SU527137A3 - Способ получени диглицидилбензимидазолидонов - Google Patents
Способ получени диглицидилбензимидазолидоновInfo
- Publication number
- SU527137A3 SU527137A3 SU1868201A SU1868201A SU527137A3 SU 527137 A3 SU527137 A3 SU 527137A3 SU 1868201 A SU1868201 A SU 1868201A SU 1868201 A SU1868201 A SU 1868201A SU 527137 A3 SU527137 A3 SU 527137A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- theory
- mol
- product
- epichlorohydrin
- epoxide
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 4
- PDTLOYCCOLRFRJ-UHFFFAOYSA-N 1,3-bis(oxiran-2-ylmethyl)benzimidazol-2-one Chemical compound C12=CC=CC=C2N(CC2OC2)C(=O)N1CC1CO1 PDTLOYCCOLRFRJ-UHFFFAOYSA-N 0.000 title claims 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 12
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 claims 6
- 150000002924 oxiranes Chemical class 0.000 claims 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 5
- 239000007788 liquid Substances 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 239000011347 resin Substances 0.000 claims 4
- 229920005989 resin Polymers 0.000 claims 4
- 235000011121 sodium hydroxide Nutrition 0.000 claims 4
- OKIZCWYLBDKLSU-UHFFFAOYSA-M N,N,N-Trimethylmethanaminium chloride Chemical compound [Cl-].C[N+](C)(C)C OKIZCWYLBDKLSU-UHFFFAOYSA-M 0.000 claims 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims 3
- 150000003839 salts Chemical class 0.000 claims 3
- 239000007864 aqueous solution Substances 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- 238000006243 chemical reaction Methods 0.000 claims 2
- 238000004821 distillation Methods 0.000 claims 2
- 239000000243 solution Substances 0.000 claims 2
- RWIIUBCMPVZLBA-UHFFFAOYSA-N 1,3,3a,4,5,6,7,7a-octahydrobenzimidazol-2-one Chemical compound C1CCCC2NC(=O)NC21 RWIIUBCMPVZLBA-UHFFFAOYSA-N 0.000 claims 1
- HMTUMIONOVAMED-UHFFFAOYSA-N 1,3,3a,4,5,6-hexahydrobenzimidazol-2-one Chemical compound C1CCC=C2NC(=O)NC21 HMTUMIONOVAMED-UHFFFAOYSA-N 0.000 claims 1
- 101100478314 Caenorhabditis elegans sre-1 gene Proteins 0.000 claims 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- 150000008064 anhydrides Chemical class 0.000 claims 1
- 238000010533 azeotropic distillation Methods 0.000 claims 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims 1
- 239000003518 caustics Substances 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000002425 crystallisation Methods 0.000 claims 1
- 230000008025 crystallization Effects 0.000 claims 1
- 238000007033 dehydrochlorination reaction Methods 0.000 claims 1
- 238000006704 dehydrohalogenation reaction Methods 0.000 claims 1
- 239000000839 emulsion Substances 0.000 claims 1
- HWJHWSBFPPPIPD-UHFFFAOYSA-N ethoxyethane;propan-2-one Chemical compound CC(C)=O.CCOCC HWJHWSBFPPPIPD-UHFFFAOYSA-N 0.000 claims 1
- 238000000605 extraction Methods 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- YAMHXTCMCPHKLN-UHFFFAOYSA-N imidazolidin-2-one Chemical compound O=C1NCCN1 YAMHXTCMCPHKLN-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 239000012074 organic phase Substances 0.000 claims 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims 1
- 125000001453 quaternary ammonium group Chemical group 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 238000011282 treatment Methods 0.000 claims 1
Landscapes
- Plural Heterocyclic Compounds (AREA)
- Epoxy Compounds (AREA)
- Epoxy Resins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH10872A CH562242A5 (enrdf_load_stackoverflow) | 1972-01-05 | 1972-01-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU527137A3 true SU527137A3 (ru) | 1976-08-30 |
Family
ID=4179449
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1868201A SU527137A3 (ru) | 1972-01-05 | 1973-01-04 | Способ получени диглицидилбензимидазолидонов |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPS4879298A (enrdf_load_stackoverflow) |
| ES (1) | ES410339A1 (enrdf_load_stackoverflow) |
| IT (1) | IT972730B (enrdf_load_stackoverflow) |
| SU (1) | SU527137A3 (enrdf_load_stackoverflow) |
| ZA (1) | ZA7328B (enrdf_load_stackoverflow) |
-
1972
- 1972-12-21 IT IT3336772A patent/IT972730B/it active
-
1973
- 1973-01-04 SU SU1868201A patent/SU527137A3/ru active
- 1973-01-04 ZA ZA730028A patent/ZA7328B/xx unknown
- 1973-01-04 ES ES410339A patent/ES410339A1/es not_active Expired
- 1973-01-05 JP JP463573A patent/JPS4879298A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| IT972730B (it) | 1974-05-31 |
| ES410339A1 (es) | 1976-01-01 |
| JPS4879298A (enrdf_load_stackoverflow) | 1973-10-24 |
| ZA7328B (en) | 1973-09-26 |
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