SU202150A1 - - Google Patents

Info

Publication number

SU202150A1

SU202150A1 SU1117974A SU1117974A SU202150A1 SU 202150 A1 SU202150 A1 SU 202150A1 SU 1117974 A SU1117974 A SU 1117974A SU 1117974 A SU1117974 A SU 1117974A SU 202150 A1 SU202150 A1 SU 202150A1

Authority

SU

USSR - Soviet Union

Prior art keywords

alkyl

trimethylene

solution

hydrogen

benzene

Prior art date

Links

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• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 27
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 18
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 15
• 125000000217 alkyl group Chemical group 0.000 description 12
• 239000000243 solution Substances 0.000 description 11
• 235000019441 ethanol Nutrition 0.000 description 10
• 239000000203 mixture Substances 0.000 description 9
• 229910052739 hydrogen Inorganic materials 0.000 description 8
• 239000001257 hydrogen Substances 0.000 description 8
• 125000004435 hydrogen atom Chemical group [H]* 0.000 description 8
• 150000003839 salts Chemical class 0.000 description 8
• 239000002585 base Substances 0.000 description 7
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
• 238000009835 boiling Methods 0.000 description 6
• 239000002244 precipitate Substances 0.000 description 6
• 229910052783 alkali metal Inorganic materials 0.000 description 5
• -1 aliphatic alcohols Chemical class 0.000 description 4
• 125000003118 aryl group Chemical group 0.000 description 4
• 125000000623 heterocyclic group Chemical group 0.000 description 4
• 238000002360 preparation method Methods 0.000 description 4
• HYHCSLBZRBJJCH-UHFFFAOYSA-M sodium hydrosulfide Chemical compound [Na+].[SH-] HYHCSLBZRBJJCH-UHFFFAOYSA-M 0.000 description 4
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
• 239000002253 acid Substances 0.000 description 3
• 150000001340 alkali metals Chemical class 0.000 description 3
• 125000003545 alkoxy group Chemical group 0.000 description 3
• 229940100198 alkylating agent Drugs 0.000 description 3
• 239000002168 alkylating agent Substances 0.000 description 3
• 239000007864 aqueous solution Substances 0.000 description 3
• 125000001246 bromo group Chemical group Br* 0.000 description 3
• VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 3
• 150000004763 sulfides Chemical class 0.000 description 3
• CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
• LVZWSLJZHVFIQJ-UHFFFAOYSA-N Cyclopropane Chemical compound C1CC1 LVZWSLJZHVFIQJ-UHFFFAOYSA-N 0.000 description 2
• 125000001931 aliphatic group Chemical group 0.000 description 2
• 150000004945 aromatic hydrocarbons Chemical class 0.000 description 2
• 125000005605 benzo group Chemical group 0.000 description 2
• 150000001875 compounds Chemical class 0.000 description 2
• 238000001816 cooling Methods 0.000 description 2
• 150000008050 dialkyl sulfates Chemical class 0.000 description 2
• 239000000975 dye Substances 0.000 description 2
• 239000000839 emulsion Substances 0.000 description 2
• 239000013067 intermediate product Substances 0.000 description 2
• 239000007788 liquid Substances 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
• 230000003287 optical effect Effects 0.000 description 2
• 125000001424 substituent group Chemical group 0.000 description 2
• 229910021653 sulphate ion Inorganic materials 0.000 description 2
• 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 2
• DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
• ONWWZKCOTGEUKS-UHFFFAOYSA-N 1-methylidene-1,3-benzothiazole Chemical compound C=S1C=NC2=C1C=CC=C2 ONWWZKCOTGEUKS-UHFFFAOYSA-N 0.000 description 1
• SGHZXLIDFTYFHQ-UHFFFAOYSA-L Brilliant Blue Chemical compound [Na+].[Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 SGHZXLIDFTYFHQ-UHFFFAOYSA-L 0.000 description 1
• 240000002319 Citrus sinensis Species 0.000 description 1
• UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
• 241001061127 Thione Species 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
• JKLNYGDWYRKFKR-UHFFFAOYSA-N ethyl methyl sulfate Chemical compound CCOS(=O)(=O)OC JKLNYGDWYRKFKR-UHFFFAOYSA-N 0.000 description 1
• XOCMLLQOZSDGRB-UHFFFAOYSA-N ethyl perchlorate Chemical compound CCOCl(=O)(=O)=O XOCMLLQOZSDGRB-UHFFFAOYSA-N 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• MYWUZJCMWCOHBA-VIFPVBQESA-N methamphetamine Chemical compound CN[C@@H](C)CC1=CC=CC=C1 MYWUZJCMWCOHBA-VIFPVBQESA-N 0.000 description 1
• 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 1
• 239000013049 sediment Substances 0.000 description 1
• 229910052711 selenium Inorganic materials 0.000 description 1
• 229910052709 silver Inorganic materials 0.000 description 1
• 239000004332 silver Substances 0.000 description 1
• 125000000547 substituted alkyl group Chemical group 0.000 description 1
• 238000003786 synthesis reaction Methods 0.000 description 1