SG11201405045YA - Production of caprolactam from adipic acid - Google Patents

Production of caprolactam from adipic acid

Info

Publication number
SG11201405045YA
SG11201405045YA SG11201405045YA SG11201405045YA SG11201405045YA SG 11201405045Y A SG11201405045Y A SG 11201405045YA SG 11201405045Y A SG11201405045Y A SG 11201405045YA SG 11201405045Y A SG11201405045Y A SG 11201405045YA SG 11201405045Y A SG11201405045Y A SG 11201405045YA
Authority
SG
Singapore
Prior art keywords
caprolactam
production
adipic acid
adipic
acid
Prior art date
Application number
SG11201405045YA
Other languages
English (en)
Inventor
Eric L Dias
Vincent J Murphy
James Longmire
Hong Jiang
Original Assignee
Rennovia Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rennovia Inc filed Critical Rennovia Inc
Publication of SG11201405045YA publication Critical patent/SG11201405045YA/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B01J37/18—Reducing with gases containing free hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D223/08—Oxygen atoms
    • C07D223/10—Oxygen atoms attached in position 2
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/64—Platinum group metals with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/652—Chromium, molybdenum or tungsten
    • B01J23/6525—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/64—Platinum group metals with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/656—Manganese, technetium or rhenium
    • B01J23/6567—Rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/8906—Iron and noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/8913—Cobalt and noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/892—Nickel and noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/8926—Copper and noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
SG11201405045YA 2012-02-23 2013-02-13 Production of caprolactam from adipic acid SG11201405045YA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201261602533P 2012-02-23 2012-02-23
PCT/US2013/025846 WO2013126250A1 (en) 2012-02-23 2013-02-13 Production of caprolactam from adipic acid

Publications (1)

Publication Number Publication Date
SG11201405045YA true SG11201405045YA (en) 2014-09-26

Family

ID=47748790

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201405045YA SG11201405045YA (en) 2012-02-23 2013-02-13 Production of caprolactam from adipic acid

Country Status (12)

Country Link
US (1) US8946411B2 (enrdf_load_stackoverflow)
EP (1) EP2817293A1 (enrdf_load_stackoverflow)
JP (1) JP2015517977A (enrdf_load_stackoverflow)
KR (1) KR20140129076A (enrdf_load_stackoverflow)
CN (1) CN104169259B (enrdf_load_stackoverflow)
AR (1) AR089980A1 (enrdf_load_stackoverflow)
BR (1) BR112014020642B1 (enrdf_load_stackoverflow)
HK (1) HK1205121A1 (enrdf_load_stackoverflow)
IN (1) IN2014DN07028A (enrdf_load_stackoverflow)
SA (1) SA113340296B1 (enrdf_load_stackoverflow)
SG (1) SG11201405045YA (enrdf_load_stackoverflow)
WO (1) WO2013126250A1 (enrdf_load_stackoverflow)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013090031A2 (en) 2011-12-14 2013-06-20 Rennovia, Inc. Water concentration reduction process
EP2790806A1 (en) 2011-12-14 2014-10-22 Rennovia, Inc. Process for the separation of mono-and di-carboxylic acid compounds
CN104557705B (zh) * 2013-10-15 2017-06-09 中国石油化工股份有限公司 一种己内酰胺精制的方法和装置
BR112017005823B1 (pt) 2014-09-29 2023-03-28 Archer-Daniels-Midland Company Processo para a preparação de um extrato
JP6672792B2 (ja) * 2014-10-30 2020-03-25 東レ株式会社 ε−カプロラクタムの製造方法
TW201718088A (zh) * 2015-09-11 2017-06-01 東麗股份有限公司 ε－己內醯胺之製造方法
JP7125674B2 (ja) * 2016-12-06 2022-08-25 東レ株式会社 ε－カプロラクタムの製造方法
KR102739203B1 (ko) * 2018-08-28 2024-12-05 현대자동차주식회사 바이오 나일론 원료의 중간체 물질인 아디프아마이드 제조방법
CN114160120B (zh) * 2021-12-24 2024-01-26 郑州中科新兴产业技术研究院 一种用于己二酸酯生产己二腈的催化剂的制备方法

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GB778253A (en) * 1955-02-02 1957-07-03 Inventa Ag Process for the manufacture of -e-caprolactam
US3652549A (en) * 1968-07-18 1972-03-28 Kanegafuchi Spinning Co Ltd Production of epsilon-caprolactam
JPS4919250B1 (enrdf_load_stackoverflow) * 1969-01-09 1974-05-16
JPS4919250A (enrdf_load_stackoverflow) * 1972-06-16 1974-02-20
US4042490A (en) 1973-12-26 1977-08-16 Texaco Inc. Hydrocarbon upgrading process
US4800227A (en) 1984-08-20 1989-01-24 Phillips Petroleum Company Process for the production of lactams
IT1214622B (it) 1985-07-10 1990-01-18 Montedipe Spa Processo catalitico per laproduzione di cicloesanonossima.
US5717089A (en) * 1995-03-01 1998-02-10 Dsm N.V. Process for the preparation of E-caprolactam
DE19548289A1 (de) * 1995-12-22 1997-06-26 Basf Ag Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
US5780623A (en) * 1996-02-23 1998-07-14 Dsm N.V. Process to prepare ε-caprolactam from 6-aminocaproic acid
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EP0984002A1 (en) 1998-09-03 2000-03-08 Dsm N.V. Process to continuously prepare an aqueous mixture of epsilon-caprolactam and epsilon-caprolactam precursors
DE19842900A1 (de) * 1998-09-18 2000-03-23 Basf Ag Verfahren zur gemeinsamen Herstellung eines cyclischen Lactams und eines cyclischen Amins
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US8283466B2 (en) 2007-02-20 2012-10-09 Board Of Trustees Of Michigan State University Catalytic deamination for caprolactam production
CN102803196B (zh) * 2009-06-13 2016-06-22 莱诺维亚公司 由含碳水化合物的物质生产己二酸和衍生物
US8669397B2 (en) 2009-06-13 2014-03-11 Rennovia, Inc. Production of adipic acid and derivatives from carbohydrate-containing materials
CN102869642A (zh) * 2010-03-05 2013-01-09 莱诺维亚公司 己二酸组合物
WO2013090031A2 (en) 2011-12-14 2013-06-20 Rennovia, Inc. Water concentration reduction process
EP2790806A1 (en) 2011-12-14 2014-10-22 Rennovia, Inc. Process for the separation of mono-and di-carboxylic acid compounds
SG11201407554UA (en) 2012-05-15 2014-12-30 Rennovia Inc Reduction catalysts
JP6209603B2 (ja) 2012-06-11 2017-10-04 レノヴィア, インコーポレイテッドRennovia, INC. １，６‐ヘキサンジオール由来のアジピン酸製造方法

Also Published As

Publication number Publication date
EP2817293A1 (en) 2014-12-31
JP2015517977A (ja) 2015-06-25
US20130225785A1 (en) 2013-08-29
BR112014020642B1 (pt) 2020-12-29
CN104169259B (zh) 2016-09-21
KR20140129076A (ko) 2014-11-06
IN2014DN07028A (enrdf_load_stackoverflow) 2015-04-10
CN104169259A (zh) 2014-11-26
US8946411B2 (en) 2015-02-03
WO2013126250A1 (en) 2013-08-29
BR112014020642A2 (pt) 2019-09-10
SA113340296B1 (ar) 2015-09-06
AR089980A1 (es) 2014-10-01
HK1205121A1 (en) 2015-12-11

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