SU1176840A3 - Способ получени фурфурола - Google Patents
Способ получени фурфурола Download PDFInfo
- Publication number
- SU1176840A3 SU1176840A3 SU813273771A SU3273771A SU1176840A3 SU 1176840 A3 SU1176840 A3 SU 1176840A3 SU 813273771 A SU813273771 A SU 813273771A SU 3273771 A SU3273771 A SU 3273771A SU 1176840 A3 SU1176840 A3 SU 1176840A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- furfural
- strong mineral
- mineral acid
- acid
- steam
- Prior art date
Links
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 238000000034 method Methods 0.000 title claims abstract description 11
- 239000002253 acid Substances 0.000 claims abstract description 13
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 9
- 150000002972 pentoses Chemical class 0.000 claims abstract description 9
- 230000007062 hydrolysis Effects 0.000 claims abstract description 8
- 230000018044 dehydration Effects 0.000 claims abstract description 5
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 5
- 238000010908 decantation Methods 0.000 claims abstract description 3
- 238000000926 separation method Methods 0.000 claims abstract description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract 7
- 239000011707 mineral Substances 0.000 claims abstract 7
- 239000000463 material Substances 0.000 claims abstract 3
- 238000009833 condensation Methods 0.000 claims abstract 2
- 230000005494 condensation Effects 0.000 claims abstract 2
- XPFVYQJUAUNWIW-UHFFFAOYSA-N furfuryl alcohol Chemical compound OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 230000036571 hydration Effects 0.000 claims 1
- 238000006703 hydration reaction Methods 0.000 claims 1
- 239000002994 raw material Substances 0.000 abstract description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 3
- 240000008042 Zea mays Species 0.000 description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 3
- 235000005822 corn Nutrition 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 239000000356 contaminant Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005903 acid hydrolysis reaction Methods 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- LBPYPRXFFYUUSI-UHFFFAOYSA-N furan-2-carbaldehyde;hydrate Chemical compound O.O=CC1=CC=CO1 LBPYPRXFFYUUSI-UHFFFAOYSA-N 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
- 239000004758 synthetic textile Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
- C07D307/50—Preparation from natural products
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Furan Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7919935A FR2462433A1 (fr) | 1979-08-03 | 1979-08-03 | Perfectionnements apportes aux procedes et aux appareillages pour l'obtention de furfural a partir de matieres vegetales |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1176840A3 true SU1176840A3 (ru) | 1985-08-30 |
Family
ID=9228585
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU813273771A SU1176840A3 (ru) | 1979-08-03 | 1981-04-02 | Способ получени фурфурола |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4366322A (enExample) |
| EP (1) | EP0033323B1 (enExample) |
| JP (1) | JPS56501046A (enExample) |
| BR (1) | BR8008782A (enExample) |
| DE (1) | DE3068793D1 (enExample) |
| FR (1) | FR2462433A1 (enExample) |
| HU (1) | HU185421B (enExample) |
| IN (1) | IN153609B (enExample) |
| SU (1) | SU1176840A3 (enExample) |
| WO (1) | WO1981000407A1 (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2608609C2 (ru) * | 2011-06-22 | 2017-01-23 | Басф Се | Способ дегидратации углеводсодержащих композиций |
| RU2723875C1 (ru) * | 2019-10-22 | 2020-06-17 | Виктор Владимирович Васильев | Способ получения фурфурольной смолы на основе гемицеллюлоз растительного сырья для склеивания древесных материалов |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2600063A1 (fr) * | 1986-06-11 | 1987-12-18 | Technip Cie | Procede et installation de traitement des matieres vegetales pour produire notamment du furfural |
| AT387408B (de) * | 1987-05-12 | 1989-01-25 | Voest Alpine Ind Anlagen | Kombiniertes verfahren zur thermischen und chemischen behandlung von lignocellulosehaltiger biomasse und zur gewinnung von furfural |
| AT387247B (de) * | 1987-05-12 | 1988-12-27 | Voest Alpine Ind Anlagen | Kombiniertes verfahren zur thermischen und chemischen behandlung von lignocellulosehaltiger biomasse und zur gewinnung von furfural |
| US5559031A (en) * | 1987-08-12 | 1996-09-24 | Technipetrol S.P.A. | Apparatus for the continuous production of ethanol from cereals |
| DE19905655A1 (de) * | 1999-02-11 | 2000-08-17 | Karl Zeitsch | Verfahren zur Herstellung von Furfural durch verzögerte Entspannung |
| GB0601828D0 (en) * | 2006-01-31 | 2006-03-08 | Tapper Company The Ltd S | A Method Of Heat Generation |
| CN1872726A (zh) * | 2006-06-07 | 2006-12-06 | 济南圣泉集团股份有限公司 | 一种糠醛生产废水的处理方法 |
| UA98002C2 (uk) * | 2007-09-07 | 2012-04-10 | Фураникс Технолоджиз Б.В. | Спосіб одержання суміші похідних фурфуралю і 5-алкоксиметилфурфуралю та паливо, що містить таку суміш |
| CN101130532B (zh) * | 2007-09-24 | 2010-11-24 | 济南圣泉集团股份有限公司 | 利用农林废弃物生产糠醛的系统及方法 |
| US8119823B2 (en) * | 2008-07-16 | 2012-02-21 | Renmatix, Inc. | Solvo-thermal hydrolysis of xylose |
| US8282738B2 (en) * | 2008-07-16 | 2012-10-09 | Renmatix, Inc. | Solvo-thermal fractionation of biomass |
| US8546560B2 (en) | 2008-07-16 | 2013-10-01 | Renmatix, Inc. | Solvo-thermal hydrolysis of cellulose |
| BRPI0915930A2 (pt) | 2008-07-16 | 2015-11-03 | Sriya Innovations Inc | método para produção de pelo menos um de glicose e furfural, processo para produção de um produto como xilose e celulose a partir de uma biomassa, processo para hidrolisar celulose e composição compreendendo um produto de hidrólise de celulose |
| FR2936803B1 (fr) | 2008-10-06 | 2012-09-28 | Arkema France | Copolymere a blocs issu de matieres renouvelables et procede de fabrication d'un tel copolymere a blocs. |
| CN105525043B (zh) | 2010-01-19 | 2021-03-19 | 瑞恩麦特克斯股份有限公司 | 使用超临界流体从生物质产生可发酵的糖和木质素 |
| WO2012038968A1 (en) | 2010-09-03 | 2012-03-29 | Ganapati Dadasaheb Yadav | Process for production of furfural from xylose using a heterogeneous mesoporous silica catalyst comprising rare earth metals |
| NL2005588C2 (en) | 2010-10-27 | 2012-05-01 | Univ Delft Tech | Process for the production of furfural from pentoses. |
| WO2012088208A2 (en) * | 2010-12-21 | 2012-06-28 | E. I. Du Pont De Nemours And Company | Methods for furfural production from branched non-fermentable sugars in stillage or syrup |
| US8801859B2 (en) | 2011-05-04 | 2014-08-12 | Renmatix, Inc. | Self-cleaning apparatus and method for thick slurry pressure control |
| MY171010A (en) | 2011-05-04 | 2019-09-23 | Renmatix Inc | Lignin production from lignocellulosic biomass |
| EP2797906A4 (en) | 2011-12-28 | 2015-06-03 | Du Pont | PROCESS FOR THE PREPARATION OF FURFURAL |
| WO2013102027A1 (en) | 2011-12-28 | 2013-07-04 | E. I. Du Pont De Nemours And Company | Process for the production of furfural |
| WO2013102007A1 (en) * | 2011-12-28 | 2013-07-04 | E. I. Du Pont De Nemours And Company | Process for the production of furfural |
| BR112014016001B8 (pt) | 2011-12-28 | 2019-06-25 | Du Pont | processos |
| US9181210B2 (en) | 2011-12-28 | 2015-11-10 | E I Du Pont De Nemours And Company | Processes for making furfurals |
| US8759498B2 (en) | 2011-12-30 | 2014-06-24 | Renmatix, Inc. | Compositions comprising lignin |
| FR3006687B1 (fr) * | 2013-06-05 | 2015-07-17 | Agro Ind Rech S Et Dev Ard | Procede de production de furfural a partir de biomasse lignocellulosique |
| NL2012819B1 (en) | 2014-05-15 | 2016-03-02 | Univ Delft Tech | Method and Apparatus for Furfural Production. |
| EP4357404A3 (en) | 2014-09-26 | 2024-11-27 | Renmatix Inc. | Cellulose-containing compositions and methods of making same |
| CN108929291A (zh) * | 2017-05-23 | 2018-12-04 | 宁津春蕾生物科技有限公司 | 糠醛的生产工艺 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1735084A (en) * | 1922-09-07 | 1929-11-12 | Quaker Oats Co | Process of manufacturing furfural |
| BE379408A (enExample) * | 1930-04-28 | |||
| DE719704C (de) * | 1936-06-20 | 1942-04-15 | Henkel & Cie Gmbh | Verfahren zur Herstellung von Furfuerol |
| DE740602C (de) * | 1941-02-25 | 1943-11-01 | Chem Fab Loewenberg Dr Warth & | Verfahren zur Herstellung von Furfurol aus Pentosen |
| BE505571A (enExample) * | 1950-09-01 | |||
| GB922685A (en) * | 1960-06-17 | 1963-04-03 | Ledoga Spa | Improvements in or relating to the extraction of xylose from vegetable material |
| US4001283A (en) * | 1974-09-23 | 1977-01-04 | Wells Jr Preston A | Method for the manufacture of furfural using hydrogen chloride |
-
1979
- 1979-08-03 FR FR7919935A patent/FR2462433A1/fr active Pending
-
1980
- 1980-07-31 DE DE8080901462T patent/DE3068793D1/de not_active Expired
- 1980-07-31 WO PCT/FR1980/000128 patent/WO1981000407A1/fr not_active Ceased
- 1980-07-31 US US06/253,851 patent/US4366322A/en not_active Expired - Fee Related
- 1980-07-31 HU HU811146A patent/HU185421B/hu unknown
- 1980-07-31 JP JP50178580A patent/JPS56501046A/ja active Pending
- 1980-07-31 BR BR8008782A patent/BR8008782A/pt unknown
- 1980-11-18 IN IN1285/CAL/80A patent/IN153609B/en unknown
-
1981
- 1981-02-24 EP EP80901462A patent/EP0033323B1/fr not_active Expired
- 1981-04-02 SU SU813273771A patent/SU1176840A3/ru active
Non-Patent Citations (1)
| Title |
|---|
| Патент Германии № 740602, кл. 12 q 24, опублик.I943. Патент FR № 1181953, кл. С 07 j , опублик.1959. * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2608609C2 (ru) * | 2011-06-22 | 2017-01-23 | Басф Се | Способ дегидратации углеводсодержащих композиций |
| RU2723875C1 (ru) * | 2019-10-22 | 2020-06-17 | Виктор Владимирович Васильев | Способ получения фурфурольной смолы на основе гемицеллюлоз растительного сырья для склеивания древесных материалов |
Also Published As
| Publication number | Publication date |
|---|---|
| WO1981000407A1 (fr) | 1981-02-19 |
| US4366322A (en) | 1982-12-28 |
| EP0033323B1 (fr) | 1984-08-01 |
| BR8008782A (pt) | 1981-05-26 |
| IN153609B (enExample) | 1984-07-28 |
| HU185421B (en) | 1985-02-28 |
| DE3068793D1 (en) | 1984-09-06 |
| FR2462433A1 (fr) | 1981-02-13 |
| EP0033323A1 (fr) | 1981-08-12 |
| JPS56501046A (enExample) | 1981-07-30 |
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