SG11201503019SA - Post-treatment of deboronated mww zeolite - Google Patents

Post-treatment of deboronated mww zeolite

Info

Publication number
SG11201503019SA
SG11201503019SA SG11201503019SA SG11201503019SA SG11201503019SA SG 11201503019S A SG11201503019S A SG 11201503019SA SG 11201503019S A SG11201503019S A SG 11201503019SA SG 11201503019S A SG11201503019S A SG 11201503019SA SG 11201503019S A SG11201503019S A SG 11201503019SA
Authority
SG
Singapore
Prior art keywords
post
treatment
mww zeolite
deboronated
deboronated mww
Prior art date
Application number
SG11201503019SA
Other languages
English (en)
Inventor
Jeff Yang
Stefan Maurer
Manuela Gaab
Karsten Seidel
Olga Gerlach
Ulrich Müller
Andrei-Nicolae Parvulescu
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of SG11201503019SA publication Critical patent/SG11201503019SA/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/05—Nuclear magnetic resonance [NMR]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/10—Infrared [IR]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/007—Borosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/16—After treatment, characterised by the effect to be obtained to increase the Si/Al ratio; Dealumination
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/37—Acid treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/40—Special temperature treatment, i.e. other than just for template removal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
SG11201503019SA 2012-10-18 2013-10-09 Post-treatment of deboronated mww zeolite SG11201503019SA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12189042 2012-10-18
PCT/EP2013/071042 WO2014060261A1 (en) 2012-10-18 2013-10-09 Post-treatment of deboronated mww zeolite

Publications (1)

Publication Number Publication Date
SG11201503019SA true SG11201503019SA (en) 2015-05-28

Family

ID=47046432

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201503019SA SG11201503019SA (en) 2012-10-18 2013-10-09 Post-treatment of deboronated mww zeolite

Country Status (13)

Country Link
US (1) US10099933B2 (enrdf_load_stackoverflow)
EP (1) EP2909141B1 (enrdf_load_stackoverflow)
JP (1) JP6267211B2 (enrdf_load_stackoverflow)
KR (1) KR102184609B1 (enrdf_load_stackoverflow)
CN (1) CN104854028B (enrdf_load_stackoverflow)
BR (1) BR112015008390B1 (enrdf_load_stackoverflow)
ES (1) ES2620030T3 (enrdf_load_stackoverflow)
MX (1) MX355246B (enrdf_load_stackoverflow)
MY (1) MY169039A (enrdf_load_stackoverflow)
RU (1) RU2638851C2 (enrdf_load_stackoverflow)
SG (1) SG11201503019SA (enrdf_load_stackoverflow)
WO (1) WO2014060261A1 (enrdf_load_stackoverflow)
ZA (1) ZA201503155B (enrdf_load_stackoverflow)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG11201503017XA (en) 2012-10-18 2015-05-28 Basf Se Post-treatment of a zeolitic material
US10196276B2 (en) * 2014-06-06 2019-02-05 Basf Se Synthesis of a boron-containing zeolite with an MWW framework structure
RU2698832C2 (ru) * 2014-09-09 2019-08-30 Басф Се Способ получения цеолитного материала mww, содержащего бор и титан
JP6656242B2 (ja) 2014-10-15 2020-03-04 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ゼオライト材料の固体熱合成方法及びそれから得られるゼオライト
US11155467B2 (en) * 2016-09-06 2021-10-26 Basf Se Solidothermal synthesis of a boron-containing zeolite with an MWW framework structure
MY199941A (en) 2016-12-20 2023-11-30 Basf Se Process for preparing an extrudable composition comprising a titanium-containing zeolitic material, having framework type mww
JP7296880B2 (ja) * 2016-12-20 2023-06-23 ビーエーエスエフ ソシエタス・ヨーロピア 骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む組成物の可塑性を低下させるための酸処理の使用方法
BR112019017044B1 (pt) 2017-02-28 2023-03-28 Basf Se Processo para preparar um composto, e, uso de um material zeolítico
US11224867B2 (en) * 2017-05-15 2022-01-18 Basf Corporation Process for preparing a zeolitic material having framework type AEI

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2445747A1 (fr) 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
US4622166A (en) * 1982-03-17 1986-11-11 Mizusawa Kagaku Kogyo Kabushiki Kaisha Process for preparation of zeolite slurry excellent in static stability and dynamic stability
DE4207745A1 (de) * 1992-03-11 1993-09-16 Basf Ag Azofarbstoffe enthaltende molekularsiebe
US7011802B2 (en) 2000-12-22 2006-03-14 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
JP4241068B2 (ja) * 2002-03-07 2009-03-18 昭和電工株式会社 Ｍｗｗ型ゼオライト物質の製造方法
US20090325790A1 (en) * 2004-06-17 2009-12-31 Yale University Size-controllable transition metal clusters in mcm-41 for improving chemical catalysis
CN100363259C (zh) * 2004-12-23 2008-01-23 中国科学院大连化学物理研究所 一种高硅mcm-22分子筛的制备方法
WO2008016456A2 (en) * 2006-07-28 2008-02-07 Exxonmobil Chemical Patents Inc. Molecular sieve composition (emm-10), its method of making, and use for hydrocarbon conversions
EP2025402A1 (en) * 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
US7737313B2 (en) * 2006-12-21 2010-06-15 Exxonmobil Chemical Patents Inc. Catalyst composition, the method of manufacturing, and the process of using thereof in hydrocarbon conversions
JP2010235605A (ja) * 2009-03-13 2010-10-21 Sumitomo Chemical Co Ltd オレフィンオキサイドの製造方法
WO2012074033A1 (ja) * 2010-11-30 2012-06-07 住友化学株式会社 チタン含有珪素酸化物成形体の製造方法及びオキシラン化合物の製造方法
US9522390B2 (en) * 2010-12-10 2016-12-20 The Regents Of The University Of California Oxide materials and synthesis by fluoride/chloride anion promoted exfoliation

Also Published As

Publication number Publication date
CN104854028A (zh) 2015-08-19
JP2015532259A (ja) 2015-11-09
BR112015008390B1 (pt) 2021-11-03
ZA201503155B (en) 2017-11-29
BR112015008390A2 (pt) 2017-08-08
RU2638851C2 (ru) 2017-12-18
MX2015004948A (es) 2016-01-20
WO2014060261A1 (en) 2014-04-24
KR20150074076A (ko) 2015-07-01
CN104854028B (zh) 2017-07-18
RU2015118225A (ru) 2016-12-10
EP2909141B1 (en) 2016-12-14
ES2620030T3 (es) 2017-06-27
EP2909141A1 (en) 2015-08-26
US20150329368A1 (en) 2015-11-19
MY169039A (en) 2019-02-07
US10099933B2 (en) 2018-10-16
MX355246B (es) 2018-04-11
KR102184609B1 (ko) 2020-12-01
JP6267211B2 (ja) 2018-01-24

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