SA517390626B1 - عملية لإنتاج حمض أسيتيك - Google Patents

عملية لإنتاج حمض أسيتيك

Info

Publication number
SA517390626B1
SA517390626B1 SA517390626A SA517390626A SA517390626B1 SA 517390626 B1 SA517390626 B1 SA 517390626B1 SA 517390626 A SA517390626 A SA 517390626A SA 517390626 A SA517390626 A SA 517390626A SA 517390626 B1 SA517390626 B1 SA 517390626B1
Authority
SA
Saudi Arabia
Prior art keywords
acetic acid
producing acetic
side stream
water concentration
concentration
Prior art date
Application number
SA517390626A
Other languages
English (en)
Inventor
دي شافير رونالد
او سكاتس مارك
ليو ياو-هوا
Original Assignee
سيلانيز انترناشونال كوربوريشن
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by سيلانيز انترناشونال كوربوريشن filed Critical سيلانيز انترناشونال كوربوريشن
Publication of SA517390626B1 publication Critical patent/SA517390626B1/ar

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/32Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42Regulation; Control
    • B01D3/4205Reflux ratio control splitter
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/09Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid esters or lactones
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

يتعلق الاختراع الحالي بعملية لإنتاج حمض أسيتيك يتم فيها التحكم بتركيز الماء في التيار الجانبي بين عمودين. وينتج عن التحكم في تركيز الماء من خلال إعادة تدوير الطور الخفيف السائل التحكم أيضًا بتركيز يوديد الهيدروجين في التيار الجانبي ليكون أقل من 50 جزء في المليون بالوزن أو يساويه.
SA517390626A 2015-07-01 2017-12-27 عملية لإنتاج حمض أسيتيك SA517390626B1 (ar)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14/788,928 US9302974B1 (en) 2015-07-01 2015-07-01 Process for producing acetic acid
PCT/US2015/053728 WO2017003497A1 (en) 2015-07-01 2015-10-02 Process for producing acetic acid

Publications (1)

Publication Number Publication Date
SA517390626B1 true SA517390626B1 (ar) 2021-05-18

Family

ID=54330062

Family Applications (1)

Application Number Title Priority Date Filing Date
SA517390626A SA517390626B1 (ar) 2015-07-01 2017-12-27 عملية لإنتاج حمض أسيتيك

Country Status (11)

Country Link
US (2) US9302974B1 (ar)
EP (2) EP3317244B1 (ar)
JP (1) JP6738356B2 (ar)
KR (1) KR102437425B1 (ar)
CN (1) CN107912038B (ar)
ES (1) ES2906720T3 (ar)
MX (2) MX2017016689A (ar)
MY (1) MY195744A (ar)
RS (1) RS62896B1 (ar)
SA (1) SA517390626B1 (ar)
WO (1) WO2017003497A1 (ar)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9302974B1 (en) * 2015-07-01 2016-04-05 Celanese International Corporation Process for producing acetic acid
EP3356321B1 (en) * 2015-10-02 2022-08-03 Celanese International Corporation Process to produce acetic acid with recycle of water
MY189357A (en) * 2017-03-28 2022-02-07 Daicel Corp Method for producing acetic acid
US20210189308A1 (en) * 2019-12-19 2021-06-24 Abv Technology, Inc. Process for separating a fermented malt beverage

Family Cites Families (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
US3791935A (en) 1971-11-10 1974-02-12 Monsanto Co Purification of carboxylic acids
US4008131A (en) 1975-12-11 1977-02-15 Monsanto Company Purification of acetic acid
US5026908A (en) 1984-05-03 1991-06-25 Hoechst Celanese Corporation Methanol carbonylation process
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
US5144068A (en) 1984-05-03 1992-09-01 Hoechst Celanese Corporation Methanol carbonylation process
US4615806B1 (en) 1985-03-07 1994-05-03 Hoechst Co American Removal of iodide compounds from non-aqueous organic media
GB9211671D0 (en) 1992-06-02 1992-07-15 Bp Chem Int Ltd Process
US5672743A (en) 1993-09-10 1997-09-30 Bp Chemicals Limited Process for the production of acetic acid
JP3377555B2 (ja) 1993-05-31 2003-02-17 ダイセル化学工業株式会社 カルボニル化反応生成物に含有されるヨウ素化合物の除去方法
JP3306227B2 (ja) * 1994-07-06 2002-07-24 ダイセル化学工業株式会社 酢酸および/または無水酢酸の製造法
US5880311A (en) * 1994-07-22 1999-03-09 Tonen Corporation Method of contacting catalyst particles with gas and liquid
US5696284A (en) 1995-06-21 1997-12-09 Bp Chemicals Limited Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof
UA48988C2 (uk) 1995-10-27 2002-09-16 Хьохст Селаниз Корпорейшн Спосіб підвищення продуктивності каталітичного розчину карбонілювання (варіанти), спосіб карбонілювання метанолу
IN192600B (ar) 1996-10-18 2004-05-08 Hoechst Celanese Corp
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
GB9625335D0 (en) 1996-12-05 1997-01-22 Bp Chem Int Ltd Process
GB9626429D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626317D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626428D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
JPH10231267A (ja) * 1997-02-19 1998-09-02 Chiyoda Corp 有機カルボン酸の製造方法
GB9816385D0 (en) 1998-07-29 1998-09-23 Bp Chem Int Ltd Process
US6552221B1 (en) * 1998-12-18 2003-04-22 Millenium Petrochemicals, Inc. Process control for acetic acid manufacture
US6225498B1 (en) 2000-03-24 2001-05-01 Celanese International Corporation Method of removing organic iodides from organic media
US6657078B2 (en) * 2001-02-07 2003-12-02 Celanese International Corporation Low energy carbonylation process
US6677480B2 (en) 2002-01-28 2004-01-13 Celanese International Corporation Process control in production of acetic acid via use of heavy phase density measurement
JP2004131389A (ja) 2002-10-08 2004-04-30 Daicel Chem Ind Ltd カルボン酸の製造方法及び製造システム
US7005541B2 (en) 2002-12-23 2006-02-28 Celanese International Corporation Low water methanol carbonylation process for high acetic acid production and for water balance control
US7223886B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7223883B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
JP4489487B2 (ja) 2004-04-02 2010-06-23 ダイセル化学工業株式会社 ヨウ化水素の分離方法
JP4732743B2 (ja) 2004-12-06 2011-07-27 ダイセル化学工業株式会社 蒸留方法
JP4526381B2 (ja) * 2004-12-27 2010-08-18 ダイセル化学工業株式会社 酢酸の製造方法
US7053241B1 (en) * 2005-02-24 2006-05-30 Celanese International Corporation Acetic acid production methods incorporating at least one metal salt as a catalyst stabilizer
US7855306B2 (en) 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
US7820855B2 (en) 2008-04-29 2010-10-26 Celanese International Corporation Method and apparatus for carbonylating methanol with acetic acid enriched flash stream
WO2009134332A2 (en) 2008-04-29 2009-11-05 Celanese International Corporation Methanol carbonylation system having absorber with multiple solvent options
US7884237B2 (en) 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal
US8889904B2 (en) 2010-05-18 2014-11-18 Celanese International Corporation Processes for producing acetic acid
CN103038207B (zh) 2010-07-26 2015-03-04 株式会社大赛璐 生产乙酸的方法
WO2012046593A1 (ja) 2010-10-06 2012-04-12 ダイセル化学工業株式会社 酢酸の製造方法
CN103153933B (zh) 2010-10-13 2016-01-06 国际人造丝公司 回收卤素促进剂和除去高锰酸盐还原化合物的方法
JP6166043B2 (ja) 2010-12-15 2017-07-19 株式会社ダイセル 酢酸の製造方法
US9115071B2 (en) 2010-12-15 2015-08-25 Daicel Corporation Process for producing acetic acid
USRE46999E1 (en) 2010-12-15 2018-08-21 Daicel Corporation Process for producing acetic acid
CN103402967B (zh) 2010-12-24 2015-11-25 株式会社大赛璐 乙酸的制备方法
US8629298B2 (en) * 2011-02-28 2014-01-14 Lyondell Chemical Technology, L.P. Acetic acid production process
US8697908B2 (en) 2011-05-05 2014-04-15 Celanese International Corporation Removal of amine compounds from carbonylation process stream containing corrosion metal contaminants
JP5894297B2 (ja) * 2011-12-28 2016-03-23 イーストマン ケミカル カンパニー 水性ヨウ化水素及び酢酸を用いた触媒回収
TWI547477B (zh) * 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
AR094541A1 (es) 2013-01-25 2015-08-12 Daicel Corp Procedimiento para producir ácido carboxílico
US9382186B1 (en) * 2015-07-01 2016-07-05 Celanese International Corporation Process for producing acetic acid
US9302974B1 (en) * 2015-07-01 2016-04-05 Celanese International Corporation Process for producing acetic acid
US9416088B1 (en) * 2015-10-02 2016-08-16 Celanese International Corporation Process to produce acetic acid with recycle of water

Also Published As

Publication number Publication date
MY195744A (en) 2023-02-08
EP3317244B1 (en) 2021-12-01
EP3950656A1 (en) 2022-02-09
ES2906720T3 (es) 2022-04-20
JP6738356B2 (ja) 2020-08-12
KR102437425B1 (ko) 2022-08-26
US20170001937A1 (en) 2017-01-05
WO2017003497A1 (en) 2017-01-05
CN107912038A (zh) 2018-04-13
US9302974B1 (en) 2016-04-05
CN107912038B (zh) 2021-05-04
MX2017016689A (es) 2018-03-26
EP3317244A1 (en) 2018-05-09
MX2023003730A (es) 2023-04-24
RS62896B1 (sr) 2022-03-31
JP2018524332A (ja) 2018-08-30
KR20180022991A (ko) 2018-03-06
US9676694B2 (en) 2017-06-13

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