SE511152C2 - Sätt att framställa en BCN-struktur som har en diamantstruktur - Google Patents
Sätt att framställa en BCN-struktur som har en diamantstrukturInfo
- Publication number
- SE511152C2 SE511152C2 SE9303605A SE9303605A SE511152C2 SE 511152 C2 SE511152 C2 SE 511152C2 SE 9303605 A SE9303605 A SE 9303605A SE 9303605 A SE9303605 A SE 9303605A SE 511152 C2 SE511152 C2 SE 511152C2
- Authority
- SE
- Sweden
- Prior art keywords
- substance
- powder
- shaped body
- give
- mixture
- Prior art date
Links
- 229910003460 diamond Inorganic materials 0.000 title claims abstract description 32
- 239000010432 diamond Substances 0.000 title claims abstract description 32
- 239000000126 substance Substances 0.000 claims abstract description 119
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 45
- 239000000843 powder Substances 0.000 claims abstract description 38
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 28
- 239000000203 mixture Substances 0.000 claims abstract description 28
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 27
- 229910052796 boron Inorganic materials 0.000 claims abstract description 27
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 26
- 238000004880 explosion Methods 0.000 claims abstract description 22
- 229910052751 metal Inorganic materials 0.000 claims abstract description 22
- 239000002184 metal Substances 0.000 claims abstract description 22
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 22
- 239000013078 crystal Substances 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims description 54
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 39
- 239000002245 particle Substances 0.000 claims description 26
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 24
- 239000010949 copper Substances 0.000 claims description 15
- 229910052802 copper Inorganic materials 0.000 claims description 15
- 239000007787 solid Substances 0.000 claims description 15
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 claims description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 13
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 12
- 239000001257 hydrogen Substances 0.000 claims description 12
- 229910052739 hydrogen Inorganic materials 0.000 claims description 12
- 239000002360 explosive Substances 0.000 claims description 9
- 239000007789 gas Substances 0.000 claims description 8
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims description 7
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 claims description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 239000010941 cobalt Substances 0.000 claims description 3
- 229910017052 cobalt Inorganic materials 0.000 claims description 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 150000002431 hydrogen Chemical class 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 2
- 229910052721 tungsten Inorganic materials 0.000 claims description 2
- 239000010937 tungsten Substances 0.000 claims description 2
- BAZAXWOYCMUHIX-UHFFFAOYSA-M sodium perchlorate Chemical compound [Na+].[O-]Cl(=O)(=O)=O BAZAXWOYCMUHIX-UHFFFAOYSA-M 0.000 claims 1
- 229910001488 sodium perchlorate Inorganic materials 0.000 claims 1
- 239000008247 solid mixture Substances 0.000 claims 1
- 239000000523 sample Substances 0.000 description 22
- 230000035939 shock Effects 0.000 description 19
- 238000002441 X-ray diffraction Methods 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 10
- 238000005481 NMR spectroscopy Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000007858 starting material Substances 0.000 description 6
- 239000002131 composite material Substances 0.000 description 5
- 238000000921 elemental analysis Methods 0.000 description 5
- 229910052582 BN Inorganic materials 0.000 description 4
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 238000003825 pressing Methods 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000002775 capsule Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000013074 reference sample Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 230000003068 static effect Effects 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 239000003082 abrasive agent Substances 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005474 detonation Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000005284 excitation Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000004445 quantitative analysis Methods 0.000 description 2
- 230000003595 spectral effect Effects 0.000 description 2
- 230000002194 synthesizing effect Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910001369 Brass Inorganic materials 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 244000309464 bull Species 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000002003 electron diffraction Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000002198 insoluble material Substances 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 150000001247 metal acetylides Chemical class 0.000 description 1
- 239000002923 metal particle Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 238000001208 nuclear magnetic resonance pulse sequence Methods 0.000 description 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Inorganic materials [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 description 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/583—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on boron nitride
- C04B35/5831—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on boron nitride based on cubic boron nitrides or Wurtzitic boron nitrides, including crystal structure transformation of powder
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
- B01J3/08—Application of shock waves for chemical reactions or for modifying the crystal structure of substances
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B29/00—Compositions containing an inorganic oxygen-halogen salt, e.g. chlorate, perchlorate
- C06B29/02—Compositions containing an inorganic oxygen-halogen salt, e.g. chlorate, perchlorate of an alkali metal
- C06B29/16—Compositions containing an inorganic oxygen-halogen salt, e.g. chlorate, perchlorate of an alkali metal with a nitrated organic compound
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/065—Composition of the material produced
- B01J2203/066—Boronitrides
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Ceramic Engineering (AREA)
- Structural Engineering (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Polishing Bodies And Polishing Tools (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP29707392 | 1992-11-06 | ||
| JP26885993A JP3346496B2 (ja) | 1992-11-06 | 1993-10-27 | 多結晶性ｂｃｎ物質及びその製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| SE9303605D0 SE9303605D0 (sv) | 1993-11-02 |
| SE9303605L SE9303605L (sv) | 1994-05-07 |
| SE511152C2 true SE511152C2 (sv) | 1999-08-16 |
Family
ID=26548504
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE9303605A SE511152C2 (sv) | 1992-11-06 | 1993-11-02 | Sätt att framställa en BCN-struktur som har en diamantstruktur |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US5866059A (de) |
| JP (1) | JP3346496B2 (de) |
| DE (1) | DE4337689A1 (de) |
| SE (1) | SE511152C2 (de) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003081615A (ja) * | 2001-09-05 | 2003-03-19 | Asahi Kasei Corp | 炭窒化硼素の製造方法 |
| US9296656B2 (en) | 2003-09-09 | 2016-03-29 | International Technology Center | UV protective coatings |
| US9260653B2 (en) * | 2005-08-30 | 2016-02-16 | International Technology Center | Enhancement of photoluminescence of nanodiamond particles |
| DE102005026804B3 (de) * | 2005-06-09 | 2007-02-22 | Membrana Gmbh | Mikrofiltrationsmembran mit verbessertem Filtrationsverhalten |
| US8449854B2 (en) * | 2007-01-29 | 2013-05-28 | William Marsh Rice University | Method for preparation of new superhard B-C-N material and material made therefrom |
| JP5393109B2 (ja) * | 2008-11-04 | 2014-01-22 | 旭化成ケミカルズ株式会社 | 窒素含有炭素材料及びその製造方法 |
| US8728429B2 (en) * | 2009-03-02 | 2014-05-20 | International Technology Center | Production of conductive nanodiamond by dynamic synthesis approaches |
| US10364389B1 (en) | 2013-09-12 | 2019-07-30 | Adámas Nanotechnologies, lnc. | Fluorescent diamond particles |
| CN108176852B (zh) * | 2017-12-27 | 2019-08-30 | 湘潭大学 | 一种可抽真空式爆炸压实金属粉末装置及其使用方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2941248A (en) * | 1958-01-06 | 1960-06-21 | Gen Electric | High temperature high pressure apparatus |
| US3367766A (en) * | 1965-06-16 | 1968-02-06 | Du Pont | Preparation of brittle inorganic polycrystalline powders by shock-wave techniques |
| US3876751A (en) * | 1972-12-18 | 1975-04-08 | Vladimir Petrovich Alexeevsky | Method for producing polycrystalline boron nitride |
| ZA77925B (en) | 1977-02-16 | 1978-09-27 | De Beers Ind Diamond | Hard materials |
| JPS5537570A (en) * | 1978-09-07 | 1980-03-15 | Kubota Ltd | Liquid conveying device |
| JPS5567570A (en) * | 1978-11-14 | 1980-05-21 | Mitsubishi Metal Corp | Ultrahigh pressure sintered tool material |
| GB2090239B (en) | 1980-07-31 | 1983-06-22 | Inst Khim Fiz An Sssr | Method of obtaining diamond and/or diamond-like modification of boron nitride |
| JPS58120505A (ja) * | 1982-01-06 | 1983-07-18 | Showa Denko Kk | 立方晶窒化ホウ素粒子 |
| US4695321A (en) * | 1985-06-21 | 1987-09-22 | New Mexico Tech Research Foundation | Dynamic compaction of composite materials containing diamond |
| JPH0699144B2 (ja) * | 1988-03-31 | 1994-12-07 | セントラル硝子株式会社 | ホウ素、炭素、窒素からなる塊状体およびその製造法 |
| JPH0699145B2 (ja) * | 1988-03-31 | 1994-12-07 | セントラル硝子株式会社 | ホウ素、炭素、窒素からなる繊維およびその製造法 |
| JPH01292823A (ja) * | 1988-05-20 | 1989-11-27 | Fujitsu Ltd | Ｘ線マスク |
| JPH0691954B2 (ja) * | 1988-06-16 | 1994-11-16 | 科学技術庁無機材質研究所長 | 立方晶ｂ−ｃ−ｎ結晶の製造法 |
| JPH02145263A (ja) * | 1988-11-25 | 1990-06-04 | Sumitomo Coal Mining Co Ltd | 研削砥石の製造方法 |
| JPH03126614A (ja) * | 1989-10-11 | 1991-05-29 | Mitsubishi Materials Corp | 炭素含有量の安定した炭窒化ボロン粉末の製造法 |
-
1993
- 1993-10-27 JP JP26885993A patent/JP3346496B2/ja not_active Expired - Lifetime
- 1993-11-02 SE SE9303605A patent/SE511152C2/sv not_active IP Right Cessation
- 1993-11-04 DE DE4337689A patent/DE4337689A1/de not_active Ceased
-
1996
- 1996-07-17 US US08/682,234 patent/US5866059A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE4337689A1 (de) | 1994-05-11 |
| JPH06316411A (ja) | 1994-11-15 |
| SE9303605D0 (sv) | 1993-11-02 |
| US5866059A (en) | 1999-02-02 |
| JP3346496B2 (ja) | 2002-11-18 |
| SE9303605L (sv) | 1994-05-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| NUG | Patent has lapsed |