SA517390626B1 - عملية لإنتاج حمض أسيتيك - Google Patents
عملية لإنتاج حمض أسيتيكInfo
- Publication number
- SA517390626B1 SA517390626B1 SA517390626A SA517390626A SA517390626B1 SA 517390626 B1 SA517390626 B1 SA 517390626B1 SA 517390626 A SA517390626 A SA 517390626A SA 517390626 A SA517390626 A SA 517390626A SA 517390626 B1 SA517390626 B1 SA 517390626B1
- Authority
- SA
- Saudi Arabia
- Prior art keywords
- acetic acid
- producing acetic
- side stream
- water concentration
- concentration
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/42—Regulation; Control
- B01D3/4205—Reflux ratio control splitter
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/09—Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid esters or lactones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
- C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
- C07C53/08—Acetic acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
يتعلق الاختراع الحالي بعملية لإنتاج حمض أسيتيك يتم فيها التحكم بتركيز الماء في التيار الجانبي بين عمودين. وينتج عن التحكم في تركيز الماء من خلال إعادة تدوير الطور الخفيف السائل التحكم أيضًا بتركيز يوديد الهيدروجين في التيار الجانبي ليكون أقل من 50 جزء في المليون بالوزن أو يساويه.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US14/788,928 US9302974B1 (en) | 2015-07-01 | 2015-07-01 | Process for producing acetic acid |
PCT/US2015/053728 WO2017003497A1 (en) | 2015-07-01 | 2015-10-02 | Process for producing acetic acid |
Publications (1)
Publication Number | Publication Date |
---|---|
SA517390626B1 true SA517390626B1 (ar) | 2021-05-18 |
Family
ID=54330062
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SA517390626A SA517390626B1 (ar) | 2015-07-01 | 2017-12-27 | عملية لإنتاج حمض أسيتيك |
Country Status (11)
Country | Link |
---|---|
US (2) | US9302974B1 (ar) |
EP (2) | EP3317244B1 (ar) |
JP (1) | JP6738356B2 (ar) |
KR (1) | KR102437425B1 (ar) |
CN (1) | CN107912038B (ar) |
ES (1) | ES2906720T3 (ar) |
MX (2) | MX2017016689A (ar) |
MY (1) | MY195744A (ar) |
RS (1) | RS62896B1 (ar) |
SA (1) | SA517390626B1 (ar) |
WO (1) | WO2017003497A1 (ar) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9302974B1 (en) * | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for producing acetic acid |
EP3356321B1 (en) * | 2015-10-02 | 2022-08-03 | Celanese International Corporation | Process to produce acetic acid with recycle of water |
MY189357A (en) * | 2017-03-28 | 2022-02-07 | Daicel Corp | Method for producing acetic acid |
US20210189308A1 (en) * | 2019-12-19 | 2021-06-24 | Abv Technology, Inc. | Process for separating a fermented malt beverage |
Family Cites Families (54)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3769329A (en) | 1970-03-12 | 1973-10-30 | Monsanto Co | Production of carboxylic acids and esters |
US3791935A (en) | 1971-11-10 | 1974-02-12 | Monsanto Co | Purification of carboxylic acids |
US4008131A (en) | 1975-12-11 | 1977-02-15 | Monsanto Company | Purification of acetic acid |
US5026908A (en) | 1984-05-03 | 1991-06-25 | Hoechst Celanese Corporation | Methanol carbonylation process |
US5001259A (en) | 1984-05-03 | 1991-03-19 | Hoechst Celanese Corporation | Methanol carbonylation process |
US5144068A (en) | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
US4615806B1 (en) | 1985-03-07 | 1994-05-03 | Hoechst Co American | Removal of iodide compounds from non-aqueous organic media |
GB9211671D0 (en) | 1992-06-02 | 1992-07-15 | Bp Chem Int Ltd | Process |
US5672743A (en) | 1993-09-10 | 1997-09-30 | Bp Chemicals Limited | Process for the production of acetic acid |
JP3377555B2 (ja) | 1993-05-31 | 2003-02-17 | ダイセル化学工業株式会社 | カルボニル化反応生成物に含有されるヨウ素化合物の除去方法 |
JP3306227B2 (ja) * | 1994-07-06 | 2002-07-24 | ダイセル化学工業株式会社 | 酢酸および/または無水酢酸の製造法 |
US5880311A (en) * | 1994-07-22 | 1999-03-09 | Tonen Corporation | Method of contacting catalyst particles with gas and liquid |
US5696284A (en) | 1995-06-21 | 1997-12-09 | Bp Chemicals Limited | Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof |
UA48988C2 (uk) | 1995-10-27 | 2002-09-16 | Хьохст Селаниз Корпорейшн | Спосіб підвищення продуктивності каталітичного розчину карбонілювання (варіанти), спосіб карбонілювання метанолу |
IN192600B (ar) | 1996-10-18 | 2004-05-08 | Hoechst Celanese Corp | |
US6339171B1 (en) | 1996-10-18 | 2002-01-15 | Celanese International Corporation | Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream |
GB9625335D0 (en) | 1996-12-05 | 1997-01-22 | Bp Chem Int Ltd | Process |
GB9626429D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
GB9626317D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
GB9626428D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
JPH10231267A (ja) * | 1997-02-19 | 1998-09-02 | Chiyoda Corp | 有機カルボン酸の製造方法 |
GB9816385D0 (en) | 1998-07-29 | 1998-09-23 | Bp Chem Int Ltd | Process |
US6552221B1 (en) * | 1998-12-18 | 2003-04-22 | Millenium Petrochemicals, Inc. | Process control for acetic acid manufacture |
US6225498B1 (en) | 2000-03-24 | 2001-05-01 | Celanese International Corporation | Method of removing organic iodides from organic media |
US6657078B2 (en) * | 2001-02-07 | 2003-12-02 | Celanese International Corporation | Low energy carbonylation process |
US6677480B2 (en) | 2002-01-28 | 2004-01-13 | Celanese International Corporation | Process control in production of acetic acid via use of heavy phase density measurement |
JP2004131389A (ja) | 2002-10-08 | 2004-04-30 | Daicel Chem Ind Ltd | カルボン酸の製造方法及び製造システム |
US7005541B2 (en) | 2002-12-23 | 2006-02-28 | Celanese International Corporation | Low water methanol carbonylation process for high acetic acid production and for water balance control |
US7223886B2 (en) | 2004-03-02 | 2007-05-29 | Celanese International Corporation | Removal of permanganate reducing compounds from methanol carbonylation process stream |
US7223883B2 (en) | 2004-03-02 | 2007-05-29 | Celanese International Corporation | Removal of permanganate reducing compounds from methanol carbonylation process stream |
JP4489487B2 (ja) | 2004-04-02 | 2010-06-23 | ダイセル化学工業株式会社 | ヨウ化水素の分離方法 |
JP4732743B2 (ja) | 2004-12-06 | 2011-07-27 | ダイセル化学工業株式会社 | 蒸留方法 |
JP4526381B2 (ja) * | 2004-12-27 | 2010-08-18 | ダイセル化学工業株式会社 | 酢酸の製造方法 |
US7053241B1 (en) * | 2005-02-24 | 2006-05-30 | Celanese International Corporation | Acetic acid production methods incorporating at least one metal salt as a catalyst stabilizer |
US7855306B2 (en) | 2005-04-28 | 2010-12-21 | Celanese International Corporation | Process for the production of acetic acid |
US7820855B2 (en) | 2008-04-29 | 2010-10-26 | Celanese International Corporation | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream |
WO2009134332A2 (en) | 2008-04-29 | 2009-11-05 | Celanese International Corporation | Methanol carbonylation system having absorber with multiple solvent options |
US7884237B2 (en) | 2008-11-07 | 2011-02-08 | Celanese International Corp. | Methanol carbonylation with improved aldehyde removal |
US8889904B2 (en) | 2010-05-18 | 2014-11-18 | Celanese International Corporation | Processes for producing acetic acid |
CN103038207B (zh) | 2010-07-26 | 2015-03-04 | 株式会社大赛璐 | 生产乙酸的方法 |
WO2012046593A1 (ja) | 2010-10-06 | 2012-04-12 | ダイセル化学工業株式会社 | 酢酸の製造方法 |
CN103153933B (zh) | 2010-10-13 | 2016-01-06 | 国际人造丝公司 | 回收卤素促进剂和除去高锰酸盐还原化合物的方法 |
JP6166043B2 (ja) | 2010-12-15 | 2017-07-19 | 株式会社ダイセル | 酢酸の製造方法 |
US9115071B2 (en) | 2010-12-15 | 2015-08-25 | Daicel Corporation | Process for producing acetic acid |
USRE46999E1 (en) | 2010-12-15 | 2018-08-21 | Daicel Corporation | Process for producing acetic acid |
CN103402967B (zh) | 2010-12-24 | 2015-11-25 | 株式会社大赛璐 | 乙酸的制备方法 |
US8629298B2 (en) * | 2011-02-28 | 2014-01-14 | Lyondell Chemical Technology, L.P. | Acetic acid production process |
US8697908B2 (en) | 2011-05-05 | 2014-04-15 | Celanese International Corporation | Removal of amine compounds from carbonylation process stream containing corrosion metal contaminants |
JP5894297B2 (ja) * | 2011-12-28 | 2016-03-23 | イーストマン ケミカル カンパニー | 水性ヨウ化水素及び酢酸を用いた触媒回収 |
TWI547477B (zh) * | 2012-03-14 | 2016-09-01 | 大賽璐股份有限公司 | 醋酸之製造方法 |
AR094541A1 (es) | 2013-01-25 | 2015-08-12 | Daicel Corp | Procedimiento para producir ácido carboxílico |
US9382186B1 (en) * | 2015-07-01 | 2016-07-05 | Celanese International Corporation | Process for producing acetic acid |
US9302974B1 (en) * | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for producing acetic acid |
US9416088B1 (en) * | 2015-10-02 | 2016-08-16 | Celanese International Corporation | Process to produce acetic acid with recycle of water |
-
2015
- 2015-07-01 US US14/788,928 patent/US9302974B1/en active Active
- 2015-10-02 EP EP15781521.8A patent/EP3317244B1/en active Active
- 2015-10-02 MY MYPI2017705052A patent/MY195744A/en unknown
- 2015-10-02 CN CN201580081306.7A patent/CN107912038B/zh active Active
- 2015-10-02 KR KR1020187003291A patent/KR102437425B1/ko active IP Right Grant
- 2015-10-02 EP EP21194488.9A patent/EP3950656A1/en active Pending
- 2015-10-02 WO PCT/US2015/053728 patent/WO2017003497A1/en active Application Filing
- 2015-10-02 ES ES15781521T patent/ES2906720T3/es active Active
- 2015-10-02 RS RS20220125A patent/RS62896B1/sr unknown
- 2015-10-02 JP JP2017566862A patent/JP6738356B2/ja active Active
- 2015-10-02 MX MX2017016689A patent/MX2017016689A/es unknown
-
2016
- 2016-03-17 US US15/073,111 patent/US9676694B2/en active Active
-
2017
- 2017-12-18 MX MX2023003730A patent/MX2023003730A/es unknown
- 2017-12-27 SA SA517390626A patent/SA517390626B1/ar unknown
Also Published As
Publication number | Publication date |
---|---|
MY195744A (en) | 2023-02-08 |
EP3317244B1 (en) | 2021-12-01 |
EP3950656A1 (en) | 2022-02-09 |
ES2906720T3 (es) | 2022-04-20 |
JP6738356B2 (ja) | 2020-08-12 |
KR102437425B1 (ko) | 2022-08-26 |
US20170001937A1 (en) | 2017-01-05 |
WO2017003497A1 (en) | 2017-01-05 |
CN107912038A (zh) | 2018-04-13 |
US9302974B1 (en) | 2016-04-05 |
CN107912038B (zh) | 2021-05-04 |
MX2017016689A (es) | 2018-03-26 |
EP3317244A1 (en) | 2018-05-09 |
MX2023003730A (es) | 2023-04-24 |
RS62896B1 (sr) | 2022-03-31 |
JP2018524332A (ja) | 2018-08-30 |
KR20180022991A (ko) | 2018-03-06 |
US9676694B2 (en) | 2017-06-13 |
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