SU619103A3 - Способ получени 1,3-бис-(третбутил-дитио)-2-диметиламинопропана или его кислых солей - Google Patents
Способ получени 1,3-бис-(третбутил-дитио)-2-диметиламинопропана или его кислых солейInfo
- Publication number
- SU619103A3 SU619103A3 SU752183107A SU2183107A SU619103A3 SU 619103 A3 SU619103 A3 SU 619103A3 SU 752183107 A SU752183107 A SU 752183107A SU 2183107 A SU2183107 A SU 2183107A SU 619103 A3 SU619103 A3 SU 619103A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- compound
- bis
- formula
- tert
- butyldithio
- Prior art date
Links
- 239000002253 acid Substances 0.000 title claims 5
- 150000003839 salts Chemical class 0.000 title claims 5
- 238000000034 method Methods 0.000 title claims 4
- 150000001875 compounds Chemical class 0.000 claims 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 8
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 6
- 239000000243 solution Substances 0.000 claims 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 5
- 239000002904 solvent Substances 0.000 claims 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 3
- -1 for example methanop Chemical compound 0.000 claims 3
- 238000003756 stirring Methods 0.000 claims 3
- 239000000126 substance Substances 0.000 claims 3
- FVZCUJCQONKGLF-UHFFFAOYSA-N 1,3-bis(tert-butyldisulfanyl)-N,N-dimethylpropan-2-amine Chemical compound C(C)(C)(C)SSCC(CSSC(C)(C)C)N(C)C FVZCUJCQONKGLF-UHFFFAOYSA-N 0.000 claims 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical group [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 2
- 238000006243 chemical reaction Methods 0.000 claims 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 238000002844 melting Methods 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 2
- 229910052700 potassium Inorganic materials 0.000 claims 2
- 239000011591 potassium Substances 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- 229910052708 sodium Chemical group 0.000 claims 2
- 239000011734 sodium Chemical group 0.000 claims 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims 1
- NNXFZAQAFHFISS-UHFFFAOYSA-N 2-methylpropane-2-thiol;sodium Chemical compound [Na].CC(C)(C)S NNXFZAQAFHFISS-UHFFFAOYSA-N 0.000 claims 1
- 241001214445 Mimetes Species 0.000 claims 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical class [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims 1
- 150000001242 acetic acid derivatives Chemical class 0.000 claims 1
- 150000008043 acidic salts Chemical class 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 150000001408 amides Chemical class 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical class OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 claims 1
- 150000001558 benzoic acid derivatives Chemical class 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 238000000354 decomposition reaction Methods 0.000 claims 1
- 125000004119 disulfanediyl group Chemical group *SS* 0.000 claims 1
- 150000003840 hydrochlorides Chemical class 0.000 claims 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims 1
- 230000003993 interaction Effects 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- AFVFQIVMOAPDHO-UHFFFAOYSA-M methanesulfonate group Chemical class CS(=O)(=O)[O-] AFVFQIVMOAPDHO-UHFFFAOYSA-M 0.000 claims 1
- 150000007522 mineralic acids Chemical class 0.000 claims 1
- VMOWKUTXPNPTEN-UHFFFAOYSA-N n,n-dimethylpropan-2-amine Chemical compound CC(C)N(C)C VMOWKUTXPNPTEN-UHFFFAOYSA-N 0.000 claims 1
- 150000002825 nitriles Chemical class 0.000 claims 1
- 150000007524 organic acids Chemical class 0.000 claims 1
- 235000005985 organic acids Nutrition 0.000 claims 1
- 239000012074 organic phase Substances 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 235000006408 oxalic acid Nutrition 0.000 claims 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 1
- 239000000741 silica gel Substances 0.000 claims 1
- 229910002027 silica gel Inorganic materials 0.000 claims 1
- 229910052938 sodium sulfate Inorganic materials 0.000 claims 1
- 235000011152 sodium sulphate Nutrition 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- WMXCDAVJEZZYLT-UHFFFAOYSA-N tert-butylthiol Chemical compound CC(C)(C)S WMXCDAVJEZZYLT-UHFFFAOYSA-N 0.000 claims 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims 1
- 238000004809 thin layer chromatography Methods 0.000 claims 1
- 125000003944 tolyl group Chemical group 0.000 claims 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom not containing sulfur-to-oxygen bonds, e.g. polysulfides
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1431274A CH607741A5 (en) | 1974-10-25 | 1974-10-25 | Pesticide, and the use thereof for controlling insects |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU619103A3 true SU619103A3 (ru) | 1978-08-05 |
Family
ID=4399768
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU752183107A SU619103A3 (ru) | 1974-10-25 | 1975-10-23 | Способ получени 1,3-бис-(третбутил-дитио)-2-диметиламинопропана или его кислых солей |
| SU762415057A SU713522A3 (ru) | 1974-10-25 | 1976-10-28 | Инсектицидное средство |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762415057A SU713522A3 (ru) | 1974-10-25 | 1976-10-28 | Инсектицидное средство |
Country Status (27)
-
1974
- 1974-10-25 CH CH1431274A patent/CH607741A5/xx not_active IP Right Cessation
-
1975
- 1975-10-16 DK DK466575AA patent/DK139816B/da unknown
- 1975-10-17 SE SE7511705A patent/SE7511705L/xx unknown
- 1975-10-20 GB GB42936/75A patent/GB1513560A/en not_active Expired
- 1975-10-20 DE DE19752546891 patent/DE2546891A1/de not_active Withdrawn
- 1975-10-21 NL NL7512321A patent/NL7512321A/xx not_active Application Discontinuation
- 1975-10-22 HU HU75SA00002847A patent/HU172715B/hu unknown
- 1975-10-22 EG EG626/75A patent/EG12155A/xx active
- 1975-10-23 PL PL1975184210A patent/PL96642B1/pl unknown
- 1975-10-23 SU SU752183107A patent/SU619103A3/ru active
- 1975-10-23 AU AU85984/75A patent/AU500951B2/en not_active Expired
- 1975-10-23 IL IL48356A patent/IL48356A/xx unknown
- 1975-10-23 FR FR7532416A patent/FR2289496A1/fr active Granted
- 1975-10-23 DD DD7500197039A patent/DD129146A5/xx unknown
- 1975-10-23 BE BE161199A patent/BE834812A/xx unknown
- 1975-10-23 BR BR7506960*A patent/BR7506960A/pt unknown
- 1975-10-23 PL PL1975195440A patent/PL97681B1/pl unknown
- 1975-10-23 AT AT807575A patent/AT352091B/de not_active IP Right Cessation
- 1975-10-23 ES ES442013A patent/ES442013A1/es not_active Expired
- 1975-10-23 TR TR19032A patent/TR19032A/xx unknown
- 1975-10-23 CA CA238,226A patent/CA1065345A/en not_active Expired
- 1975-10-23 JP JP50128248A patent/JPS5167724A/ja active Pending
- 1975-10-23 DD DD189022A patent/DD123326A5/xx unknown
- 1975-10-23 IE IE2315/75A patent/IE41817B1/en unknown
- 1975-10-24 IT IT28678/75A patent/IT1043648B/it active
- 1975-10-24 ZA ZA756704A patent/ZA756704B/xx unknown
- 1975-10-24 AR AR260911A patent/AR215424A1/es active
- 1975-10-24 RO RO7583720A patent/RO68807A/ro unknown
- 1975-10-24 GR GR49200A patent/GR58589B/el unknown
-
1976
- 1976-10-28 SU SU762415057A patent/SU713522A3/ru active
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