RU2749036C2 - Способ производства ксилолов и фенола из полученных из угля жидкостей - Google Patents

Способ производства ксилолов и фенола из полученных из угля жидкостей Download PDF

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RU2749036C2
RU2749036C2 RU2019131139A RU2019131139A RU2749036C2 RU 2749036 C2 RU2749036 C2 RU 2749036C2 RU 2019131139 A RU2019131139 A RU 2019131139A RU 2019131139 A RU2019131139 A RU 2019131139A RU 2749036 C2 RU2749036 C2 RU 2749036C2
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stream
zone
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phenols
phenol
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RU2019131139A
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RU2019131139A (ru
RU2019131139A3 (ja
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Лубо ЧЖОУ
Шугуан Чжан
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Чайна Петролеум Энд Кемикал Корпорейшн
Юоп Ллс
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C6/00Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions
    • C07C6/08Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond
    • C07C6/12Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring
    • C07C6/126Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring of more than one hydrocarbon
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02Monocyclic hydrocarbons
    • C07C15/067C8H10 hydrocarbons
    • C07C15/08Xylenes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/48Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by exchange of hydrocarbon groups, which may be substituted, from the same of other compounds, e.g. transalkylation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/50Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions decreasing the number of carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/74Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/02Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
    • C07C39/04Phenol
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C6/00Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions
    • C07C6/08Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond
    • C07C6/12Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/04Purification; Separation; Use of additives by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/12Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/14Purification; Separation; Use of additives by crystallisation; Purification or separation of the crystals
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/06Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
    • C10G21/12Organic compounds only
    • C10G21/16Oxygen-containing compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
RU2019131139A 2017-11-21 2017-11-21 Способ производства ксилолов и фенола из полученных из угля жидкостей RU2749036C2 (ru)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/US2017/062827 WO2019103726A1 (en) 2017-11-21 2017-11-21 Process for making xylenes and phenol from coal derived liquids

Publications (3)

Publication Number Publication Date
RU2019131139A RU2019131139A (ru) 2021-04-05
RU2019131139A3 RU2019131139A3 (ja) 2021-04-05
RU2749036C2 true RU2749036C2 (ru) 2021-06-03

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RU2019131139A RU2749036C2 (ru) 2017-11-21 2017-11-21 Способ производства ксилолов и фенола из полученных из угля жидкостей

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Country Link
US (1) US10723675B2 (ja)
EP (1) EP3713906B1 (ja)
JP (1) JP7025443B2 (ja)
CN (1) CN110914229B (ja)
RU (1) RU2749036C2 (ja)
WO (1) WO2019103726A1 (ja)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7320066B2 (ja) * 2019-02-04 2023-08-02 チャイナ・ペトロリアム・アンド・ケミカル・コーポレーション フェノールおよびキシレンを製造するためのプロセス
WO2021101557A1 (en) * 2019-11-22 2021-05-27 Uop Llc Process for treating coal derived liquids by separate processing of polar and non-polar compounds
US20230286889A1 (en) 2020-09-30 2023-09-14 Uop Llc Transalkylation of alkylated phenols
WO2023063973A1 (en) 2021-10-14 2023-04-20 Uop Llc Process for producing cresol and xylene
WO2023177449A1 (en) 2022-03-17 2023-09-21 Uop Llc An integrated process to produce phenol from coal derived liquid

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2683763A (en) * 1952-09-30 1954-07-13 Standard Oil Co Refining with hf and cbf5
GB1232027A (ja) * 1967-08-16 1971-05-19
US4041091A (en) * 1976-02-19 1977-08-09 Uop Inc. Fractionation of aromatic streams
EA018886B1 (ru) * 2007-12-12 2013-11-29 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. Способ конверсии этана или смешанных низших алканов в ароматические углеводороды
WO2016012103A1 (en) * 2014-07-24 2016-01-28 L'air Liquide Societe Anonyme Pour L'etude Et L' Exploitation Des Procedes Georges Claude Process for separating phenols and btx aromatics from gas condensate

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2838763A (en) 1955-02-17 1958-06-17 John R Brennan Brushing device
US3284514A (en) 1962-12-19 1966-11-08 Gulf Research Development Co Process for the hydrodealkylation of a polyalkylated phenol
US4191844A (en) 1978-05-04 1980-03-04 Phillips Petroleum Company Hydrodealkylation process and catalyst
US4205017A (en) 1978-06-19 1980-05-27 Phillips Petroleum Company Hydrodehydroxylation process using a rhenium-fluorided alumina catalyst
US4230895A (en) 1978-11-30 1980-10-28 Hydrocarbon Research, Inc. Thermal hydrodealkylation of alkyl phenols
US4431850A (en) 1981-11-09 1984-02-14 Hri, Inc. Low temperature hydrodealkylation of alkylated phenols
US4605790A (en) 1985-05-21 1986-08-12 E. I. Du Pont De Nemours And Company Phenol from coal and biomass
IT1255264B (it) * 1992-05-22 1995-10-25 Giuseppe Messina Procedimento per il recupero di fenolo da sue miscele contenenti cumene e alfa-metilstirene
AU4077797A (en) * 1996-08-20 1998-03-06 Dow Chemical Company, The Process for the production of alkylated benzenes
US6291724B1 (en) * 1997-09-24 2001-09-18 General Electric Company Suppression of highly alkylated phenols in the catalytic alkylation reaction of phenol
KR20100040936A (ko) * 2007-07-30 2010-04-21 유오피 엘엘씨 공급 원료 처리를 통합한 크실렌 제조 방법 및 장치
CN103596907B (zh) 2011-06-10 2016-04-27 埃克森美孚化学专利公司 对二甲苯的生产
BR112014029716A2 (pt) 2012-05-31 2017-06-27 Exxonmobil Chemical Patents Inc remoção de fenol em processo de recuperação de paraxileno
US20150065768A1 (en) * 2013-08-29 2015-03-05 Uop Llc Systems and methods for xylene isomer production
US9073811B2 (en) * 2013-11-19 2015-07-07 Uop Llc Process for providing aromatics from coal tar
US9079816B2 (en) 2013-11-19 2015-07-14 Uop Llc Process for producing alkylated aromatic compounds
WO2015094500A2 (en) 2013-12-20 2015-06-25 Exxonmobil Chemical Patents Inc. Production of para-xylene
KR101917490B1 (ko) * 2014-06-30 2018-11-09 엑손모빌 케미칼 패턴츠 인코포레이티드 파라-크실렌의 제조 방법
CN105693458B (zh) * 2014-11-28 2019-06-28 神华集团有限责任公司 煤基混合芳烃和煤直接液化石脑油各自生产邻二甲苯和对二甲苯的方法及组合装置
CN106187671B (zh) * 2014-11-28 2019-07-05 神华集团有限责任公司 煤基混合芳烃生产对二甲苯的方法和煤直接液化石脑油生产对二甲苯的方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2683763A (en) * 1952-09-30 1954-07-13 Standard Oil Co Refining with hf and cbf5
GB1232027A (ja) * 1967-08-16 1971-05-19
US4041091A (en) * 1976-02-19 1977-08-09 Uop Inc. Fractionation of aromatic streams
EA018886B1 (ru) * 2007-12-12 2013-11-29 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. Способ конверсии этана или смешанных низших алканов в ароматические углеводороды
WO2016012103A1 (en) * 2014-07-24 2016-01-28 L'air Liquide Societe Anonyme Pour L'etude Et L' Exploitation Des Procedes Georges Claude Process for separating phenols and btx aromatics from gas condensate

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Publication number Publication date
RU2019131139A (ru) 2021-04-05
JP2021504292A (ja) 2021-02-15
JP7025443B2 (ja) 2022-02-24
US20200031741A1 (en) 2020-01-30
CN110914229B (zh) 2023-01-31
EP3713906A1 (en) 2020-09-30
WO2019103726A1 (en) 2019-05-31
CN110914229A (zh) 2020-03-24
US10723675B2 (en) 2020-07-28
EP3713906B1 (en) 2023-04-05
RU2019131139A3 (ja) 2021-04-05

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