SU104860A1 - Apparatus for continuous distillation and separation of liquid mixtures under vacuum - Google Patents

Apparatus for continuous distillation and separation of liquid mixtures under vacuum

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Publication number
SU104860A1
SU104860A1 SU453818A SU453818A SU104860A1 SU 104860 A1 SU104860 A1 SU 104860A1 SU 453818 A SU453818 A SU 453818A SU 453818 A SU453818 A SU 453818A SU 104860 A1 SU104860 A1 SU 104860A1
Authority
SU
USSR - Soviet Union
Prior art keywords
separation
under vacuum
continuous distillation
column
liquid mixtures
Prior art date
Application number
SU453818A
Other languages
Russian (ru)
Inventor
В.В. Васильев
Н.Н. Попов
К.И. Цирков
Original Assignee
В.В. Васильев
Н.Н. Попов
К.И. Цирков
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by В.В. Васильев, Н.Н. Попов, К.И. Цирков filed Critical В.В. Васильев
Priority to SU453818A priority Critical patent/SU104860A1/en
Application granted granted Critical
Publication of SU104860A1 publication Critical patent/SU104860A1/en

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

Предметом изобретени   вл етс  аппарат дл  непрерывной перегонки и разделени  жидких смесей под вакуумом, Шзшолненный в виде вертикальной колонны с отражателем .The subject of the invention is an apparatus for continuous distillation and separation of liquid mixtures under vacuum, filled in a vertical column with a reflector.

По сравнению с известными предлагаемый аппарат имеет преимущество , которое заключаетс  в обеспечении интенсивного и краткозреAiCHHoro воздействи  пара на распыленную обрабатываемую смесь.In comparison with the known ones, the proposed apparatus has the advantage of providing an intense and short-term effect of steam on the sprayed mixture to be treated.

Особенность аппарата состоит в том, что дл  подвода обрабатываемой смеси применены распылительные паровые форсунки, установленные в нижней частп колонны .The peculiarity of the apparatus is that spray steam nozzles installed in the lower part of the column are used to supply the treated mixture.

В аппарате применены расиоложенный по оси ко.таины над отражателем жалюзийный лабиринт и концентрично ему размещенньп теплообменник, заключенны) в кожух .In the apparatus, the louvered labyrinth, rationalized along the axis of the complex above the reflector, is applied and the heat exchanger placed concentrically in it, enclosed) in a casing.

На чертеже изображе)а схема аппарата .In the drawing image) a diagram of the apparatus.

Аипарат выполнен в виде колонь Ы /, зах.пючепно в чожух 2 и снабженной отражателем 3. В нижней части колонны установлены паровые распылительные qbopcyHKn 4, например, ч т-смы Шухова.The device is made in the form of columns N /, zap.pyuchepno to chuzhuh 2 and equipped with a reflector 3. In the lower part of the column there are steam spray qbopcyHKn 4, for example, Shukhov metropolitan hours.

В верхней части кожуха 2, по оси колонны 1, монтирован жалюзпйный лабиринт 5 и концентрично ему рамещен теплообменник 6.In the upper part of the casing 2, along the axis of the column 1, the louvered labyrinth 5 is mounted and the heat exchanger 6 is concentric with it.

В аппарате с помош,ью эжекторHoii установки (на схе.ме не показана ) создаетс  глубоки вакуум.In the apparatus, with the help of a new unit ejector (not shown in the diagram), a deep vacuum is created.

Жидка  смесь, подогрета  в теплообменнике 6, вместе с острым, перегретым до 220 паром через патрубки 7 подаетс  в форсунки 4 и распыл етс  в паход щуюс  под вакуумом колонну /.The liquid mixture, preheated in the heat exchanger 6, together with the sharp, superheated steam to 220 through the nozzles 7 is fed to the nozzles 4 and sprayed into a column under vacuum.

При этом из смеси распылениых жидкостей выдел ютс  летучис компоненты, которые устремл ютс  вверх и, проход  через жалюзий ный лабиринт, отдают свое тепло поступающим на обработку по трубам теплообменника 6 смес м жи.а,костей , конденсируютс  и стекают в сборник S. Нескондеисировавщиес  газы отвод тс  по трубе 9.At the same time, volatile components are released from the mixture of sprayed liquids, which rush upward and, passing through the lamellar labyrinth, give up their heat to the treatment through the heat exchanger 6 of the mixtures of mi and bones, condense and drain into the collection S. Non-condensable gases pipe tap 9.

Освободивша с  от летучих компонентов жидкость с помощью отражател  3 направл етс  на стенк кожуха 2, стекает на дно и выводитс  нз аипарата через патрубок 10.The liquid freed from volatile components by means of the reflector 3 is directed onto the wall of the casing 2, flows down to the bottom and is discharged from the device through the nozzle 10.

При необходимости аппараты мо. гут быть последовательно соединены в батарею.If necessary, the apparatus mo. can be connected in series to the battery.

Предмет изобретени Subject invention

Claims (2)

1. Аппарат дл  непрерывной перегонки и разделени  жидких емесси под вакуумом, выполненный в виде вертикальной колонны с отражателем , отличающийс  тем, что, с целью обеспечени  интенсивного и кратковременного воздействи  пара на распыленную обрабатываемую смесь, дл  подвода последней1. An apparatus for continuous distillation and separation of liquids by vacuum under a vacuum, made in the form of a vertical column with a reflector, characterized in that, in order to ensure an intense and short-term effect of steam on the sprayed mixture to be processed, применены распылительные паровые форсунки, установленные в нижней части колонны.spray nozzles installed at the bottom of the column were used. 2. В аппарате/ по п. 1 применение дл  рекуперации тепла отход щих паров расположенного по оси колонны над отражателем жалюзийного лабиринта и размещенного коицентрично ему теплообменника, заключенного в кожух.2. In the apparatus / in accordance with claim 1, the application for heat recovery of waste vapor of the column located along the axis of the louver labyrinth above the reflector and placed in the center of the heat exchanger encased in a casing.
SU453818A 1956-01-16 1956-01-16 Apparatus for continuous distillation and separation of liquid mixtures under vacuum SU104860A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU453818A SU104860A1 (en) 1956-01-16 1956-01-16 Apparatus for continuous distillation and separation of liquid mixtures under vacuum

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU453818A SU104860A1 (en) 1956-01-16 1956-01-16 Apparatus for continuous distillation and separation of liquid mixtures under vacuum

Publications (1)

Publication Number Publication Date
SU104860A1 true SU104860A1 (en) 1956-11-30

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Family Applications (1)

Application Number Title Priority Date Filing Date
SU453818A SU104860A1 (en) 1956-01-16 1956-01-16 Apparatus for continuous distillation and separation of liquid mixtures under vacuum

Country Status (1)

Country Link
SU (1) SU104860A1 (en)

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