SU222269A1 - - Google Patents

Info

Publication number

SU222269A1

SU222269A1 SU1166854A SU1166854A SU222269A1 SU 222269 A1 SU222269 A1 SU 222269A1 SU 1166854 A SU1166854 A SU 1166854A SU 1166854 A SU1166854 A SU 1166854A SU 222269 A1 SU222269 A1 SU 222269A1

Authority

SU

USSR - Soviet Union

Prior art keywords

acid

amino

allylamine

mol

thia

Prior art date

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• VVJKKWFAADXIJK-UHFFFAOYSA-N Allylamine Chemical compound NCC=C VVJKKWFAADXIJK-UHFFFAOYSA-N 0.000 claims description 13
• 238000000034 method Methods 0.000 claims description 10
• 239000000126 substance Substances 0.000 claims description 6
• CYVCWLWYKRJZII-UHFFFAOYSA-N 3-(3-aminopropylsulfanyl)propanoic acid Chemical compound NCCCSCCC(O)=O CYVCWLWYKRJZII-UHFFFAOYSA-N 0.000 claims description 5
• 150000002429 hydrazines Chemical class 0.000 claims description 2
• 239000002904 solvent Substances 0.000 claims description 2
• 239000011261 inert gas Substances 0.000 claims 1
• 238000004519 manufacturing process Methods 0.000 claims 1
• 239000002253 acid Substances 0.000 description 8
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
• 239000011541 reaction mixture Substances 0.000 description 6
• 239000000243 solution Substances 0.000 description 5
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
• 239000007864 aqueous solution Substances 0.000 description 4
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• 150000002825 nitriles Chemical class 0.000 description 3
• 239000000047 product Substances 0.000 description 3
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
• KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
• 238000004821 distillation Methods 0.000 description 2
• 150000002148 esters Chemical class 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 238000010992 reflux Methods 0.000 description 2
• 150000003839 salts Chemical class 0.000 description 2
• VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
• 150000007513 acids Chemical class 0.000 description 1
• QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 238000005341 cation exchange Methods 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 238000002425 crystallisation Methods 0.000 description 1
• 230000008025 crystallization Effects 0.000 description 1
• RIZMRRKBZQXFOY-UHFFFAOYSA-N ethion Chemical class CCOP(=S)(OCC)SCSP(=S)(OCC)OCC RIZMRRKBZQXFOY-UHFFFAOYSA-N 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 239000007787 solid Substances 0.000 description 1
• 239000007858 starting material Substances 0.000 description 1