SU780873A1 - Apparatus for removing solution from autoclave - Google Patents

Apparatus for removing solution from autoclave Download PDF

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Publication number
SU780873A1
SU780873A1 SU782694112A SU2694112A SU780873A1 SU 780873 A1 SU780873 A1 SU 780873A1 SU 782694112 A SU782694112 A SU 782694112A SU 2694112 A SU2694112 A SU 2694112A SU 780873 A1 SU780873 A1 SU 780873A1
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SU
USSR - Soviet Union
Prior art keywords
autoclave
valve
drain pipe
membrane
shut
Prior art date
Application number
SU782694112A
Other languages
Russian (ru)
Inventor
Борис Васильевич Михайлов
Александр Федорович Маслов
Владимир Алексеевич КЛИПОВ
Original Assignee
Предприятие П/Я В-2854
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Filing date
Publication date
Application filed by Предприятие П/Я В-2854 filed Critical Предприятие П/Я В-2854
Priority to SU782694112A priority Critical patent/SU780873A1/en
Application granted granted Critical
Publication of SU780873A1 publication Critical patent/SU780873A1/en

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Description

. Изобретение относитси к устройствам ОЛЯ разгрузки резе|шу1аров под давлени в частности дл  удалени  раствора из автоклава при выращивании монокристаллов кварца в гидротермальных услови х, и может быть использовано в химическо промышленности. Известно устройство дл  удалени  продукта из аппарата, включающее сливИую трубу с запорным вентилем QQ, Однако устройство имеет недостаточно высокую надежность в работе. Цель изобретени  - повышение надежности работы устройства за счет предотвращени  попадани  раствора в сливную трубу во врем  протекани  процесса в автоклаве. Цель достигаетс  тем, что слив а  труба снабжена расположенной под запорным вентилем предохранительной мембраной, а часть сливной грубы между предохранительной мембраной и запорным вентилем заполнена жидкостью .На 4мг. 1 изображена схема устрой- . ства, общий вид; на фиг. 2 - узел 1 на фиг. 1. Устройство дл  удалени  раствора из автоклава включает сливйую трубу 1 и запортый вентиль 2. Спав а  труба состоит из трубки 3, расположенной внутри автоклава, и трубки 4, проход щей через отверстие в крышке 5 автоклава. Трубка 3 соединена с трубкой 4 при помощи штуцера 6 и гайки 7. Сливна  труба 1 снабжена предохранительной мембраной 8, размещенной между уплотнительными шайбами 9, выполненной в виде двух сложенных вместе круглых пластинок из хоподнснштакой;, стальной ленты (ГОСТ 5ОЗ-71) толщиной 0,05 мм. Часть сливной трубЫ 1 между предохранительной мембраной 8 и запорным вентилем 2 заполнена на 98% жидкостью, например водой. Мембрана рассчитана на давление, составл ющее 6О-65% от давлени , при котором начинают удал ть раствор из автоклава. . The invention relates to OLA devices for unloading pressurized chambers, in particular, for removing the solution from the autoclave when growing single crystals of quartz under hydrothermal conditions, and can be used in the chemical industry. A device for removing a product from an apparatus is known, including a discharge pipe with a stop valve QQ. However, the device does not have sufficiently high operational reliability. The purpose of the invention is to increase the reliability of the device by preventing the solution from entering the drain pipe during the process in the autoclave. The goal is achieved by the fact that the drain and the pipe is equipped with a safety membrane located under the shut-off valve, and a part of the drainage between the safety membrane and the shut-off valve is filled with liquid. On 4 mg. 1 shows a device diagram. general appearance; in fig. 2 — node 1 in FIG. 1. A device for removing the solution from the autoclave includes a drain pipe 1 and a stop valve 2. When the pipe collapses, it consists of a tube 3 located inside the autoclave and a tube 4 passing through an opening in the lid 5 of the autoclave. The tube 3 is connected to the tube 4 by means of fitting 6 and a nut 7. The drain pipe 1 is equipped with a safety membrane 8 placed between sealing washers 9, made in the form of two round plates folded together, made of steel tape (GOST 5ОЗ-71) 0 thickness , 05 mm. Part of the discharge pipe 1 between the safety membrane 8 and the shut-off valve 2 is filled to 98% liquid, such as water. The membrane is designed for a pressure of 6O-65% of the pressure at which they begin to remove the solution from the autoclave.

Claims (1)

о р м у л а изобретения Устройство для удаления раствора из автоклава, преимущественно при синтезе монокристаллов кварца, включаю5 шее сливную трубу с запорным вентилем, отличающееся тем, что, с : целью повышения надежности работы устройства, сливная труба снабжена расположенной под запорным вентилем предо10 хранительной мембраной, а часть сливной трубы между предохранительной мембраной и запорным вентилем заполнена жидкостью.of p m y l and apparatus of the invention for removing liquor from the autoclave, preferably in the synthesis of quartz single crystal vklyuchayu5 neck drain pipe with a stop valve, characterized in that, with: to improve the reliability of the device, the drain pipe is provided beneath the cut-off valve predo10 hranitelnoy membrane, and part of the drain pipe between the safety membrane and the shut-off valve is filled with liquid. Источники информации,Information sources, 13 принятые во внимание при экспертизе13 taken into account during the examination 1. Авторское свидетельство СССР № 162829, кл. В 01 J 3/02, 30.10.611. USSR author's certificate No. 162829, cl. B 01 J 3/02, 10.30.61
SU782694112A 1978-12-06 1978-12-06 Apparatus for removing solution from autoclave SU780873A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU782694112A SU780873A1 (en) 1978-12-06 1978-12-06 Apparatus for removing solution from autoclave

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU782694112A SU780873A1 (en) 1978-12-06 1978-12-06 Apparatus for removing solution from autoclave

Publications (1)

Publication Number Publication Date
SU780873A1 true SU780873A1 (en) 1980-11-23

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
SU782694112A SU780873A1 (en) 1978-12-06 1978-12-06 Apparatus for removing solution from autoclave

Country Status (1)

Country Link
SU (1) SU780873A1 (en)

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