SI2880190T1 - Postopek proizvodnje silicijeve jeklene pločevine z orientiranimi zrni, električna jeklena pločevina z orientiranimi zrni in njena uporaba - Google Patents

Postopek proizvodnje silicijeve jeklene pločevine z orientiranimi zrni, električna jeklena pločevina z orientiranimi zrni in njena uporaba Download PDF

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SI2880190T1
SI2880190T1 SI201330978T SI201330978T SI2880190T1 SI 2880190 T1 SI2880190 T1 SI 2880190T1 SI 201330978 T SI201330978 T SI 201330978T SI 201330978 T SI201330978 T SI 201330978T SI 2880190 T1 SI2880190 T1 SI 2880190T1
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steel sheet
cold
temperature
rolled
steel
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Ban Gabor
De Putte Tom Van
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Arcelormittal
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/12Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
    • H01F1/14Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
    • H01F1/147Alloys characterised by their composition
    • H01F1/14766Fe-Si based alloys
    • H01F1/14775Fe-Si based alloys in the form of sheets
    • H01F1/14783Fe-Si based alloys in the form of sheets with insulating coating
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    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
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    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1205Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties involving a particular fabrication or treatment of ingot or slab
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    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1216Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the working step(s) being of interest
    • C21D8/1222Hot rolling
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    • C21METALLURGY OF IRON
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    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1216Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the working step(s) being of interest
    • C21D8/1233Cold rolling
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    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1244Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
    • C21D8/1261Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest following hot rolling
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    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1244Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
    • C21D8/1272Final recrystallisation annealing
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    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1277Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties involving a particular surface treatment
    • C21D8/1283Application of a separating or insulating coating
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    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/46Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals
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    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/001Ferrous alloys, e.g. steel alloys containing N
    • CCHEMISTRY; METALLURGY
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    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/002Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
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    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
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    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
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    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/16Ferrous alloys, e.g. steel alloys containing copper
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    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F27/00Details of transformers or inductances, in general
    • H01F27/24Magnetic cores
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    • C21D2201/00Treatment for obtaining particular effects
    • C21D2201/05Grain orientation
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    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/004Dispersions; Precipitations

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  • Manufacturing Of Steel Electrode Plates (AREA)
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Claims (11)

  1. Postopek proizvodnje silicijeve jeklene pločevine z orientiranimi zrni, električna jeklena pločevina z orientiranimi zrni in njena uporaba Patentni zahtevki
    1. Postopek proizvodnje hladno valjanje Fe-Si jeklene pločevine, ki obsega zaporedne stopnje, ki sestojijo iz: - taljenja jeklenega sestavka, ki vsebuje, v masnih odstotkih: 2,8 s Si s 4 0,4 ž Cu s 0,6 0,05 s Mn s 0,4 0,001 S Al S 0,04 0,025 žCž 0,05 0,005 SNS 0,02 0,005 s Sn ž 0,03 S <0,015 in po izbiri Ti, Nb, V ali B v skupni količini pod 0,02, pri čemer so upoštevana naslednja razmerja: Mn/Sn s 40 2,0 s C/N s 5,0 Al/N ž 1,20, in pri čemer so preostanek Fe in druge neizogibne nečistote; in proizvodnje brame, ki ima debelino ne več kot 80 mm, tako da se po strditvi površina navedene brame ne ohladi pod 850 °C za več kot 5 minut, ponovno segrevanje navedene brame do temperature med 1080 °C in 1200 °C za vsaj 20 minut, nato toplo valjanje navedene brame, pri čemer poteče prvo zmanjšanje debeline, medtem ko je temperatura navedene brame nad 1060 °C in poteče zadnje zmanjšanje debeline nad temperaturo dovršilnega valjanja 950 °C z namenom, da dobimo topel trak, ohlajanje navedenega toplega traku na temperaturo med 500 °C in 600 °C v manj kot 10 sekundah, nato navijanje toplega traku, kjer topel trak Fe-Si vsebuje manj kot 60 % kislinsko topnega Al v oborjeni obliki, pri čemer navedena oborina sploh ne vsebuje A1N oborin v velikostnem območju med 5 nm in 150 nm, nato čiščenje njegove površine, nato izvedbo prve stopnje hladnega valjanja toplega traku z razmerjem hladnega valjanja vsaj 60 %, ne da bi predhodno žarili navedeni topli trak, nato izvedbo stopnje primarnega rekristalizacijskega žaljenja pri temperaturi Ti med 780 °C in 920 °C, pri čemer se jeklo vzdržuje pri Ti za minimalen čas ti 2 minut v atmosferi, ki je sestavljena iz zmesi vodika, dušika in vodne pare, nato ohlajanje na sobno temperaturo, tako da po ohlajanju dobimo vsebnost ogljika v jeklu pod 0,004 % in primarno povprečno velikost zrn pod 16 pm, nato izvedbo druge stopnje hladnega valjanja z razmeijem hladnega valjanja vsaj 50 %, da dobimo končno debelino hladno valjane jeklene pločevine, nato depozicijo plasti izolacijskega separatorja na površini navedene hladno valjane jeklene pločevine, nato izvedbo sekundarnega žarjenja izolirane hladno valjane jeklene pločevine v atmosferi, ki vsebuje vodik in dušik, pri čemer je segrevalna hitrost VI pod 15 °C na uro med 600 °C in 1150 °C, pri čemer se temperatura pločevine vzdržuje na minimalni temperaturi T21150 °C za minimalni čas t2 600 minut, pri čemer je celokupni čas žaljenja nad 120 ur, tako da se zniža vsebnost vsakega od žvepla in dušika pod 0,001 % in da ima sekundarno povprečno velikost zrn pod 15 mm, nato izvedbo počasnega ohlajanja do sobne temperature.
  2. 2. Postopek proizvodnje hladno valjane Fe-Si jeklene pločevine po zahtevku 1, kjer je vsebnost žvepla nižja od 0,010 %.
  3. 3. Postopek proizvodnje hladno valjane Fe-Si jeklene pločevine po zahtevku 1 ali 2, kjer je vsebnost ogljika med 0,025 % in 0,032 %.
  4. 4. Postopek proizvodnje hladno valjane Fe-Si jeklene pločevine po katerem koli od zahtevkov 1 do 3, kjer se brama uliva z minimalno hitrostjo 4,0 metrov na minuto.
  5. 5. Postopek proizvodnje hladno valjane Fe-Si jeklene pločevine po katerem koli od zahtevkov 1 do 4, kjer je temperatura dovršilnega valjanja vsaj 980 °C.
  6. 6. Postopek proizvodnje po katerem koli od zahtevkov 1 do 5, kjer je jeklena pločevina z orientiranimi zrni prevlečena z izolacijsko in natezno oblogo na osnovi emulzije koloidnega silicijevega dioksida.
  7. 7. Postopek proizvodnje po katerem koli od zahtevkov 1 do 6, kjer je po primarnem rekristalizacijskem žaljenju vsebnost ogljika v jeklu pod 0,0025 %.
  8. 8. Postopek proizvodnje po katerem koli od zahtevkov 1 do 7, kjer je po primarnem žarjenju primarna povprečna velikost zrn pod 10 pm.
  9. 9. Postopek proizvodnje po katerem koli od zahtevkov 1 do 8, kjer je po sekundarnem žarjenju sekundama povprečna velikost zrn pod 10 mm.
  10. 10. Jeklena pločevina z orientiranimi zrni, dobljena s postopkom po katerem koli od zahtevkov 1 do 9, ki daje indukcijsko vrednosti pri 800A/m nad 1,870 Tesla in izgubo jedrne moči nižjo od 1,3 W/kg pri specifični magnetni indukciji 1,7 Tesla (T).
  11. 11. Močnostni transformator, ki vključuje del, izdelan iz jeklene pločevine z orientiranimi zrni po zahtevku 10.
SI201330978T 2012-07-31 2013-07-30 Postopek proizvodnje silicijeve jeklene pločevine z orientiranimi zrni, električna jeklena pločevina z orientiranimi zrni in njena uporaba SI2880190T1 (sl)

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Application Number Priority Date Filing Date Title
PCT/IB2012/001475 WO2014020369A1 (en) 2012-07-31 2012-07-31 Method of production of grain-oriented silicon steel sheet grain oriented electrical steel sheet and use thereof
PCT/IB2013/001657 WO2014020406A1 (en) 2012-07-31 2013-07-30 Method of production of grain-oriented silicon steel sheet grain oriented electrical steel sheet and use thereof
EP13773324.2A EP2880190B1 (en) 2012-07-31 2013-07-30 Method of production of grain-oriented silicon steel sheet grain oriented electrical steel sheet and use thereof

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US (1) US9831020B2 (sl)
EP (1) EP2880190B1 (sl)
JP (3) JP6294319B2 (sl)
KR (1) KR101575633B1 (sl)
CN (1) CN104884642B (sl)
BR (1) BR112015002254B1 (sl)
CA (1) CA2880724C (sl)
DK (1) DK2880190T3 (sl)
EA (1) EA028436B1 (sl)
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HR (1) HRP20180388T1 (sl)
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IN (1) IN2015DN00804A (sl)
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NO (1) NO2880190T3 (sl)
PL (1) PL2880190T3 (sl)
PT (1) PT2880190T (sl)
RS (1) RS57048B1 (sl)
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