SU460615A3 - Способ получени полифторспиртов - Google Patents
Способ получени полифторспиртовInfo
- Publication number
- SU460615A3 SU460615A3 SU1885657A SU1885657A SU460615A3 SU 460615 A3 SU460615 A3 SU 460615A3 SU 1885657 A SU1885657 A SU 1885657A SU 1885657 A SU1885657 A SU 1885657A SU 460615 A3 SU460615 A3 SU 460615A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- water
- product
- theory
- hours
- phosphoric acid
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 21
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 230000003301 hydrolyzing effect Effects 0.000 claims description 4
- 150000002334 glycols Chemical class 0.000 claims description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 3
- 101000686031 Homo sapiens Proto-oncogene tyrosine-protein kinase ROS Proteins 0.000 claims 1
- 102100023347 Proto-oncogene tyrosine-protein kinase ROS Human genes 0.000 claims 1
- 238000002955 isolation Methods 0.000 claims 1
- 239000000047 product Substances 0.000 description 14
- 150000001875 compounds Chemical class 0.000 description 11
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 9
- 238000000859 sublimation Methods 0.000 description 8
- 230000008022 sublimation Effects 0.000 description 8
- 239000007795 chemical reaction product Substances 0.000 description 7
- 238000004821 distillation Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 239000012071 phase Substances 0.000 description 7
- 238000006460 hydrolysis reaction Methods 0.000 description 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 5
- 230000007062 hydrolysis Effects 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 239000011574 phosphorus Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- YZBOZNXACBQJHI-UHFFFAOYSA-N 1-dichlorophosphoryloxyethane Chemical compound CCOP(Cl)(Cl)=O YZBOZNXACBQJHI-UHFFFAOYSA-N 0.000 description 2
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 125000004494 ethyl ester group Chemical group 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 206010063659 Aversion Diseases 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 241001331845 Equus asinus x caballus Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000012445 acidic reagent Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- HUMHYXGDUOGHTG-HEZXSMHISA-N alpha-D-GalpNAc-(1->3)-[alpha-L-Fucp-(1->2)]-D-Galp Chemical compound O[C@H]1[C@H](O)[C@H](O)[C@H](C)O[C@H]1O[C@@H]1[C@@H](O[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](O)[C@@H](CO)OC1O HUMHYXGDUOGHTG-HEZXSMHISA-N 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 230000001588 bifunctional effect Effects 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- -1 ethylene glycol Chemical class 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000003014 phosphoric acid esters Chemical class 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/34—Halogenated alcohols
- C07C31/40—Halogenated alcohols perhalogenated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Paper (AREA)
- Surface Treatment Of Glass (AREA)
- Coloring (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH255272A CH565724A5 (en, 2012) | 1972-02-22 | 1972-02-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU460615A3 true SU460615A3 (ru) | 1975-02-15 |
Family
ID=4236360
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1885657A SU460615A3 (ru) | 1972-02-22 | 1973-02-21 | Способ получени полифторспиртов |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3927126A (en, 2012) |
| JP (1) | JPS4896505A (en, 2012) |
| BE (1) | BE795705A (en, 2012) |
| CH (1) | CH565724A5 (en, 2012) |
| DE (1) | DE2307204A1 (en, 2012) |
| FR (1) | FR2173033B1 (en, 2012) |
| GB (1) | GB1395454A (en, 2012) |
| SU (1) | SU460615A3 (en, 2012) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4264484A (en) | 1979-01-24 | 1981-04-28 | Minnesota Mining And Manufacturing Company | Carpet treatment |
| DE3051168C2 (de) * | 1979-01-24 | 1998-08-27 | Minnesota Mining & Mfg | Mono- bzw. Polycarbonsäureester oder deren Gemische oder Ester bzw. deren Gemische aus Isocyanaten und fluor- bzw. chlorhaltigen aliphatischen Alkoholen |
| US4382891A (en) * | 1980-05-09 | 1983-05-10 | E. I. Du Pont De Nemours And Company | Use of fluoroalkoxysulfur fluorides in fluorinations |
| US4517376A (en) * | 1981-06-26 | 1985-05-14 | E. I. Du Pont De Nemours And Company | Manufacture of chloromethyl-substituted polyfluoroalkyl esters |
| US5242487A (en) * | 1988-11-11 | 1993-09-07 | Daikin Industries Ltd. | Water- and oil-repellant composition |
| US7470818B2 (en) * | 2006-11-13 | 2008-12-30 | E.I. Du Pont De Nemours & Company | Fluoroalkyl phosphate compositions |
| US7674928B2 (en) * | 2006-11-13 | 2010-03-09 | E.I. Du Pont De Nemours And Company | Polyfluoroether-based phosphates |
| CN110184847A (zh) * | 2019-05-17 | 2019-08-30 | 华南理工大学 | 一种撕不烂仿皮纸及其制造方法与应用 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2725394A (en) * | 1950-08-03 | 1955-11-29 | Ici Ltd | Production of esters of orthophosphoric acid and salts thereof |
| US2866807A (en) * | 1954-04-15 | 1958-12-30 | Virginia Carolina Chem Corp | Aliphatic aryl phosphites |
| US2929833A (en) * | 1958-04-23 | 1960-03-22 | Ethyl Corp | Process of preparing phenyl dimethyl phosphates |
| US2960527A (en) * | 1958-08-20 | 1960-11-15 | Akad Wissenschaften Ddr | Process for the preparation of dichloro phosphoric esters |
| US3059016A (en) * | 1959-08-05 | 1962-10-16 | Celanese Corp | Manufacture of aryl phosphate esters |
| NL282705A (en, 2012) * | 1961-09-01 |
-
0
- BE BE795705D patent/BE795705A/xx unknown
-
1972
- 1972-02-22 CH CH255272A patent/CH565724A5/xx not_active IP Right Cessation
-
1973
- 1973-02-14 DE DE19732307204 patent/DE2307204A1/de active Pending
- 1973-02-15 GB GB748373A patent/GB1395454A/en not_active Expired
- 1973-02-16 US US333246A patent/US3927126A/en not_active Expired - Lifetime
- 1973-02-19 FR FR7305744A patent/FR2173033B1/fr not_active Expired
- 1973-02-21 SU SU1885657A patent/SU460615A3/ru active
- 1973-02-22 JP JP48020753A patent/JPS4896505A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US3927126A (en) | 1975-12-16 |
| BE795705A (fr) | 1973-08-21 |
| GB1395454A (en) | 1975-05-29 |
| FR2173033B1 (en, 2012) | 1976-05-14 |
| DE2307204A1 (de) | 1973-08-30 |
| FR2173033A1 (en, 2012) | 1973-10-05 |
| CH565724A5 (en, 2012) | 1975-08-29 |
| JPS4896505A (en, 2012) | 1973-12-10 |
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