SU194099A1 - - Google Patents

Info

Publication number

SU194099A1

SU194099A1 SU1048636A SU1048636A SU194099A1 SU 194099 A1 SU194099 A1 SU 194099A1 SU 1048636 A SU1048636 A SU 1048636A SU 1048636 A SU1048636 A SU 1048636A SU 194099 A1 SU194099 A1 SU 194099A1

Authority

SU

USSR - Soviet Union

Prior art keywords

phenylenediamine

diphenyl

formic acid

acid

product

Prior art date

Links

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• BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 20
• OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 10
• 235000019253 formic acid Nutrition 0.000 description 10
• 239000000047 product Substances 0.000 description 10
• CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 8
• 239000002253 acid Substances 0.000 description 5
• 230000003287 optical effect Effects 0.000 description 5
• 239000002904 solvent Substances 0.000 description 5
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
• 238000001914 filtration Methods 0.000 description 3
• 238000000034 method Methods 0.000 description 3
• 239000002244 precipitate Substances 0.000 description 3
• 238000000746 purification Methods 0.000 description 3
• UTGQNNCQYDRXCH-UHFFFAOYSA-N N,N'-diphenyl-1,4-phenylenediamine Chemical compound C=1C=C(NC=2C=CC=CC=2)C=CC=1NC1=CC=CC=C1 UTGQNNCQYDRXCH-UHFFFAOYSA-N 0.000 description 2
• 239000004305 biphenyl Substances 0.000 description 2
• 238000004140 cleaning Methods 0.000 description 2
• 238000011109 contamination Methods 0.000 description 2
• 238000000926 separation method Methods 0.000 description 2
• 239000000725 suspension Substances 0.000 description 2
• ZNZCBZJTANSNGL-TVSHPJQCSA-N C1(=C(C=CC=C1)[2H])NC1=C(C=CC=C1)NC1=C(C=CC=C1)[2H] Chemical compound C1(=C(C=CC=C1)[2H])NC1=C(C=CC=C1)NC1=C(C=CC=C1)[2H] ZNZCBZJTANSNGL-TVSHPJQCSA-N 0.000 description 1
• 238000010306 acid treatment Methods 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 235000010290 biphenyl Nutrition 0.000 description 1
• 125000006267 biphenyl group Chemical group 0.000 description 1
• 238000004821 distillation Methods 0.000 description 1
• 230000000694 effects Effects 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 239000012535 impurity Substances 0.000 description 1
• 150000007522 mineralic acids Chemical class 0.000 description 1
• 230000007935 neutral effect Effects 0.000 description 1
• 150000007524 organic acids Chemical class 0.000 description 1
• 235000005985 organic acids Nutrition 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 230000003647 oxidation Effects 0.000 description 1
• 238000007254 oxidation reaction Methods 0.000 description 1
• ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
• BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
• 238000003786 synthesis reaction Methods 0.000 description 1