SE7712368L - PROCEDURE FOR THE PREPARATION OF 9- (B-D-ARABINOFURANOSYL) ADENIN-5'-PHOSPHATE - Google Patents
PROCEDURE FOR THE PREPARATION OF 9- (B-D-ARABINOFURANOSYL) ADENIN-5'-PHOSPHATEInfo
- Publication number
- SE7712368L SE7712368L SE7712368A SE7712368A SE7712368L SE 7712368 L SE7712368 L SE 7712368L SE 7712368 A SE7712368 A SE 7712368A SE 7712368 A SE7712368 A SE 7712368A SE 7712368 L SE7712368 L SE 7712368L
- Authority
- SE
- Sweden
- Prior art keywords
- arabinofuranosyl
- phosphate
- mixture
- adenin
- procedure
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H19/00—Compounds containing a hetero ring sharing one ring hetero atom with a saccharide radical; Nucleosides; Mononucleotides; Anhydro-derivatives thereof
- C07H19/02—Compounds containing a hetero ring sharing one ring hetero atom with a saccharide radical; Nucleosides; Mononucleotides; Anhydro-derivatives thereof sharing nitrogen
- C07H19/04—Heterocyclic radicals containing only nitrogen atoms as ring hetero atom
- C07H19/16—Purine radicals
- C07H19/20—Purine radicals with the saccharide radical esterified by phosphoric or polyphosphoric acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The 9-( beta -D-arabinofuranosyl)adenine 5'-phosphate is prepared from a mixture obtained by reaction of 9-( beta -D-arabinofuranosyl)adenine with a phosphorylating agent, in a trialkyl phosphate as solvent. The mixture is then subjected to an aqueous hydrolysis, the pH of the hydrolysis mixture is adjusted to a value sufficiently high to bring about separation into aqueous and nonaqueous liquid phases; the trialkyl phosphate, which is the solvent, is removed and then the product is precipitated so as to separate it from the residual aqueous mixture and it is isolated.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US73842576A | 1976-11-03 | 1976-11-03 | |
| US05/831,703 US4123609A (en) | 1976-11-03 | 1977-09-12 | Process for the production of 9-(β-D-arabinofuranosyl)adenine, 5'-phosphate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| SE7712368L true SE7712368L (en) | 1978-05-04 |
| SE442404B SE442404B (en) | 1985-12-23 |
Family
ID=27113366
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE7712368A SE442404B (en) | 1976-11-03 | 1977-11-02 | PROCEDURE FOR PREPARING 9- (BETA-D-ARABINOFURANOSYL) ADENIN-5'-PHOSPHATE |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS5356691A (en) |
| AT (1) | AT358187B (en) |
| CA (2) | CA1077030A (en) |
| CH (1) | CH626377A5 (en) |
| DE (1) | DE2749056A1 (en) |
| DK (1) | DK151263C (en) |
| ES (1) | ES463768A1 (en) |
| FR (1) | FR2370057A1 (en) |
| GB (1) | GB1559456A (en) |
| HK (1) | HK3884A (en) |
| NL (1) | NL191060C (en) |
| SE (1) | SE442404B (en) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1383572A (en) * | 1964-02-28 | 1964-12-24 | Necchi Spa | Improvements in automatic shut-off devices for sewing machines |
| DE1645896C3 (en) * | 1965-03-17 | 1975-01-02 | Ajinomoto Co., Inc., Tokio | Process for the preparation of 5'-ribonucleotides and S'-deoxyribonucleotides |
| BE756704A (en) * | 1969-09-26 | 1971-03-01 | Parke Davis & Co | PROCESS FOR THE PRODUCTION OF 5'-PHOSPHATE OF 9- (BETA-D- ARABINOFURANOSYL) ADENINE AND ITS SALTS |
-
1977
- 1977-11-02 FR FR7732871A patent/FR2370057A1/en active Granted
- 1977-11-02 CA CA290,047A patent/CA1077030A/en not_active Expired
- 1977-11-02 DE DE19772749056 patent/DE2749056A1/en active Granted
- 1977-11-02 DK DK487177A patent/DK151263C/en not_active IP Right Cessation
- 1977-11-02 NL NL7712102A patent/NL191060C/en not_active IP Right Cessation
- 1977-11-02 JP JP13216277A patent/JPS5356691A/en active Pending
- 1977-11-02 SE SE7712368A patent/SE442404B/en not_active IP Right Cessation
- 1977-11-02 GB GB4564777A patent/GB1559456A/en not_active Expired
- 1977-11-02 AT AT779577A patent/AT358187B/en not_active IP Right Cessation
- 1977-11-02 CH CH1335777A patent/CH626377A5/en not_active IP Right Cessation
- 1977-11-02 ES ES463768A patent/ES463768A1/en not_active Expired
-
1979
- 1979-12-18 CA CA342,182A patent/CA1088927A/en not_active Expired
-
1984
- 1984-01-12 HK HK3884A patent/HK3884A/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE2749056A1 (en) | 1978-05-18 |
| CA1088927A (en) | 1980-11-04 |
| DE2749056C2 (en) | 1987-07-16 |
| GB1559456A (en) | 1980-01-16 |
| NL191060C (en) | 1995-01-02 |
| CH626377A5 (en) | 1981-11-13 |
| AT358187B (en) | 1980-08-25 |
| ATA779577A (en) | 1980-01-15 |
| NL7712102A (en) | 1978-05-08 |
| DK151263C (en) | 1988-05-16 |
| HK3884A (en) | 1984-01-20 |
| FR2370057B1 (en) | 1980-06-13 |
| NL191060B (en) | 1994-08-01 |
| ES463768A1 (en) | 1978-06-01 |
| FR2370057A1 (en) | 1978-06-02 |
| DK151263B (en) | 1987-11-16 |
| JPS5356691A (en) | 1978-05-23 |
| SE442404B (en) | 1985-12-23 |
| DK487177A (en) | 1978-05-04 |
| CA1077030A (en) | 1980-05-06 |
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