SU210869A1 - - Google Patents

Info

Publication number

SU210869A1

SU210869A1 SU1105939A SU1105939A SU210869A1 SU 210869 A1 SU210869 A1 SU 210869A1 SU 1105939 A SU1105939 A SU 1105939A SU 1105939 A SU1105939 A SU 1105939A SU 210869 A1 SU210869 A1 SU 210869A1

Authority

SU

USSR - Soviet Union

Prior art keywords

trinitro

dichlorobenzene

trinitro1

chloroanisole

trinitrobenzene

Prior art date

Links

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• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
• KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
• 238000000034 method Methods 0.000 description 4
• VNOJQYPHLMLHGQ-UHFFFAOYSA-N 2,4-dichloro-1,3,5-trinitrobenzene Chemical compound [O-][N+](=O)C1=CC([N+]([O-])=O)=C(Cl)C([N+]([O-])=O)=C1Cl VNOJQYPHLMLHGQ-UHFFFAOYSA-N 0.000 description 2
• VMTPKDWABYEOPS-UHFFFAOYSA-N 2-chloro-4-methoxy-1,3,5-trinitrobenzene Chemical compound COC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C(Cl)=C1[N+]([O-])=O VMTPKDWABYEOPS-UHFFFAOYSA-N 0.000 description 2
• CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
• HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
• 238000006243 chemical reaction Methods 0.000 description 2
• 238000006140 methanolysis reaction Methods 0.000 description 2
• 239000000047 product Substances 0.000 description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
• WQNORCJSQCPHTP-UHFFFAOYSA-N 3-chloro-2,4,6-trinitrophenol Chemical compound OC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C(Cl)=C1[N+]([O-])=O WQNORCJSQCPHTP-UHFFFAOYSA-N 0.000 description 1
• 125000001309 chloro group Chemical class Cl* 0.000 description 1
• 229940117389 dichlorobenzene Drugs 0.000 description 1
• 238000007069 methylation reaction Methods 0.000 description 1
• 239000012452 mother liquor Substances 0.000 description 1
• 239000001103 potassium chloride Substances 0.000 description 1
• 235000011164 potassium chloride Nutrition 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 238000000746 purification Methods 0.000 description 1
• 238000001953 recrystallisation Methods 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1