SU156556A1 - - Google Patents

Info

Publication number

SU156556A1

SU156556A1 SU788408A SU788408A SU156556A1 SU 156556 A1 SU156556 A1 SU 156556A1 SU 788408 A SU788408 A SU 788408A SU 788408 A SU788408 A SU 788408A SU 156556 A1 SU156556 A1 SU 156556A1

Authority

SU

USSR - Soviet Union

Prior art keywords

piperidine

yield

formylpiperidine

catalyst

pressure

Prior art date

Links

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• NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 description 10
• FEWLNYSYJNLUOO-UHFFFAOYSA-N 1-Piperidinecarboxaldehyde Chemical compound O=CN1CCCCC1 FEWLNYSYJNLUOO-UHFFFAOYSA-N 0.000 description 8
• WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 8
• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
• 239000003054 catalyst Substances 0.000 description 5
• 238000000034 method Methods 0.000 description 5
• 230000006315 carbonylation Effects 0.000 description 3
• 238000005810 carbonylation reaction Methods 0.000 description 3
• PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
• UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 229910002091 carbon monoxide Inorganic materials 0.000 description 1
• 238000004821 distillation Methods 0.000 description 1
• 239000007789 gas Substances 0.000 description 1
• 229910052759 nickel Inorganic materials 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 229910052708 sodium Inorganic materials 0.000 description 1
• 239000011734 sodium Substances 0.000 description 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1