SG11201907559WA - Implementation of feedback control for improved electrochemical system design - Google Patents

Implementation of feedback control for improved electrochemical system design

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Publication number
SG11201907559WA
SG11201907559WA SG11201907559WA SG11201907559WA SG11201907559WA SG 11201907559W A SG11201907559W A SG 11201907559WA SG 11201907559W A SG11201907559W A SG 11201907559WA SG 11201907559W A SG11201907559W A SG 11201907559WA SG 11201907559W A SG11201907559W A SG 11201907559WA
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Singapore
Prior art keywords
international
electrochemical cell
march
anode
cathode
Prior art date
Application number
SG11201907559WA
Inventor
Simon Paul Dukes
George Y Gu
Joshua Griffis
Michael J Shaw
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Evoqua Water Tech Llc
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Application filed by Evoqua Water Tech Llc filed Critical Evoqua Water Tech Llc
Publication of SG11201907559WA publication Critical patent/SG11201907559WA/en

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    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/17Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • C25B9/19Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms
    • C25B9/23Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms comprising ion-exchange membranes in or on which electrode material is embedded
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    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
    • C02F1/467Treatment of water, waste water, or sewage by electrochemical methods by electrolysis by electrochemical disinfection; by electrooxydation or by electroreduction
    • C02F1/4672Treatment of water, waste water, or sewage by electrochemical methods by electrolysis by electrochemical disinfection; by electrooxydation or by electroreduction by electrooxydation
    • C02F1/4674Treatment of water, waste water, or sewage by electrochemical methods by electrolysis by electrochemical disinfection; by electrooxydation or by electroreduction by electrooxydation with halogen or compound of halogens, e.g. chlorine, bromine
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    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
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    • C25B1/00Electrolytic production of inorganic compounds or non-metals
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    • C25B1/26Chlorine; Compounds thereof
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    • C25B15/00Operating or servicing cells
    • C25B15/02Process control or regulation
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00Fuel cells; Manufacture thereof
    • H01M8/06Combination of fuel cells with means for production of reactants or for treatment of residues
    • H01M8/0606Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants
    • H01M8/0656Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants by electrochemical means
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    • C02F2201/46Apparatus for electrochemical processes
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    • C02F2201/46105Details relating to the electrolytic devices
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    • C02F2201/4613Inversing polarity
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    • C02F2201/46175Electrical pulses
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    • C02F2209/04Oxidation reduction potential [ORP]
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    • C02F2209/30H2
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    • C02F2209/40Liquid flow rate
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    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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    • C02F2303/04Disinfection
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    • C25B1/00Electrolytic production of inorganic compounds or non-metals
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    • C25B9/17Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/36Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
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  • Chemical & Material Sciences (AREA)
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  • Metallurgy (AREA)
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  • Inorganic Chemistry (AREA)
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  • Sustainable Energy (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Analytical Chemistry (AREA)
  • Secondary Cells (AREA)

Abstract

Flowof product solution to storage or point of use 7 -800 805 1000 J -1015J -820 910 815 810--, 1010 900 1000 1100 905 Flow of aqueous solution from source FIG. 5 825 (12) INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (19) World Intellectual Property Organization International Bureau (43) International Publication Date 13 September 2018 (13.09.2018) WIP0 I PCT IiiimmoimiolollmonolomommuomolommovoimIE (10) International Publication Number WO 2018/165127 Al (51) International Patent Classification: H01M 12/00 (2006.01) HO1M 12/02 (2006.01) (21) International Application Number: PCT/US2018/021103 (22) International Filing Date: 06 March 2018 (06.03.2018) (25) Filing Language: English (26) Publication Language: English (30) Priority Data: 62/467,518 06 March 2017 (06.03.2017) US 62/468,544 08 March 2017 (08.03.2017) US 62/469,224 09 March 2017 (09.03.2017) US (71) Applicant: EVOQUA WATER TECHNOLOGIES LLC [US/US]; 210 Sixth Avenue, Suite 3300, Pittsburgh, Penn- sylvania 01851 (US). (72) Inventors: DUKES, Simon Paul; 10 Wiggin Street, Chelmsford, Massachusetts 01824 (US). GU, George Y.; 4 Mulberry Circle, Andover, Massachusetts 01810 (US). GRIFFIS, Joshua; 20 Whitney Drive, Ashburnham, Mass- achusetts 01430 (US). SHAW, Michael J.; 6 Pingree Hill Road, Deny, New Hampshire 03038 (US). (74) Agent: WILKINS, Frederick C.; 10 Technology Drive, Lowell, Massachusetts 01851 (US). (81) Designated States (unless otherwise indicated, for every kind of national protection available): AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW. (84) Designated States (unless otherwise indicated, for every kind of regional protection available): ARIPO (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW), Eurasian (AM, AZ, BY, KG, KZ, RU, TJ, TM), European (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, (54) Title: IMPLEMENTATION OF FEEDBACK CONTROL FOR IMPROVED ELECTROCHEMICAL SYSTEM DESIGN (57) : A method of operating an electrochemical cell including introducing an aqueous solution into the electrochemical cell, applying a current across an anode and a cathode to produce a product, monitoring the voltage, dissolved hydrogen, or a condition of the aqueous solution, and reversing polarity of the anode and the cathode responsive to one of the measured parameters is disclosed. An electrochemical system including an electrochemical cell including an anode and a cathode, a source of an aqueous solution having an outlet fluidly connectable to the electrochemical cell, a sensor for measuring a parameter, and a controller configured to cause the anode and the cathode to reverse polarity responsive to the parameter measurement is disclosed. Methods of suppressing accumulation of hydrogen gas within the electrochemical cell are also disclosed. Methods of facilitating operation of an electrochemical cell are also disclosed. [Continued on next page] WO 2018/165127 Al MIDEDIMOMMIDIREIDIDEMIMII11111111011111111111111111111111 MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR), OAPI (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG). Published: — with international search report (Art. 21(3))
SG11201907559WA 2017-03-06 2018-03-06 Implementation of feedback control for improved electrochemical system design SG11201907559WA (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201762467518P 2017-03-06 2017-03-06
US201762468544P 2017-03-08 2017-03-08
US201762469224P 2017-03-09 2017-03-09
PCT/US2018/021103 WO2018165127A1 (en) 2017-03-06 2018-03-06 Implementation of feedback control for improved electrochemical system design

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SG11201907475YA SG11201907475YA (en) 2017-03-06 2018-03-06 Pulsed power supply for sustainable redox agent supply for hydrogen abatement during electrochemical hypochlorite generation
SG11201907559WA SG11201907559WA (en) 2017-03-06 2018-03-06 Implementation of feedback control for improved electrochemical system design
SG10202109750R SG10202109750RA (en) 2017-03-06 2018-03-06 Pulsed power supply for sustainable redox agent supply for hydrogen abatement during electrochemical hypochlorite generation
SG11201907477VA SG11201907477VA (en) 2017-03-06 2018-03-06 Half-cell electrochemical configurations for self-cleaning electrochlorination devices
SG10202109751U SG10202109751UA (en) 2017-03-06 2018-03-06 Half-cell electrochemical configurations for self-cleaning electrochlorination devices
SG10202109754T SG10202109754TA (en) 2017-03-06 2018-03-06 Implementation of feedback control for improved electrochemical system design

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SG10202109750R SG10202109750RA (en) 2017-03-06 2018-03-06 Pulsed power supply for sustainable redox agent supply for hydrogen abatement during electrochemical hypochlorite generation
SG11201907477VA SG11201907477VA (en) 2017-03-06 2018-03-06 Half-cell electrochemical configurations for self-cleaning electrochlorination devices
SG10202109751U SG10202109751UA (en) 2017-03-06 2018-03-06 Half-cell electrochemical configurations for self-cleaning electrochlorination devices
SG10202109754T SG10202109754TA (en) 2017-03-06 2018-03-06 Implementation of feedback control for improved electrochemical system design

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US (5) US11802063B2 (en)
EP (3) EP3592882A4 (en)
JP (3) JP7137574B2 (en)
KR (3) KR102578933B1 (en)
CN (3) CN110366608B (en)
AU (3) AU2018231010B2 (en)
CA (3) CA3053501A1 (en)
SG (6) SG11201907475YA (en)
WO (3) WO2018165127A1 (en)

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IT201800006544A1 (en) * 2018-06-21 2019-12-21 ANODE FOR ELECTROLYTIC EVOLUTION OF CHLORINE
WO2020075202A1 (en) * 2018-10-09 2020-04-16 Atmonia Ehf. Electrochemical reactions with cyclic varied potential
DE102018009448A1 (en) * 2018-12-04 2020-06-04 Heinz Günther Römer Immersion electrolytic cell
US11491443B2 (en) * 2019-04-04 2022-11-08 Hamilton Sundstrand Corporation Process water gas management of electrochemical inert gas generating system
CA3138381A1 (en) 2019-04-29 2020-11-05 Spa Logic, Inc. Water sanitation system and method
EP3976859A4 (en) * 2019-06-03 2023-10-18 Garwood Medical Devices, LLC Autonomous hydrogen evolution reaction threshold detection method and device
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