US6294684B1 (en) | 1999-12-08 | 2001-09-25 | General Electric Company | Method and apparatus for the continuous production of diaryl carbonates |
| JP3799968B2 (ja) | 2000-06-16 | 2006-07-19 | 東海ゴム工業株式会社 | 耐久性に優れた防振ゴムの製造方法 |
| US7345187B2 (en) | 2001-08-14 | 2008-03-18 | General Electric Company | Method and apparatus for preparing a dialkyl carbonate, and its use in the preparation of diaryl carbonates and polycarbonates |
| US7514521B2 (en) | 2001-08-14 | 2009-04-07 | Sabic Innovative Plastics Ip B.V. | Method for preparing a dialkyl carbonate, and its use in the preparation of diaryl carbonates and polycarbonates |
| US6784277B2 (en) | 2001-08-14 | 2004-08-31 | General Electric Company | Method for preparing a dialkyl carbonate, and its use in the preparation of diaryl carbonates and polycarbonates |
| US6977308B2 (en) | 2002-06-25 | 2005-12-20 | General Electric Company | Method and apparatus for preparing a dialkyl carbonate |
| US7049457B2 (en) * | 2003-09-05 | 2006-05-23 | Exxonmobil Chemical Patents Inc. | Use of an ionic halide free copper catalyst for the production of dialkyl carbonates |
| ES2245254B1 (es) * | 2004-06-11 | 2007-03-01 | Universidad Politecnica De Valencia | Procedimiento para la obtencion compuestos organicos poli-oxigenados. |
| US7622602B2 (en) * | 2005-10-12 | 2009-11-24 | Sabic Innovative Plastics Ip B.V. | Method for preparing a dialkyl carbonate, and its use in the preparation of diaryl carbonates and polycarbonates |
| TW200831458A (en) * | 2007-01-17 | 2008-08-01 | China Petrochemical Dev Corp | The manufacturing method of dialkyl carbonate |
| TW200846319A (en) | 2007-05-28 | 2008-12-01 | China Petrochemical Dev Corp | Method for preparing carbonate diester |
| TW201004703A (en) * | 2008-07-31 | 2010-02-01 | China Petrochemical Dev Corp | Catalytic system for the oxidative carbonylation reaction and the manufacturing method for alkyl dimethyl ester of carbonic acid using the catalytic system |
| CN104892423B (zh) * | 2015-05-18 | 2017-01-04 | 太原理工大学 | 一种甲醇氧化羰基化制备碳酸二甲酯的工艺 |
| CN106478421B (zh) | 2015-08-31 | 2019-09-13 | 亚申科技(浙江)有限公司 | 碳酸二甲酯生产工艺 |
| CN107335443B (zh) * | 2017-07-12 | 2018-08-21 | 太原理工大学 | 爆炸法快速制备石墨烯负载多金属催化剂的方法 |
| WO2020127287A1 (en) | 2018-12-20 | 2020-06-25 | Haldor Topsøe A/S | A process for preparing dimethyl carbonate |
| CN111548273B (zh) * | 2020-05-09 | 2021-10-01 | 中国科学技术大学 | 使用铜/氧化亚铜纳米片催化剂热催化甲醇与二氧化碳生成碳酸二甲酯的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA923139A (en) * | 1970-03-04 | 1973-03-20 | Snamprogetti S.P.A. | Process for the preparation of esters of the carbonic acid |
| DE2520708A1 (de) * | 1975-05-09 | 1976-11-25 | Roehm Gmbh | Verfahren zur herstellung von kohlensaeureestern |
| US4113762A (en) * | 1975-05-09 | 1978-09-12 | Rohm Gmbh | Method of making carbonic acid esters |
| US4218391A (en) * | 1976-09-30 | 1980-08-19 | Anic, S.P.A. | Method for the preparation of esters of carbonic acid |
| US4234504A (en) * | 1978-12-15 | 1980-11-18 | General Electric Company | Carbonylation process |
-
1979
- 1979-12-04 IT IT27816/79A patent/IT1127270B/it active
-
1980
- 1980-11-12 US US06/205,949 patent/US4318862A/en not_active Expired - Lifetime
- 1980-11-12 ZA ZA00806994A patent/ZA806994B/xx unknown
- 1980-11-13 CA CA000364530A patent/CA1158663A/en not_active Expired
- 1980-11-17 AU AU64449/80A patent/AU542124B2/en not_active Ceased
- 1980-11-19 GB GB8037080A patent/GB2064525B/en not_active Expired
- 1980-11-20 DK DK495980A patent/DK161248C/da not_active IP Right Cessation
- 1980-12-01 JP JP16812380A patent/JPS5695151A/ja active Granted
- 1980-12-01 BE BE0/203043A patent/BE886495A/fr not_active IP Right Cessation
- 1980-12-01 CH CH888080A patent/CH645610A5/it not_active IP Right Cessation
- 1980-12-01 LU LU82971A patent/LU82971A1/fr unknown
- 1980-12-02 FR FR8025580A patent/FR2471363A1/fr active Granted
- 1980-12-02 NO NO803631A patent/NO152696C/no not_active IP Right Cessation
- 1980-12-03 SE SE8008501A patent/SE445827B/sv unknown
- 1980-12-03 NL NLAANVRAGE8006591,A patent/NL186510C/xx not_active IP Right Cessation
- 1980-12-04 SU SU803261151A patent/SU988186A3/ru active
- 1980-12-04 DE DE3045767A patent/DE3045767C2/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2471363A1 (fr) | 1981-06-19 |
| NO152696B (no) | 1985-07-29 |
| US4318862A (en) | 1982-03-09 |
| AU6444980A (en) | 1983-01-20 |
| NL186510C (nl) | 1990-12-17 |
| SE8008501L (sv) | 1981-06-05 |
| CA1158663A (en) | 1983-12-13 |
| NO152696C (no) | 1985-11-06 |
| DE3045767C2 (de) | 1983-06-01 |
| FR2471363B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1984-03-02 |
| LU82971A1 (fr) | 1981-07-23 |
| GB2064525A (en) | 1981-06-17 |
| ZA806994B (en) | 1981-10-28 |
| AU542124B2 (en) | 1985-02-07 |
| IT1127270B (it) | 1986-05-21 |
| NO803631L (no) | 1981-06-05 |
| DK495980A (da) | 1981-06-05 |
| IT7927816A0 (it) | 1979-12-04 |
| DE3045767A1 (de) | 1981-06-11 |
| SE445827B (sv) | 1986-07-21 |
| JPS5695151A (en) | 1981-08-01 |
| NL186510B (nl) | 1990-07-16 |
| NL8006591A (nl) | 1981-07-01 |
| DK161248C (da) | 1991-12-02 |
| CH645610A5 (it) | 1984-10-15 |
| DK161248B (da) | 1991-06-17 |
| BE886495A (fr) | 1981-06-04 |
| JPS6338018B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-07-28 |
| GB2064525B (en) | 1983-09-14 |
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