SU1212952A1 - Method of removing ferrum from zirconium tetrachloride - Google Patents
Method of removing ferrum from zirconium tetrachloride Download PDFInfo
- Publication number
- SU1212952A1 SU1212952A1 SU833670471A SU3670471A SU1212952A1 SU 1212952 A1 SU1212952 A1 SU 1212952A1 SU 833670471 A SU833670471 A SU 833670471A SU 3670471 A SU3670471 A SU 3670471A SU 1212952 A1 SU1212952 A1 SU 1212952A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- zirconium tetrachloride
- ampoule
- tetrachloride
- removing ferrum
- fecl
- Prior art date
Links
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Description
ч 1h 1
Изобретение относитс к неорганической химии и может быть использовано в технологии циркони и его .соединений.This invention relates to inorganic chemistry and can be used in the technology of zirconium and its compounds.
Цель изобретени - ускорение про-, цесса очистки.The purpose of the invention is to accelerate the cleaning process.
Пример 1. Исходный продукт, содержащий 2,20 г ZrCl и 1,2 мг FeCl (исходное содержание FeCl, 0,055 мас.%) помещают в стекл нную ампулу объемом 300 см, ампулу эвакуируют до остаточного давлени Example 1. A starting material containing 2.20 g of ZrCl and 1.2 mg of FeCl (initial content of FeCl, 0.055% by weight) was placed in a 300 cm glass ampoule, the ampoule was evacuated to a residual pressure.
.10.ten
-2-2
ММ рт.ст. и заполн ют з лоромMmHg. and filled with dust
(так, чтобы его давление при температуре перекристаллизации составило 100 мм рт.ст.). Запа нную ампулу помещают на 50 ч в вертик;альном положении в термостат при 260°С. После завершени термостатировани ампулу быстро перенос т в емкость с холодной водой и далее после тщательного удалени воды со стенок ампулы(so that its pressure at the recrystallization temperature is 100 mm Hg). The sealed ampoule is placed for 50 hours in a vertical position in a thermostat at 260 ° C. After thermostating is complete, the ampoule is quickly transferred to a container of cold water and then after thoroughly removing water from the walls of the ampoule.
21295222129522
в сухой камере ее вскрывают и отдел ют сконденсировавшиес на стенках пары FeCl с примесью ЕгСЦ от основной массы ZrCl, оставшейс на дне 5 ампулы в виде, твердого вещества.in a dry chamber, it is opened and the FeCl vapor mixed with EGC from the main mass of ZrCl, remaining at the bottom of the 5 ampoule in the form of a solid substance, condensed on the walls of the cell is separated.
Получают 2,10 г ZrCl с содержанием железа (в расчете на FeCl) 0,0024 мас.% (анализ на железо провод т радиометрически с использова- 10 нием радионуклидов ) .2.10 g of ZrCl with an iron content (calculated as FeCl) of 0.0024 wt.% Are obtained (the analysis for iron is carried out radiometrically using 10 radionuclides).
Пример 2. В услови х примера 1 провод т очистку с измельчением «продукта. На дно ампулы поме- 15 щают тетрахлорид циркони и 3 стекл нных шарика диаметром 5 мм. Ампулу в процессе термостатировани в} ащают со скоростью 3 об./с. ка на уровне примера 1 достигнута 20 за 2 ч.Example 2. Under the conditions of Example 1, the purification was performed by grinding the "product. Zirconium tetrachloride and 3 glass beads with a diameter of 5 mm are placed at the bottom of the ampoule. The ampoule in the process of thermostating is set at a speed of 3 vol / s. ka at the level of example 1 reached 20 in 2 hours.
Результаты опытов приведены в таблице.The results of the experiments are given in the table.
Редактор И.ДербакEditor I. Derbak
Составитель В.Дубровска Compiled by V.Dubrovska
Техред М.Пароцай Корректор 0.Лугова Tehred M. Parotsay Proofreader 0. Lugov
Заказ 716/31Тираж 452ПодписноеOrder 716/31 Circulation 452Subscription
ВНИИПИ Государственного комитета СССРVNIIPI USSR State Committee
по делам изобретений и открытий 113035, Москва, Ж--35, Раушска наб.,, д. 4/5for inventions and discoveries 113035, Moscow, F - 35, Raushsk nab., d. 4/5
Филиал ППП Патент, г.Ужгород, ул.Проектна , 4Branch PPP Patent, Uzhgorod, Proektna St., 4
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU833670471A SU1212952A1 (en) | 1983-12-01 | 1983-12-01 | Method of removing ferrum from zirconium tetrachloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU833670471A SU1212952A1 (en) | 1983-12-01 | 1983-12-01 | Method of removing ferrum from zirconium tetrachloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1212952A1 true SU1212952A1 (en) | 1986-02-23 |
Family
ID=21092133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU833670471A SU1212952A1 (en) | 1983-12-01 | 1983-12-01 | Method of removing ferrum from zirconium tetrachloride |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU1212952A1 (en) |
-
1983
- 1983-12-01 SU SU833670471A patent/SU1212952A1/en active
Non-Patent Citations (1)
| Title |
|---|
| Патент US № 2953433, кл. 23-87, 1960. Патент US № 2946654, кл. 23-87, 1960. * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| FI61136C (en) | OVER ANCHORING OVERCLOSING AV AVASTER | |
| US3084995A (en) | Process for storage of chlorine dioxide | |
| SE8306843D0 (en) | DEVICE AND DEVICE FOR HEAT TREATMENT OF ORGANIC MATERIAL | |
| JPH01261208A (en) | Method for purifying nitrogen trifluoride gas | |
| DE3062847D1 (en) | Counter-current process for the treatment of liquids with ion-exchange materials and ion-exchange filter for carrying out the process | |
| SU661994A3 (en) | Method of processing tobacco | |
| FR2502382A1 (en) | PROCESS FOR THE FINAL TREATMENT OF A RADIO-ACTIVE ORGANIC MATTER | |
| PT81684A (en) | Process for isolating phosphatidylcholine free of lysophosphatidylcholine from egg powder | |
| SU1212952A1 (en) | Method of removing ferrum from zirconium tetrachloride | |
| DE3575679D1 (en) | METHOD FOR ULTRA DRYING A GAS. | |
| GB1410142A (en) | Method of producing bubble-free and oh-group free transparent fused silica and apparatus for putting the method into effect | |
| Swindell et al. | Extensively rearranged derivatives of sulfur tetrafluoride, trifluoromethylsulfur trifluoride, and bis (trifluoromethyl) sulfur difluoride from hexafluoroisopropylideniminolithium reactions | |
| Brauns | Optical rotation and atomic dimension. Experimental progress on the walden inversion | |
| SU715458A1 (en) | Method of producing ferromagnetic carbon adsorbent | |
| GB834383A (en) | Improvements in or relating to methods of removing impurities from silica | |
| Owen | 1071. The pyrolysis of decaborane | |
| CA1052292A (en) | Removal of hydrogen fluoride from gaseous mixture by absorption on alkaline earth metal fluoride | |
| RU2004491C1 (en) | Method for cleaning detonation diamonds | |
| US2733124A (en) | Rosenfeld | |
| US3172724A (en) | Production of stannous fluoride | |
| SU893870A1 (en) | Method of dehydrating cupric diflhoride | |
| SU785288A1 (en) | Method of purifying carbon tetrachloride from sulfur chlorides | |
| GB829857A (en) | Process and apparatus for vaporization of nitric acid | |
| SU977384A1 (en) | Method of determining tritium in lithium-containing materials | |
| RU2056346C1 (en) | Method of calcium superoxide producing |