SU1323952A1 - Способ изготовлени стекл нных капилл рных хроматографических колонок - Google Patents
Способ изготовлени стекл нных капилл рных хроматографических колонок Download PDFInfo
- Publication number
- SU1323952A1 SU1323952A1 SU864015377A SU4015377A SU1323952A1 SU 1323952 A1 SU1323952 A1 SU 1323952A1 SU 864015377 A SU864015377 A SU 864015377A SU 4015377 A SU4015377 A SU 4015377A SU 1323952 A1 SU1323952 A1 SU 1323952A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- column
- capillary
- purging
- boron trifluoride
- glass capillary
- Prior art date
Links
- 239000011521 glass Substances 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 15
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 claims abstract description 11
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000007791 liquid phase Substances 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims abstract description 6
- 229910015900 BF3 Inorganic materials 0.000 claims abstract description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000001257 hydrogen Substances 0.000 claims abstract description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 4
- AIYUHDOJVYHVIT-UHFFFAOYSA-M caesium chloride Chemical compound [Cl-].[Cs+] AIYUHDOJVYHVIT-UHFFFAOYSA-M 0.000 claims abstract description 4
- 239000001301 oxygen Substances 0.000 claims abstract description 4
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 4
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 claims abstract 6
- 238000010926 purge Methods 0.000 claims abstract 4
- 238000002386 leaching Methods 0.000 claims abstract 3
- 239000005051 trimethylchlorosilane Substances 0.000 claims abstract 3
- 229910052736 halogen Inorganic materials 0.000 claims abstract 2
- 238000005406 washing Methods 0.000 claims abstract 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 10
- 229910052786 argon Inorganic materials 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 claims description 3
- 239000005297 pyrex Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 239000012071 phase Substances 0.000 claims description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000002367 halogens Chemical class 0.000 claims 1
- 150000004756 silanes Chemical class 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- HNQXCHVZYRDHJN-UHFFFAOYSA-N cyanosilicon Chemical compound [Si]C#N HNQXCHVZYRDHJN-UHFFFAOYSA-N 0.000 abstract description 3
- 229920006395 saturated elastomer Polymers 0.000 abstract description 3
- 239000011261 inert gas Substances 0.000 abstract 2
- -1 halogen derivative of silane Chemical class 0.000 abstract 1
- 238000012986 modification Methods 0.000 abstract 1
- 230000004048 modification Effects 0.000 abstract 1
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
- 230000003068 static effect Effects 0.000 description 4
- 239000012153 distilled water Substances 0.000 description 2
- QABCGOSYZHCPGN-UHFFFAOYSA-N chloro(dimethyl)silicon Chemical compound C[Si](C)Cl QABCGOSYZHCPGN-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
Landscapes
- Polymerisation Methods In General (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU864015377A SU1323952A1 (ru) | 1986-01-21 | 1986-01-21 | Способ изготовлени стекл нных капилл рных хроматографических колонок |
| CS87423A CS268710B1 (cs) | 1986-01-21 | 1987-01-21 | Způsob nanášeni stacionární kapalné fáze do skleněné nebo křemenné kapiláry chromatografické kolony |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU864015377A SU1323952A1 (ru) | 1986-01-21 | 1986-01-21 | Способ изготовлени стекл нных капилл рных хроматографических колонок |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1323952A1 true SU1323952A1 (ru) | 1987-07-15 |
Family
ID=21219079
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU864015377A SU1323952A1 (ru) | 1986-01-21 | 1986-01-21 | Способ изготовлени стекл нных капилл рных хроматографических колонок |
Country Status (2)
| Country | Link |
|---|---|
| CS (1) | CS268710B1 (cs) |
| SU (1) | SU1323952A1 (cs) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2356048C2 (ru) * | 2007-06-13 | 2009-05-20 | Государственное образовательное учреждение высшего профессионального образования "Самарский государственный университет" | Способ получения капиллярных колонок и устройство для его осуществления |
| RU2391303C1 (ru) * | 2008-11-05 | 2010-06-10 | Институт аналитического приборостроения Российской Академии Наук (ИАнП РАН) | Способ удаления внешнего полиимидного покрытия кварцевого капилляра |
-
1986
- 1986-01-21 SU SU864015377A patent/SU1323952A1/ru active
-
1987
- 1987-01-21 CS CS87423A patent/CS268710B1/cs unknown
Non-Patent Citations (1)
| Title |
|---|
| Патент US № 4376641, кл. G 01 N 31/08, 1980. Авторское свидетельство СССР № 817582, кл. G 01 N 30/50, 1980. * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2356048C2 (ru) * | 2007-06-13 | 2009-05-20 | Государственное образовательное учреждение высшего профессионального образования "Самарский государственный университет" | Способ получения капиллярных колонок и устройство для его осуществления |
| RU2391303C1 (ru) * | 2008-11-05 | 2010-06-10 | Институт аналитического приборостроения Российской Академии Наук (ИАнП РАН) | Способ удаления внешнего полиимидного покрытия кварцевого капилляра |
Also Published As
| Publication number | Publication date |
|---|---|
| CS268710B1 (cs) | 1990-04-11 |
| CS42387A1 (en) | 1989-09-12 |
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