SG102067A1 - Method and apparatus for the production of nitrogen trifluoride - Google Patents

Method and apparatus for the production of nitrogen trifluoride

Info

Publication number
SG102067A1
SG102067A1 SG200300103A SG200300103A SG102067A1 SG 102067 A1 SG102067 A1 SG 102067A1 SG 200300103 A SG200300103 A SG 200300103A SG 200300103 A SG200300103 A SG 200300103A SG 102067 A1 SG102067 A1 SG 102067A1
Authority
SG
Singapore
Prior art keywords
production
nitrogen trifluoride
trifluoride
nitrogen
Prior art date
Application number
SG200300103A
Other languages
English (en)
Inventor
Prentice Satchell Donald Jr
R Mohan Vasu
Original Assignee
Boc Group Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Boc Group Inc filed Critical Boc Group Inc
Publication of SG102067A1 publication Critical patent/SG102067A1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/083—Compounds containing nitrogen and non-metals and optionally metals containing one or more halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/16—Halides of ammonium
    • C01C1/162—Ammonium fluoride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/435—Mixing tubes composed of concentric tubular members
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/244—Concentric tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/246—Stationary reactors without moving elements inside provoking a loop type movement of the reactants internally, i.e. the mixture circulating inside the vessel such that the upward stream is separated physically from the downward stream(s)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/083—Compounds containing nitrogen and non-metals and optionally metals containing one or more halogen atoms
    • C01B21/0832—Binary compounds of nitrogen with halogens
    • C01B21/0835—Nitrogen trifluoride
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C01B7/191—Hydrogen fluoride
    • C01B7/194—Preparation from ammonium fluoride
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/16—Halides of ammonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2215/00—Auxiliary or complementary information in relation with mixing
    • B01F2215/04—Technical information in relation with mixing
    • B01F2215/0413—Numerical information
    • B01F2215/0436—Operational information
    • B01F2215/0468—Numerical pressure values
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2215/00—Auxiliary or complementary information in relation with mixing
    • B01F2215/04—Technical information in relation with mixing
    • B01F2215/0413—Numerical information
    • B01F2215/0436—Operational information
    • B01F2215/0472—Numerical temperature values
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20—Mixing gases with liquids
    • B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20—Jet mixers, i.e. mixers using high-speed fluid streams
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2219/00108—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
SG200300103A 2002-02-08 2003-01-17 Method and apparatus for the production of nitrogen trifluoride SG102067A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10/071,114 US6908601B2 (en) 2002-02-08 2002-02-08 Method for the production of nitrogen trifluoride

Publications (1)

Publication Number Publication Date
SG102067A1 true SG102067A1 (en) 2004-02-27

Family

ID=27659163

Family Applications (1)

Application Number Title Priority Date Filing Date
SG200300103A SG102067A1 (en) 2002-02-08 2003-01-17 Method and apparatus for the production of nitrogen trifluoride

Country Status (7)

Country Link
US (2) US6908601B2 (enExample)
EP (1) EP1338559A3 (enExample)
JP (1) JP2003238122A (enExample)
KR (1) KR20030067587A (enExample)
CN (1) CN1261349C (enExample)
SG (1) SG102067A1 (enExample)
TW (1) TW200303287A (enExample)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100452233B1 (ko) * 2002-07-19 2004-10-12 한국과학기술연구원 젯트루프식 분사형 반응기를 이용한 삼불화질소 제조방법
US20040096386A1 (en) * 2002-11-19 2004-05-20 Syvret Robert George Method for nitrogen trifluoride production
US7128885B2 (en) * 2002-12-23 2006-10-31 The Boc Group, Inc. NF3 production reactor
US7582793B2 (en) * 2004-09-02 2009-09-01 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) * 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7589231B2 (en) * 2004-09-02 2009-09-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7507857B2 (en) 2004-09-02 2009-03-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7381836B2 (en) 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7572936B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) * 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7692037B2 (en) * 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7045107B2 (en) * 2004-09-20 2006-05-16 Air Products And Chemicals, Inc. Process for the production of nitrogen trifluoride
US7884232B2 (en) 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7413722B2 (en) * 2005-08-04 2008-08-19 Foosung Co., Ltd. Method and apparatus for manufacturing nitrogen trifluoride
JP4624905B2 (ja) * 2005-10-27 2011-02-02 昭和電工株式会社 三フッ化窒素の製造方法
JP4624920B2 (ja) * 2005-12-28 2011-02-02 昭和電工株式会社 三フッ化窒素の製造方法
US20100239485A1 (en) * 2007-12-27 2010-09-23 Central Glass Co., Ltd. Method of manufacturing fluorinated gas compounds and apparatus for manufacturing the same
DE102008021628A1 (de) * 2008-04-25 2009-12-24 Ibh Engineering Gmbh Vorrichtung und Verfahren sowie Verwendung eines Reaktors zur Herstellung von Roh,- Brenn- und Kraftstoffen aus organischen Substanzen
US8163262B1 (en) 2011-01-04 2012-04-24 Omotowa Bamidele A Method for production of nitrogen trifluoride from trimethylsilylamines
JP2017512133A (ja) * 2014-02-10 2017-05-18 ハネウェル・インターナショナル・インコーポレーテッド 液相フッ素化のための反応器デザイン
CN104043363A (zh) * 2014-06-26 2014-09-17 苏州创维晟自动化科技有限公司 一种用于制造汽车内饰的自动化物料搅拌桶
CN106397761B (zh) * 2016-09-06 2021-06-18 天津长芦新材料研究院有限公司 氟化全氟聚醚酸端基的方法
CN106311097B (zh) * 2016-09-06 2018-12-14 天津长芦新材料研究院有限公司 气液接触反应装置在氟化全氟聚醚酸方面的应用
CN112742232B (zh) * 2019-10-29 2023-04-18 中国石油化工股份有限公司 一种喷氨静态混合器

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4091081A (en) * 1977-04-19 1978-05-23 Air Products And Chemicals, Inc. Preparation of nitrogen trifluoride
US5637285A (en) * 1996-01-30 1997-06-10 Air Products And Chemicals, Inc. Process for nitrogen trifluoride synthesis

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4001380A (en) 1961-05-16 1977-01-04 Allied Chemical Corporation Manufacture of nitrogen trifluoride
JPS6071503A (ja) 1983-09-27 1985-04-23 Central Glass Co Ltd Νｆ↓３の製造法
DE3722163A1 (de) 1987-07-04 1989-01-12 Kali Chemie Ag Verfahren zur herstellung von nf(pfeil abwaerts)3(pfeil abwaerts)
EP0366078B1 (en) 1988-10-25 1996-06-26 MITSUI TOATSU CHEMICALS, Inc. Method for Purifying nitrogen trifluoride gas
EP0424727B1 (en) 1989-10-26 1995-04-19 MITSUI TOATSU CHEMICALS, Inc. Method for producing nitrogen trifluoride
JPH05105411A (ja) * 1991-10-22 1993-04-27 Onoda Cement Co Ltd 三フツ化窒素の製造方法
US5804447A (en) * 1992-07-23 1998-09-08 Basf Aktiengesellschaft Use of compounds which absorb and/or fluoresce in the IR region as markers for liquids
US5628894A (en) 1995-10-17 1997-05-13 Florida Scientific Laboratories, Inc. Nitrogen trifluoride process
US6010605A (en) 1995-10-17 2000-01-04 Florida Scientific Laboratories Inc. Nitrogen trifluoride production apparatus
US5933158A (en) * 1997-09-09 1999-08-03 Compaq Computer Corporation Use of a link bit to fetch entries of a graphic address remapping table
DE19836807A1 (de) 1998-08-14 2000-02-17 Basf Ag Verfahren zur Herstellung von Aldehyden und/oder Alkoholen oder Aminen
WO2001085603A2 (en) * 2000-05-12 2001-11-15 Showa Denko K. K. Process for producing nitrogen trifluoride and use thereof
US6986874B2 (en) * 2000-12-14 2006-01-17 The Boc Group, Inc. Method and apparatus for the production of nitrogen trifluoride

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4091081A (en) * 1977-04-19 1978-05-23 Air Products And Chemicals, Inc. Preparation of nitrogen trifluoride
US5637285A (en) * 1996-01-30 1997-06-10 Air Products And Chemicals, Inc. Process for nitrogen trifluoride synthesis

Also Published As

Publication number Publication date
CN1449992A (zh) 2003-10-22
EP1338559A3 (en) 2004-04-21
US20040191156A1 (en) 2004-09-30
CN1261349C (zh) 2006-06-28
EP1338559A2 (en) 2003-08-27
US6908601B2 (en) 2005-06-21
TW200303287A (en) 2003-09-01
JP2003238122A (ja) 2003-08-27
US20030152507A1 (en) 2003-08-14
KR20030067587A (ko) 2003-08-14

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