SU318222A1 - - Google Patents

Info

Publication number

SU318222A1

SU318222A1 SU1313322A SU1313322A SU318222A1 SU 318222 A1 SU318222 A1 SU 318222A1 SU 1313322 A SU1313322 A SU 1313322A SU 1313322 A SU1313322 A SU 1313322A SU 318222 A1 SU318222 A1 SU 318222A1

Authority

SU

USSR - Soviet Union

Prior art keywords

alkyl

distilled water

dihydro

hydrogen

general formula

Prior art date

Links

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• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 11
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
• 125000000217 alkyl group Chemical group 0.000 description 6
• 239000012153 distilled water Substances 0.000 description 6
• 238000000034 method Methods 0.000 description 5
• WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
• 229910052739 hydrogen Inorganic materials 0.000 description 4
• 239000001257 hydrogen Substances 0.000 description 4
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• 150000001875 compounds Chemical class 0.000 description 3
• 239000000047 product Substances 0.000 description 3
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
• CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
• 125000003710 aryl alkyl group Chemical group 0.000 description 2
• 239000000284 extract Substances 0.000 description 2
• 150000002431 hydrogen Chemical class 0.000 description 2
• 239000003960 organic solvent Substances 0.000 description 2
• 239000000243 solution Substances 0.000 description 2
• 239000000725 suspension Substances 0.000 description 2
• YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
• LCGTWRLJTMHIQZ-UHFFFAOYSA-N 5H-dibenzo[b,f]azepine Chemical compound C1=CC2=CC=CC=C2NC2=CC=CC=C21 LCGTWRLJTMHIQZ-UHFFFAOYSA-N 0.000 description 1
• UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
• AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 1
• 239000013543 active substance Substances 0.000 description 1
• 229910052782 aluminium Inorganic materials 0.000 description 1
• WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
• 239000011260 aqueous acid Substances 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• XYOVOXDWRFGKEX-UHFFFAOYSA-N azepine Chemical compound N1C=CC=CC=C1 XYOVOXDWRFGKEX-UHFFFAOYSA-N 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 239000003518 caustics Substances 0.000 description 1
• 239000002826 coolant Substances 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 235000019441 ethanol Nutrition 0.000 description 1
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
• 238000001704 evaporation Methods 0.000 description 1
• 230000008020 evaporation Effects 0.000 description 1
• 238000002474 experimental method Methods 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 150000004678 hydrides Chemical class 0.000 description 1
• 238000006460 hydrolysis reaction Methods 0.000 description 1
• 238000002955 isolation Methods 0.000 description 1
• 239000012280 lithium aluminium hydride Substances 0.000 description 1
• -1 lithium aluminum hydride Chemical compound 0.000 description 1
• 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
• 235000019341 magnesium sulphate Nutrition 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• 239000008188 pellet Substances 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 239000011541 reaction mixture Substances 0.000 description 1
• 235000011121 sodium hydroxide Nutrition 0.000 description 1
• 239000007787 solid Substances 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1
• 238000003786 synthesis reaction Methods 0.000 description 1