SU532573A1 - Method for producing barium carbonate - Google Patents

Method for producing barium carbonate

Info

Publication number
SU532573A1
SU532573A1 SU2113397A SU2113397A SU532573A1 SU 532573 A1 SU532573 A1 SU 532573A1 SU 2113397 A SU2113397 A SU 2113397A SU 2113397 A SU2113397 A SU 2113397A SU 532573 A1 SU532573 A1 SU 532573A1
Authority
SU
USSR - Soviet Union
Prior art keywords
barium carbonate
producing barium
barium
resulting
drum
Prior art date
Application number
SU2113397A
Other languages
Russian (ru)
Inventor
Зинаида Фоминична Гаврилова
Вадим Иванович Панов
Федор Иванович Стригунов
Ольга Николаевна Сытина
Геннадий Алексеевич Трутнев
Original Assignee
Предприятие П/Я А-3732
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Предприятие П/Я А-3732 filed Critical Предприятие П/Я А-3732
Priority to SU2113397A priority Critical patent/SU532573A1/en
Application granted granted Critical
Publication of SU532573A1 publication Critical patent/SU532573A1/en

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  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Description

Процесс описываетс  следующими химическими реакци ми:The process is described by the following chemical reactions:

-BaCe.,p..-BaCe., P ..

......

BaCe...- -H S- 2NH;-CO ..,Ce.,,sfBaCe ...- -H S- 2NH; -CO .., Ce. ,, sf

Образующуюс  суспензию раздел ют на барабанных вакуум-фильтрах.The resulting suspension is divided in drum vacuum filters.

Пасту карбоната бари  промывают водой методом репульпации - фильтраци  до OTcjTCTBHH 5 -иона в промывной воде и сушато Маточные растворы, содержащие .ц Си , возвращают в цикл на обработку раствора сернистого бари .The barium carbonate paste is washed with water by repulping - filtering until the OTcjTCTBHH 5 -ion in the wash water and dried. The mother liquors containing .ts Cu are recycled to the treatment of the sulfur barium solution.

П р и м е р. 162О г баритового кон центрата смешивают с 405 г кокса и гранулируют в присутствии сульфит-спиртовой барды. Полученные гранулы подвергаютPRI me R. 162O g of barite concentrate is mixed with 405 g of coke and granulated in the presence of sulfite-alcohol bards. The obtained granules are subjected

восстановительному обжигу во вращающейс  бараба шой печи при 1100-1150°С. Образовавшийс  плав сернистого бари  в количестве 1000 г выщелачивают промывной водой, вз той в соотнощении 1:4 при к раздел ют.reduction firing in a rotary drum at 1100-1150 ° C. 1000 g of the resulting sulphuric barium melt is leached with wash water taken at a ratio of 1: 4 and the k is separated.

Полученные 4000 г осветленного раствра сернистого бари  обрабатывают 2000 г 20%-ного раствора хлористого аммони  и подают в карбонизатор, куда одновременно подают 285,1 г углекислого газа. Карбонизацию провод т при 40 С, осажда  при этом карбонат бари . Образующуюс  суспензию фильтруют на барабанном вакуум-филь тре, отдел ют пасту карбоната бари , промывают и сущат в барабанной вращающейс  сущилке. Получают 720 г карбоната бари .The obtained 4000 g of the clarified solution of barium sulphide are treated with 2000 g of a 20% ammonium chloride solution and fed into the carbonizer, to which 285.1 g of carbon dioxide are simultaneously supplied. Carbonation is carried out at 40 ° C, while barium carbonate precipitates. The resulting slurry is filtered on a drum vacuum filter, the barium carbonate paste is separated, washed, and existed in a drum rotary nut. 720 g of barium carbonate are obtained.

Полученный продукт имеет состав по сравнению с продуктом по известному способу , приведенному в таблице.The resulting product has a composition compared to the product by a known method, shown in the table.

SU2113397A 1975-03-11 1975-03-11 Method for producing barium carbonate SU532573A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU2113397A SU532573A1 (en) 1975-03-11 1975-03-11 Method for producing barium carbonate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU2113397A SU532573A1 (en) 1975-03-11 1975-03-11 Method for producing barium carbonate

Publications (1)

Publication Number Publication Date
SU532573A1 true SU532573A1 (en) 1976-10-25

Family

ID=20612692

Family Applications (1)

Application Number Title Priority Date Filing Date
SU2113397A SU532573A1 (en) 1975-03-11 1975-03-11 Method for producing barium carbonate

Country Status (1)

Country Link
SU (1) SU532573A1 (en)

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