RU2541063C2 - Новые осажденные кремниевые кислоты для применения в качестве носителей - Google Patents

Info

Publication number

RU2541063C2

RU2541063C2 RU2011107350/05A RU2011107350A RU2541063C2 RU 2541063 C2 RU2541063 C2 RU 2541063C2 RU 2011107350/05 A RU2011107350/05 A RU 2011107350/05A RU 2011107350 A RU2011107350 A RU 2011107350A RU 2541063 C2 RU2541063 C2 RU 2541063C2

Authority

RU

Russia

Prior art keywords

silicic acid

precipitated silicic

dryer

precipitated

range

Prior art date

2008-08-01

Links

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• Global Dossier
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• 235000012239 silicon dioxide Nutrition 0.000 title claims abstract description 179
• 125000005624 silicic acid group Chemical class 0.000 title claims description 63
• RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims abstract description 114
• 239000002245 particle Substances 0.000 claims abstract description 44
• 239000000126 substance Substances 0.000 claims abstract description 39
• DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims abstract description 37
• 238000000034 method Methods 0.000 claims description 46
• 239000002585 base Substances 0.000 claims description 39
• 238000001035 drying Methods 0.000 claims description 37
• -1 hydroxides alkaline earth metals Chemical class 0.000 claims description 30
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 27
• 238000002360 preparation method Methods 0.000 claims description 18
• 239000000243 solution Substances 0.000 claims description 18
• 239000003637 basic solution Substances 0.000 claims description 13
• 239000007789 gas Substances 0.000 claims description 11
• BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 10
• 239000000203 mixture Substances 0.000 claims description 9
• QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 8
• 239000002535 acidifier Substances 0.000 claims description 8
• 239000000654 additive Substances 0.000 claims description 7
• NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
• 239000002250 absorbent Substances 0.000 claims description 6
• 230000002745 absorbent Effects 0.000 claims description 6
• XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 6
• JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 6
• 238000005507 spraying Methods 0.000 claims description 6
• 239000000725 suspension Substances 0.000 claims description 6
• OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 5
• 239000006185 dispersion Substances 0.000 claims description 5
• 235000019253 formic acid Nutrition 0.000 claims description 5
• 239000007787 solid Substances 0.000 claims description 5
• 239000007921 spray Substances 0.000 claims description 5
• 229910021529 ammonia Inorganic materials 0.000 claims description 4
• 239000000284 extract Substances 0.000 claims description 4
• 239000001763 2-hydroxyethyl(trimethyl)azanium Substances 0.000 claims description 3
• 235000005881 Calendula officinalis Nutrition 0.000 claims description 3
• 235000019743 Choline chloride Nutrition 0.000 claims description 3
• 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
• 229910052799 carbon Inorganic materials 0.000 claims description 3
• SGMZJAMFUVOLNK-UHFFFAOYSA-M choline chloride Chemical compound [Cl-].C[N+](C)(C)CCO SGMZJAMFUVOLNK-UHFFFAOYSA-M 0.000 claims description 3
• 229960003178 choline chloride Drugs 0.000 claims description 3
• 238000007865 diluting Methods 0.000 claims description 3
• 239000004310 lactic acid Substances 0.000 claims description 3
• 235000014655 lactic acid Nutrition 0.000 claims description 3
• 238000002156 mixing Methods 0.000 claims description 3
• 229910052756 noble gas Inorganic materials 0.000 claims description 3
• 150000002835 noble gases Chemical class 0.000 claims description 3
• 235000011007 phosphoric acid Nutrition 0.000 claims description 3
• 239000000419 plant extract Substances 0.000 claims description 3
• 235000019260 propionic acid Nutrition 0.000 claims description 3
• IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 3
• 239000011550 stock solution Substances 0.000 claims description 3
• BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 2
• 229920000877 Melamine resin Polymers 0.000 claims description 2
• 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
• 229910000272 alkali metal oxide Inorganic materials 0.000 claims description 2
• 229910000287 alkaline earth metal oxide Inorganic materials 0.000 claims description 2
• 150000003973 alkyl amines Chemical class 0.000 claims description 2
• 150000001412 amines Chemical class 0.000 claims description 2
• 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
• 239000003973 paint Substances 0.000 claims description 2
• 239000002966 varnish Substances 0.000 claims description 2
• QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims 1
• 240000000785 Tagetes erecta Species 0.000 claims 1
• 229940022663 acetate Drugs 0.000 claims 1
• 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
• 150000003712 vitamin E derivatives Chemical class 0.000 claims 1
• 230000000694 effects Effects 0.000 abstract description 3
• 239000007788 liquid Substances 0.000 description 16
• 238000005259 measurement Methods 0.000 description 14
• 239000000463 material Substances 0.000 description 13
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 12
• 230000000052 comparative effect Effects 0.000 description 11
• 230000008569 process Effects 0.000 description 10
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
• 239000013543 active substance Substances 0.000 description 9
• 239000000969 carrier Substances 0.000 description 9
• 238000002604 ultrasonography Methods 0.000 description 8
• 238000010521 absorption reaction Methods 0.000 description 7
• 239000000047 product Substances 0.000 description 7
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
• 239000003921 oil Substances 0.000 description 6
• 229940088594 vitamin Drugs 0.000 description 6
• 235000013343 vitamin Nutrition 0.000 description 6
• 239000011782 vitamin Substances 0.000 description 6
• 229930003231 vitamin Natural products 0.000 description 6
• 239000006096 absorbing agent Substances 0.000 description 5
• 238000012937 correction Methods 0.000 description 5
• 238000009826 distribution Methods 0.000 description 5
• 229910052500 inorganic mineral Inorganic materials 0.000 description 5
• 238000004519 manufacturing process Methods 0.000 description 5
• 239000011707 mineral Substances 0.000 description 5
• 235000010755 mineral Nutrition 0.000 description 5
• 239000011148 porous material Substances 0.000 description 5
• 239000000377 silicon dioxide Substances 0.000 description 5
• 150000001413 amino acids Chemical class 0.000 description 4
• 239000003674 animal food additive Substances 0.000 description 4
• 239000002537 cosmetic Substances 0.000 description 4
• VYFYYTLLBUKUHU-UHFFFAOYSA-N dopamine Chemical compound NCCC1=CC=C(O)C(O)=C1 VYFYYTLLBUKUHU-UHFFFAOYSA-N 0.000 description 4
• 239000011521 glass Substances 0.000 description 4
• 238000004898 kneading Methods 0.000 description 4
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• 235000001014 amino acid Nutrition 0.000 description 3
• 238000004458 analytical method Methods 0.000 description 3
• 230000008901 benefit Effects 0.000 description 3
• 230000015572 biosynthetic process Effects 0.000 description 3
• 238000006243 chemical reaction Methods 0.000 description 3
• 235000013305 food Nutrition 0.000 description 3
• 230000003287 optical effect Effects 0.000 description 3
• 150000007524 organic acids Chemical class 0.000 description 3
• 235000005985 organic acids Nutrition 0.000 description 3
• 239000004094 surface-active agent Substances 0.000 description 3
• 238000005406 washing Methods 0.000 description 3
• KWTSXDURSIMDCE-QMMMGPOBSA-N (S)-amphetamine Chemical compound C[C@H](N)CC1=CC=CC=C1 KWTSXDURSIMDCE-QMMMGPOBSA-N 0.000 description 2
• OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical compound OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 description 2
• GHOSNRCGJFBJIB-UHFFFAOYSA-N Candesartan cilexetil Chemical compound C=12N(CC=3C=CC(=CC=3)C=3C(=CC=CC=3)C3=NNN=N3)C(OCC)=NC2=CC=CC=1C(=O)OC(C)OC(=O)OC1CCCCC1 GHOSNRCGJFBJIB-UHFFFAOYSA-N 0.000 description 2
• OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
• ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 description 2
• AOJJSUZBOXZQNB-TZSSRYMLSA-N Doxorubicin Chemical compound O([C@H]1C[C@@](O)(CC=2C(O)=C3C(=O)C=4C=CC=C(C=4C(=O)C3=C(O)C=21)OC)C(=O)CO)[C@H]1C[C@H](N)[C@H](O)[C@H](C)O1 AOJJSUZBOXZQNB-TZSSRYMLSA-N 0.000 description 2
• UGJMXCAKCUNAIE-UHFFFAOYSA-N Gabapentin Chemical compound OC(=O)CC1(CN)CCCCC1 UGJMXCAKCUNAIE-UHFFFAOYSA-N 0.000 description 2
• HTTJABKRGRZYRN-UHFFFAOYSA-N Heparin Chemical compound OC1C(NC(=O)C)C(O)OC(COS(O)(=O)=O)C1OC1C(OS(O)(=O)=O)C(O)C(OC2C(C(OS(O)(=O)=O)C(OC3C(C(O)C(O)C(O3)C(O)=O)OS(O)(=O)=O)C(CO)O2)NS(O)(=O)=O)C(C(O)=O)O1 HTTJABKRGRZYRN-UHFFFAOYSA-N 0.000 description 2
• WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
• RJKFOVLPORLFTN-LEKSSAKUSA-N Progesterone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H](C(=O)C)[C@@]1(C)CC2 RJKFOVLPORLFTN-LEKSSAKUSA-N 0.000 description 2
• YASAKCUCGLMORW-UHFFFAOYSA-N Rosiglitazone Chemical compound C=1C=CC=NC=1N(C)CCOC(C=C1)=CC=C1CC1SC(=O)NC1=O YASAKCUCGLMORW-UHFFFAOYSA-N 0.000 description 2
• 229910000831 Steel Inorganic materials 0.000 description 2
• 241000736851 Tagetes Species 0.000 description 2
• 239000002253 acid Substances 0.000 description 2
• 150000007513 acids Chemical class 0.000 description 2
• 239000004480 active ingredient Substances 0.000 description 2
• OIRDTQYFTABQOQ-KQYNXXCUSA-N adenosine Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](CO)[C@@H](O)[C@H]1O OIRDTQYFTABQOQ-KQYNXXCUSA-N 0.000 description 2
• 230000000844 anti-bacterial effect Effects 0.000 description 2
• 125000003118 aryl group Chemical group 0.000 description 2
• CUFNKYGDVFVPHO-UHFFFAOYSA-N azulene Chemical compound C1=CC=CC2=CC=CC2=C1 CUFNKYGDVFVPHO-UHFFFAOYSA-N 0.000 description 2
• 238000004140 cleaning Methods 0.000 description 2
• 230000001143 conditioned effect Effects 0.000 description 2
• 230000003750 conditioning effect Effects 0.000 description 2
• ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 description 2
• ADEBPBSSDYVVLD-UHFFFAOYSA-N donepezil Chemical compound O=C1C=2C=C(OC)C(OC)=CC=2CC1CC(CC1)CCN1CC1=CC=CC=C1 ADEBPBSSDYVVLD-UHFFFAOYSA-N 0.000 description 2
• 229960003638 dopamine Drugs 0.000 description 2
• 239000000428 dust Substances 0.000 description 2
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• 230000000855 fungicidal effect Effects 0.000 description 2
• JYGXADMDTFJGBT-VWUMJDOOSA-N hydrocortisone Chemical compound O=C1CC[C@]2(C)[C@H]3[C@@H](O)C[C@](C)([C@@](CC4)(O)C(=O)CO)[C@@H]4[C@@H]3CCC2=C1 JYGXADMDTFJGBT-VWUMJDOOSA-N 0.000 description 2
• 230000002209 hydrophobic effect Effects 0.000 description 2
• CGIGDMFJXJATDK-UHFFFAOYSA-N indomethacin Chemical compound CC1=C(CC(O)=O)C2=CC(OC)=CC=C2N1C(=O)C1=CC=C(Cl)C=C1 CGIGDMFJXJATDK-UHFFFAOYSA-N 0.000 description 2
• NOESYZHRGYRDHS-UHFFFAOYSA-N insulin Chemical compound N1C(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(NC(=O)CN)C(C)CC)CSSCC(C(NC(CO)C(=O)NC(CC(C)C)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CCC(N)=O)C(=O)NC(CC(C)C)C(=O)NC(CCC(O)=O)C(=O)NC(CC(N)=O)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CSSCC(NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2C=CC(O)=CC=2)NC(=O)C(CC(C)C)NC(=O)C(C)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2NC=NC=2)NC(=O)C(CO)NC(=O)CNC2=O)C(=O)NCC(=O)NC(CCC(O)=O)C(=O)NC(CCCNC(N)=N)C(=O)NCC(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC(O)=CC=3)C(=O)NC(C(C)O)C(=O)N3C(CCC3)C(=O)NC(CCCCN)C(=O)NC(C)C(O)=O)C(=O)NC(CC(N)=O)C(O)=O)=O)NC(=O)C(C(C)CC)NC(=O)C(CO)NC(=O)C(C(C)O)NC(=O)C1CSSCC2NC(=O)C(CC(C)C)NC(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CC(N)=O)NC(=O)C(NC(=O)C(N)CC=1C=CC=CC=1)C(C)C)CC1=CN=CN1 NOESYZHRGYRDHS-UHFFFAOYSA-N 0.000 description 2
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• 239000007800 oxidant agent Substances 0.000 description 2
• HYAFETHFCAUJAY-UHFFFAOYSA-N pioglitazone Chemical compound N1=CC(CC)=CC=C1CCOC(C=C1)=CC=C1CC1C(=O)NC(=O)S1 HYAFETHFCAUJAY-UHFFFAOYSA-N 0.000 description 2
• PDEDQSAFHNADLV-UHFFFAOYSA-M potassium;disodium;dinitrate;nitrite Chemical compound [Na+].[Na+].[K+].[O-]N=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O PDEDQSAFHNADLV-UHFFFAOYSA-M 0.000 description 2
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