RU99111265A - COMPOSITION FOR DIRECT COLORING KERATIN FIBERS WITH DIRECT CATIONIC DYE AND POLYOL AND / OR SIMPLE POLYOL ETHER - Google Patents

COMPOSITION FOR DIRECT COLORING KERATIN FIBERS WITH DIRECT CATIONIC DYE AND POLYOL AND / OR SIMPLE POLYOL ETHER

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Publication number
RU99111265A
RU99111265A RU99111265/14A RU99111265A RU99111265A RU 99111265 A RU99111265 A RU 99111265A RU 99111265/14 A RU99111265/14 A RU 99111265/14A RU 99111265 A RU99111265 A RU 99111265A RU 99111265 A RU99111265 A RU 99111265A
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Prior art keywords
composition
direct
composition according
polyol
alkyl
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RU99111265/14A
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Russian (ru)
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RU2166930C2 (en
Inventor
Кристин Рондо
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Л`Ореаль
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Priority claimed from FR9806751A external-priority patent/FR2779055B1/en
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Claims (1)

1. Композиция для прямого окрашивания кератиновых волокон, в частности, кератиновых волокон человека таких как волосы, содержащая в подходящей для окрашивания среде, которая не содержит оксидаз или оксиредуктаз, по меньшей мере один прямой катионный краситель приведенных ниже формул I, II, III и III':
Figure 00000001

где D обозначает атом азота или группу -СН;
R1 и R2, одинаковые или разные, обозначают атом водорода, радикал С1-С4-алкил, который может быть замещен радикалами CN, ОН или NH2, или вместе с атомом углерода бензольного цикла образуют кислород- или азотсодержащий гетероцикл, который может быть замещен одним или несколькими С1-С4-алкилами, или радикал 4'-аминофенил;
R3 и R3' одинаковые или разные, обозначают атом водорода или галогена, выбранный из хлора, брома, иода и фтора, радикал циано, С1-С4-алкил, С1-С4-алкокси или ацетокси;
X- обозначает анион, преимущественно выбранный из хлорида, метилсульфата и ацетата;
А обозначает группу, выбранную из приведенных ниже структур А1-А18:
Figure 00000002

Figure 00000003

Figure 00000004

Figure 00000005

Figure 00000006

Figure 00000007

Figure 00000008

Figure 00000009

Figure 00000010

Figure 00000011

Figure 00000012

Figure 00000013

Figure 00000014

Figure 00000015

Figure 00000016

Figure 00000017

Figure 00000018

Figure 00000019

где R4 обозначает С1-С4-алкил, который может быть замещен гидроксилом,
R5 обозначает С1-С4-алкокси-радикал при условии, что, когда D обозначает -СН, А обозначает А4 или А13 и R3 не является алкокси-радикалом, то R1 и R2 не могут быть одновременно атомами водорода;
Figure 00000020

где R6 обозначает атом водорода или С1-С4-алкил;
R7 обозначает атом водорода, радикал алкил, который может быть замещен радикалом -CN или аминогруппой, радикал 4'-аминофенил, или вместе с R6 образует кислород- и/или азотсодержащий гетероцикл, который может быть замещен С1-С4-алкилом;
R8 и R9, одинаковые или разные, обозначают атом водорода или галогена, выбранный из хлора, брома, иода и фтора, радикалы С1-С4-алкил, С1-С4-алкокси или -CN;
Х- обозначает анион, преимущественно выбранный из хлорида, метилсульфата и ацетата;
В обозначает группу, выбранную из приведенных ниже структур B1-B6:
Figure 00000021

Figure 00000022

Figure 00000023

Figure 00000024

Figure 00000025

Figure 00000026

где R1 обозначает С1-С4-алкил;
R11 и R12, одинаковые или разные, обозначают атом водорода или С1-С4-алкил;
Figure 00000027

Figure 00000028

где R13 обозначает атом водорода, С1-С4-алкокси, атом галогена, выбранный из хлора, брома, иода и фтора, или аминогруппу;
R14 обозначает атом водорода, С1-С4-алкил или, вместе с атомом углерода бензольного цикла, образует кислород- содержащий и/или замещенный одним или несколькими С1-С4-алкил-радикалами гетероцикл;
R15 обозначает атом водорода или галогена: хлор, бром, иод или фтор;
R16 и R17, одинаковые или разные, обозначают атом водорода или С1-С4-алкил;
D1 и D2, одинаковые или разные, обозначают атом азота или группу -СН;
m = 0 или 1,
при условии, что, когда R13 обозначает незамещенную аминогруппу, тогда D1 и D2 одновременно обозначают группу -СН и m=0;
Х- обозначает анион, преимущественно выбранный из хлорида, метилсульфата и ацетата;
Е обозначает группу, выбранную из приведенных ниже структур Е1-Е8:
Figure 00000029

Figure 00000030

Figure 00000031

Figure 00000032

Figure 00000033

Figure 00000034

Figure 00000035

Figure 00000036

где R' обозначает С1-С4-алкил;
когда m = 0 и D1 обозначает атом азота, тогда Е может также обозначать группу, имеющую приведенную ниже структуру E9
Figure 00000037

где R' обозначает С1-С4-алкил;
причем названная композиция отличается тем, что она также содержит по меньшей мере один полиол или простой алифатический С1-С8-эфир С3-С9-полиола и/или простой ароматический С6-С8-эфир С2-С9-полиола.1. Composition for direct dyeing of keratin fibers, in particular, human keratin fibers such as hair, containing at least one direct cationic dye of the following formulas in the following suitable for dyeing that does not contain oxidases or oxidoreductases; ':
Figure 00000001

where D denotes a nitrogen atom or a group-CH;
R 1 and R 2 , which are the same or different, denote a hydrogen atom, a C 1 -C 4 -alkyl radical which may be substituted by CN, OH or NH 2 , or together with the carbon atom of the benzene ring form an oxygen or nitrogen-containing heterocycle may be substituted with one or more C 1 -C 4 -alkyls, or the 4'-aminophenyl radical;
R 3 and R 3 'are the same or different, represent a hydrogen or halogen atom selected from chlorine, bromine, iodine and fluorine, a cyano radical, C 1 -C 4 alkyl, C 1 -C 4 alkoxy or acetoxy;
X - denotes an anion predominantly selected from chloride, methyl sulfate and acetate;
And indicates a group selected from the following structures A1-A18:
Figure 00000002

Figure 00000003

Figure 00000004

Figure 00000005

Figure 00000006

Figure 00000007

Figure 00000008

Figure 00000009

Figure 00000010

Figure 00000011

Figure 00000012

Figure 00000013

Figure 00000014

Figure 00000015

Figure 00000016

Figure 00000017

Figure 00000018

Figure 00000019

where R 4 stands With 1 -C 4 -alkyl, which may be substituted by hydroxyl,
R 5 is a C 1 -C 4 -alkoxy radical provided that when D is —CH, A is A4 or A13 and R 3 is not an alkoxy radical, then R 1 and R 2 cannot be hydrogen atoms simultaneously;
Figure 00000020

where R 6 denotes a hydrogen atom or a C 1 -C 4 -alkyl;
R 7 denotes a hydrogen atom, an alkyl radical, which may be substituted by a -CN radical or an amino group, a 4'-aminophenyl radical, or together with R 6 forms an oxygen- and / or nitrogen-containing heterocycle, which may be substituted with C 1 -C 4 alkyl ;
R 8 and R 9 , which are the same or different, represent a hydrogen or halogen atom selected from chlorine, bromine, iodine and fluorine, C 1 -C 4 -alkyl radicals, C 1 -C 4 -alkoxy or -CN;
X - denotes an anion predominantly selected from chloride, methyl sulfate and acetate;
B stands for a group selected from the structures B 1 -B 6 below:
Figure 00000021

Figure 00000022

Figure 00000023

Figure 00000024

Figure 00000025

Figure 00000026

where R 1 stands With 1 -C 4 -alkyl;
R 11 and R 12 , which are the same or different, represent a hydrogen atom or C 1 -C 4 -alkyl;
Figure 00000027

Figure 00000028

where R 13 denotes a hydrogen atom, C 1 -C 4 -alkoxy, a halogen atom selected from chlorine, bromine, iodine and fluorine, or an amino group;
R 14 represents a hydrogen atom, C 1 -C 4 -alkyl or, together with the carbon atom of the benzene ring, forms an oxygen-containing and / or heterocycle substituted by one or more C 1 -C 4 -alkyl radicals;
R 15 denotes a hydrogen or halogen atom: chlorine, bromine, iodine or fluorine;
R 16 and R 17 , which are the same or different, represent a hydrogen atom or C 1 -C 4 -alkyl;
D 1 and D 2 , the same or different, represent a nitrogen atom or a —CH group;
m = 0 or 1,
provided that when R 13 denotes an unsubstituted amino group, then D 1 and D 2 simultaneously denote the group —CH and m = 0;
X - denotes an anion predominantly selected from chloride, methyl sulfate and acetate;
E denotes a group selected from the following structures E1-E8:
Figure 00000029

Figure 00000030

Figure 00000031

Figure 00000032

Figure 00000033

Figure 00000034

Figure 00000035

Figure 00000036

where R 'is a C 1 -C 4 -alkyl;
when m = 0 and D 1 denotes a nitrogen atom, then E may also denote a group having the following structure E9
Figure 00000037

where R 'is a C 1 -C 4 -alkyl;
moreover, the above composition is characterized in that it also contains at least one polyol or a simple aliphatic C 1 -C 8 -ether C 3 -C 9 -polyol and / or a simple aromatic C 6 -C 8 -ether C 2 -C 9 - polyol. 2. Композиция по п.1, отличающаяся тем, что прямые катионные красители формулы I выбраны из приведенных ниже структур I 1 - I 54:
Figure 00000038

Figure 00000039

Figure 00000040

Figure 00000041

Figure 00000042

Figure 00000043

Figure 00000044

Figure 00000045

Figure 00000046

Figure 00000047

Figure 00000048

Figure 00000049

Figure 00000050

Figure 00000051

Figure 00000052

Figure 00000053

Figure 00000054

Figure 00000055

Figure 00000056

Figure 00000057

Figure 00000058

Figure 00000059

Figure 00000060

Figure 00000061

Figure 00000062

Figure 00000063

Figure 00000064

Figure 00000065

Figure 00000066

Figure 00000067

Figure 00000068

Figure 00000069

Figure 00000070

Figure 00000071

Figure 00000072

Figure 00000073

Figure 00000074

Figure 00000075

Figure 00000076

Figure 00000077

Figure 00000078

Figure 00000079

Figure 00000080

Figure 00000081

Figure 00000082

Figure 00000083

Figure 00000084

Figure 00000085

Figure 00000086

Figure 00000087

Figure 00000088

Figure 00000089

Figure 00000090

Figure 00000091

3. Композиция по п.2, отличающаяся тем, что прямые катионные красители соответствуют структурам I 1, I 2, I 4 и I 31.2. The composition according to claim 1, characterized in that the direct cationic dyes of the formula I are selected from the following structures I 1 - I 54:
Figure 00000038

Figure 00000039

Figure 00000040

Figure 00000041

Figure 00000042

Figure 00000043

Figure 00000044

Figure 00000045

Figure 00000046

Figure 00000047

Figure 00000048

Figure 00000049

Figure 00000050

Figure 00000051

Figure 00000052

Figure 00000053

Figure 00000054

Figure 00000055

Figure 00000056

Figure 00000057

Figure 00000058

Figure 00000059

Figure 00000060

Figure 00000061

Figure 00000062

Figure 00000063

Figure 00000064

Figure 00000065

Figure 00000066

Figure 00000067

Figure 00000068

Figure 00000069

Figure 00000070

Figure 00000071

Figure 00000072

Figure 00000073

Figure 00000074

Figure 00000075

Figure 00000076

Figure 00000077

Figure 00000078

Figure 00000079

Figure 00000080

Figure 00000081

Figure 00000082

Figure 00000083

Figure 00000084

Figure 00000085

Figure 00000086

Figure 00000087

Figure 00000088

Figure 00000089

Figure 00000090

Figure 00000091

3. The composition according to claim 2, characterized in that the direct cationic dyes correspond to the structures I 1, I 2, I 4 and I 31. 4. Композиция по п.1, отличающаяся тем, что прямые катионные красители формулы II выбраны из числа соединений, отвечающих приведенным ниже структурам II 1 - II 9:
Figure 00000092

Figure 00000093

Figure 00000094

Figure 00000095

Figure 00000096

Figure 00000097

Figure 00000098

Figure 00000099

Figure 00000100

5. Композиция по п.1, отличающаяся тем, что прямые катионные красители формулы III выбраны из числа соединений, отвечающих приведенным ниже структурам III 1 - III 18:
Figure 00000101

Figure 00000102

Figure 00000103

Figure 00000104

Figure 00000105

Figure 00000106

Figure 00000107

Figure 00000108

Figure 00000109

Figure 00000110

Figure 00000111

Figure 00000112

Figure 00000113

Figure 00000114

Figure 00000115

Figure 00000116

Figure 00000117

Figure 00000118

6. Композиция по п.5, отличающаяся тем, что прямые катионные красители формулы III выбраны из числа соединений, отвечающих структурам III 4, III 5 и III 13.4. The composition according to claim 1, characterized in that the direct cationic dyes of formula II are selected from among the compounds corresponding to the structures II 1 - II 9 below:
Figure 00000092

Figure 00000093

Figure 00000094

Figure 00000095

Figure 00000096

Figure 00000097

Figure 00000098

Figure 00000099

Figure 00000100

5. The composition according to claim 1, characterized in that the direct cationic dyes of the formula III are selected from among the compounds corresponding to the structures III 1 to III 18 below:
Figure 00000101

Figure 00000102

Figure 00000103

Figure 00000104

Figure 00000105

Figure 00000106

Figure 00000107

Figure 00000108

Figure 00000109

Figure 00000110

Figure 00000111

Figure 00000112

Figure 00000113

Figure 00000114

Figure 00000115

Figure 00000116

Figure 00000117

Figure 00000118

6. The composition according to claim 5, characterized in that the direct cationic dyes of formula III are selected from among the compounds corresponding to structures III 4, III 5 and III 13. 7. Композиция по п.1, отличающаяся тем, что прямые катионные красители формулы III' выбраны из числа соединений, отвечающих приведенным ниже структурам III' 1 и III' 3:
Figure 00000119

Figure 00000120

Figure 00000121

8. Композиция по одному из предыдущих пунктов, отличающаяся тем, что прямой катионный краситель или красители формул I, II, III или III' составляют 0,001 - 10% от общей массы композиции.7. The composition according to claim 1, characterized in that the direct cationic dyes of the formula III 'are selected from among the compounds corresponding to the structures III' 1 and III '3 below:
Figure 00000119

Figure 00000120

Figure 00000121

8. Composition according to one of the preceding paragraphs, characterized in that the direct cationic dye or dyes of formulas I, II, III or III 'are 0.001 - 10% of the total weight of the composition. 9. Композиция по п.8, отличающаяся тем, что прямые катионные красители формул I, II, III или III' составляют 0,005 - 5% от общей массы композиции. 9. The composition according to claim 8, characterized in that the direct cationic dyes of the formulas I, II, III or III 'are 0.005 - 5% by weight of the total composition. 10. Композиция по одному из предыдущих пунктов, отличающаяся тем, что полиол и/или простой алифатический С1-С8-эфир С3-С9-полиола и/или простой ароматический С6-С8-эфир С2-С9-полиола составляют 0,1 - 40% от общей массы композиции.10. Composition according to one of the preceding paragraphs, characterized in that the polyol and / or simple aliphatic C 1 -C 8 -ether C 3 -C 9 -polyol and / or simple aromatic C 6 -C 8 -ether C 2 -C 9 polyols comprise 0.1 to 40% by weight of the total composition. 11. Композиция по п.10, отличающаяся тем, что полиол и/или простой алифатический С1-С8-эфир С3-С9-полиола и/или простой ароматический С6-С8-эфир С2-С9-полиола составляют 0,5 - 20% от общей массы композиции.11. The composition according to claim 10, characterized in that the polyol and / or simple aliphatic C 1 -C 8 the ether With 3 -C 9 -polyol and / or simple aromatic C 6 -C 8 the ether With 2 -C 9 - polyol is 0.5 to 20% of the total weight of the composition. 12. Композиция по одному из предыдущих пунктов, отличающаяся тем, что она дополнительно содержит дополнительные прямые красители. 12. Composition according to one of the preceding paragraphs, characterized in that it additionally contains additional direct dyes. 13. Композиция по любому из предыдущих пунктов, отличающаяся тем, что пригодная для окрашивания кератиновых волокон среда (носитель) состоит из смеси воды с по меньшей мере одним растворителем из числа полиолов и/или простых эфиров подполов, определенных в п.1. 13. Composition according to any one of the preceding paragraphs, characterized in that the medium (carrier) suitable for dyeing keratin fibers consists of a mixture of water with at least one solvent from among polyols and / or ethers of subfields as defined in claim 1. 14. Композиция по п.13, отличающаяся тем, что среда дополнительно содержит по меньшей мере один органический растворитель. 14. The composition according to p. 13, characterized in that the medium further comprises at least one organic solvent. 15. Композиция по одному из предыдущих пунктов, отличающаяся тем, что она имеет 2 - 11, преимущественно 5 - 10. 15. Composition according to one of the preceding paragraphs, characterized in that it has 2 to 11, preferably 5 to 10. 16. Композиция по одному из предыдущих пунктов, отличающаяся тем, что она предназначена для прямого осветляющего окрашивания и содержит по меньшей мере один окислительный агент. 16. Composition according to one of the preceding paragraphs, characterized in that it is intended for direct lightening staining and contains at least one oxidizing agent. 17. Способ прямого окрашивания кератиновых волокон, в частности, кератиновых волокон человека таких как волосы, отличающийся тем, что на волокна наносят по меньшей мере одну красящую композицию по одному из пп.1-15, на время, достаточное для проявления желаемой окраски, после чего волокна ополаскивают, моют в некоторых случаях шампунем, вновь ополаскивают и сушат. 17. A method of direct dyeing of keratin fibers, in particular, human keratin fibers such as hair, characterized in that at least one dye composition in accordance with one of claims 1 to 15 is applied to the fibers for a time sufficient for the desired color to develop, after which the fibers are rinsed, washed in some cases with shampoo, rinsed again and dried. 18. Способ прямого окрашивания кератиновых волокон, в частности, кератиновых волокон человека таких как волосы, отличающийся тем, что на волокна наносят по меньшей мере одну красящую композицию по одному из пп.1-15, на время, достаточное для проявления желаемой окраски, без последующего ополаскивания. 18. A method of direct dyeing keratin fibers, in particular, human keratin fibers such as hair, characterized in that at least one dye composition in accordance with one of claims 1 to 15 is applied to the fibers for a time sufficient for the desired color to develop, without subsequent rinsing. 19. Способ прямого окрашивания кератиновых волокон, в частности, кератиновых волокон человека таких как волосы, отличающийся тем, что он включает предварительную стадию, состоящую в раздельном хранении, с одной стороны, композиции А, содержащей в пригодной для окрашивания среде по меньшей мере один прямой катионный краситель из числа красителей определенных в предыдущих пунктах и, о другой стороны, композиции В, содержащей в пригодной для окрашивания среде, по меньшей мере один окислительный агент, не относящийся к числу оксидаз и/или оксидоредуктаз, после чего непосредственно перед употреблением производится смешение композиций, причем либо композиция А либо композиция В содержит полиол и/или простой эфир полиола, определенный в п. 1. 19. A method of direct dyeing keratin fibers, in particular, human keratin fibers such as hair, characterized in that it includes a preliminary stage consisting in separate storage, on the one hand, of composition A containing at least one direct medium suitable for dyeing cationic dye from the number of dyes defined in the preceding paragraphs and, on the other hand, the composition B containing, in a suitable medium for dyeing, at least one oxidizing agent not related to oxidase and / or hydroxy oreduktaz, then immediately prior to use the compositions produced mixture, wherein either composition A or composition B comprises a polyol and / or polyol ether as defined in claim. 1. 20. Устройство с несколькими отделениями, или красильный "набор" с несколькими отделениями, отличающееся тем, что первое отделение содержит композицию А, определенную в п.19, и второе отделение содержит композицию В, определенную в п.19. 20. A device with several compartments, or a dye "kit" with several compartments, characterized in that the first compartment contains composition A, as defined in paragraph 19, and the second compartment contains composition B, as defined in paragraph 19.
RU99111265/14A 1998-05-28 1999-05-27 Composition for direct coloring of keratin fibers, particularly, man's hair, method of its coloring, packaging of set for coloring composition RU2166930C2 (en)

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Application Number Priority Date Filing Date Title
FR9806751A FR2779055B1 (en) 1998-05-28 1998-05-28 DIRECT DYE COMPOSITION FOR KERATINIC FIBERS WITH CATIONIC DIRECT DYE AND POLYOL AND / OR POLYOL ETHER
FR9806751 1998-05-28

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RU99111265A true RU99111265A (en) 2001-03-27
RU2166930C2 RU2166930C2 (en) 2001-05-20

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