SA516380564B1 - عملية لتحضير داي أمينات وعديد أمينات من سلسلة داي فنيل ميثان - Google Patents
عملية لتحضير داي أمينات وعديد أمينات من سلسلة داي فنيل ميثان Download PDFInfo
- Publication number
- SA516380564B1 SA516380564B1 SA516380564A SA516380564A SA516380564B1 SA 516380564 B1 SA516380564 B1 SA 516380564B1 SA 516380564 A SA516380564 A SA 516380564A SA 516380564 A SA516380564 A SA 516380564A SA 516380564 B1 SA516380564 B1 SA 516380564B1
- Authority
- SA
- Saudi Arabia
- Prior art keywords
- aniline
- reactor
- formaldehyde
- flow rate
- mass flow
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract 13
- 229920000768 polyamine Polymers 0.000 title claims abstract 6
- CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical class C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 title claims 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims abstract 36
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract 36
- 239000002253 acid Substances 0.000 claims 6
- 150000004985 diamines Chemical class 0.000 claims 3
- 150000007854 aminals Chemical class 0.000 claims 2
- CUHVTYCUTYWQOR-UHFFFAOYSA-N formaldehyde Chemical compound O=C.O=C CUHVTYCUTYWQOR-UHFFFAOYSA-N 0.000 claims 2
- 239000012074 organic phase Substances 0.000 claims 2
- 239000011541 reaction mixture Substances 0.000 claims 2
- 241000196324 Embryophyta Species 0.000 claims 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims 1
- 102000036770 Islet Amyloid Polypeptide Human genes 0.000 claims 1
- 108010041872 Islet Amyloid Polypeptide Proteins 0.000 claims 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 1
- 239000003377 acid catalyst Substances 0.000 claims 1
- 239000008346 aqueous phase Substances 0.000 claims 1
- 239000002956 ash Substances 0.000 claims 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-O phenylazanium Chemical class [NH3+]C1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-O 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 230000002123 temporal effect Effects 0.000 claims 1
- 239000011800 void material Substances 0.000 claims 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
- C07C209/78—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton from carbonyl compounds, e.g. from formaldehyde, and amines having amino groups bound to carbon atoms of six-membered aromatic rings, with formation of methylene-diarylamines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
- C07C211/44—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
- C07C211/49—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/0059—Sequential processes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14173582 | 2014-06-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SA516380564B1 true SA516380564B1 (ar) | 2020-11-03 |
Family
ID=50980958
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SA516380564A SA516380564B1 (ar) | 2014-06-24 | 2016-12-21 | عملية لتحضير داي أمينات وعديد أمينات من سلسلة داي فنيل ميثان |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US10125091B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP3160936B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP6742923B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR20170021850A (cg-RX-API-DMAC7.html) |
| CN (1) | CN106458845B (cg-RX-API-DMAC7.html) |
| HU (1) | HUE057295T2 (cg-RX-API-DMAC7.html) |
| PT (1) | PT3160936T (cg-RX-API-DMAC7.html) |
| SA (1) | SA516380564B1 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2015197520A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015197519A1 (de) * | 2014-06-24 | 2015-12-30 | Covestro Deutschland Ag | Verfahren zur herstellung von di- und polyaminen derdiphenylmethanreihe |
| US10640453B2 (en) | 2016-12-22 | 2020-05-05 | Covestro Deutschland Ag | Method of producing diamines and polyamines of the diphenylmethane series |
| US10640455B1 (en) | 2016-12-22 | 2020-05-05 | Covestro Deutschland Ag | Method of producing diamines and polyamines of the diphenylmethane series |
| CN110291063B (zh) * | 2016-12-22 | 2022-07-05 | 科思创德国股份有限公司 | 在不同的生产能力下制备二苯基甲烷系列的二胺和多胺的方法 |
| EP3558928B1 (de) | 2016-12-22 | 2021-01-20 | Covestro Intellectual Property GmbH & Co. KG | Verfahren zur herstellung von di- und polyaminen der diphenylmethanreihe bei unterschiedlichen produktions-kapazitäten |
| CN114315598B (zh) * | 2020-09-29 | 2024-02-02 | 万华化学集团股份有限公司 | 一种二苯基甲烷系列二胺和多胺的制备方法 |
| US11542223B1 (en) * | 2022-07-21 | 2023-01-03 | Covestro Llc | Process for preparing di- and polyamines of the diphenyl methane series |
| EP4345088B1 (en) | 2022-09-29 | 2025-10-22 | Covestro Deutschland AG | A process for preparing di- and polyamines of the diphenyl methane series |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE844896C (de) | 1944-04-04 | 1952-09-15 | Bayer Ag | Verfahren zur Herstellung von organischen Isocyanaten |
| GB1517585A (en) | 1974-11-13 | 1978-07-12 | Mobay Chemical Corp | Process for the production of a polyamino-polyphenyl-(poly)-methylene polyamine |
| US4792624A (en) * | 1987-02-26 | 1988-12-20 | The Dow Chemical Company | Process for polymeric MDA, recycle of finished polymeric MDA |
| JP2825604B2 (ja) | 1990-04-11 | 1998-11-18 | 三井化学株式会社 | メチレン架橋されたポリアリールアミンの製造方法 |
| DE4021712A1 (de) * | 1990-07-07 | 1992-01-09 | Basf Ag | Verfahren zur herstellung von mischungen aus diphenylmethan-diisocyanaten und polyphenol-polymethylen-polyisocyanaten mit einer verminderten iodfarbzahl |
| US5286760A (en) | 1992-10-09 | 1994-02-15 | Miles, Inc. | Process for reducing impurity levels in methylene diphenyamines |
| DE19804915A1 (de) | 1998-02-07 | 1999-08-12 | Basf Ag | Verfahren zur Herstellung von Methylendi(phenylamin) und Methylendi(phenylisocyanat) |
| DE19817691A1 (de) | 1998-04-21 | 1999-10-28 | Basf Ag | Verfahren zur Herstellung von Mischungen aus Diphenylmehandiisocyanaten und Polyphenylen-polymethylen-polyisocyanaten mit vermindertem Gehalt an chlorierten Nebenprodukten und verminderter Jodfarbzahl |
| DE10006452A1 (de) | 2000-02-14 | 2001-08-16 | Bayer Ag | Verfahren zur Herstellung von Diaminodiphenylmethanen |
| DE102004032416A1 (de) | 2004-07-05 | 2006-02-02 | Bayer Materialscience Ag | Verfahren zur Herstellung von Polyaminen der Diphenylmethanreihe bei niedriger Protonierung |
| DE102004052370A1 (de) | 2004-10-28 | 2006-05-04 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| DE102006004047A1 (de) | 2006-01-28 | 2007-08-02 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| DE102006004041A1 (de) | 2006-01-28 | 2007-08-02 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| DE102008015123A1 (de) | 2008-03-20 | 2009-09-24 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| HUE026867T2 (en) * | 2010-12-29 | 2016-08-29 | Wanhua Chemical Group Co Ltd | Fast mixing reactor and application |
| WO2015197519A1 (de) * | 2014-06-24 | 2015-12-30 | Covestro Deutschland Ag | Verfahren zur herstellung von di- und polyaminen derdiphenylmethanreihe |
-
2015
- 2015-06-22 JP JP2016575046A patent/JP6742923B2/ja active Active
- 2015-06-22 HU HUE15731295A patent/HUE057295T2/hu unknown
- 2015-06-22 KR KR1020177001651A patent/KR20170021850A/ko not_active Withdrawn
- 2015-06-22 US US15/318,102 patent/US10125091B2/en active Active
- 2015-06-22 EP EP15731295.0A patent/EP3160936B1/de active Active
- 2015-06-22 PT PT157312950T patent/PT3160936T/pt unknown
- 2015-06-22 CN CN201580034279.8A patent/CN106458845B/zh not_active Expired - Fee Related
- 2015-06-22 WO PCT/EP2015/063923 patent/WO2015197520A1/de not_active Ceased
-
2016
- 2016-12-21 SA SA516380564A patent/SA516380564B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP3160936B1 (de) | 2021-10-13 |
| US20170107171A1 (en) | 2017-04-20 |
| CN106458845B (zh) | 2019-10-22 |
| HUE057295T2 (hu) | 2022-05-28 |
| JP2017520564A (ja) | 2017-07-27 |
| KR20170021850A (ko) | 2017-02-28 |
| PT3160936T (pt) | 2021-12-29 |
| EP3160936A1 (de) | 2017-05-03 |
| JP6742923B2 (ja) | 2020-08-19 |
| US10125091B2 (en) | 2018-11-13 |
| CN106458845A (zh) | 2017-02-22 |
| WO2015197520A1 (de) | 2015-12-30 |
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