RU2080087C1 - Способ сушки и гранулирования аспартама - Google Patents
Способ сушки и гранулирования аспартама Download PDFInfo
- Publication number
- RU2080087C1 RU2080087C1 SU5052488/13A SU5052488A RU2080087C1 RU 2080087 C1 RU2080087 C1 RU 2080087C1 SU 5052488/13 A SU5052488/13 A SU 5052488/13A SU 5052488 A SU5052488 A SU 5052488A RU 2080087 C1 RU2080087 C1 RU 2080087C1
- Authority
- RU
- Russia
- Prior art keywords
- aspartame
- drying
- crystals
- moisture content
- wet mass
- Prior art date
Links
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 title claims abstract description 60
- 238000000034 method Methods 0.000 title claims abstract description 40
- 238000001035 drying Methods 0.000 title claims abstract description 33
- 238000005469 granulation Methods 0.000 title abstract 3
- 230000003179 granulation Effects 0.000 title abstract 3
- 239000013078 crystal Substances 0.000 claims abstract description 29
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 108010011485 Aspartame Proteins 0.000 claims description 57
- 235000010357 aspartame Nutrition 0.000 claims description 57
- 239000000605 aspartame Substances 0.000 claims description 57
- 229960003438 aspartame Drugs 0.000 claims description 57
- 239000002245 particle Substances 0.000 claims description 20
- 239000000843 powder Substances 0.000 claims description 6
- 230000002906 microbiologic effect Effects 0.000 claims description 4
- 244000005700 microbiome Species 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 239000002826 coolant Substances 0.000 claims 3
- 238000011169 microbiological contamination Methods 0.000 claims 1
- 239000008187 granular material Substances 0.000 abstract description 36
- 239000012159 carrier gas Substances 0.000 abstract description 10
- 239000000126 substance Substances 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 2
- 238000007669 thermal treatment Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 18
- 238000009826 distribution Methods 0.000 description 8
- 238000000354 decomposition reaction Methods 0.000 description 6
- 239000000428 dust Substances 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 238000012546 transfer Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 229920001817 Agar Polymers 0.000 description 2
- 239000008272 agar Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 241000193755 Bacillus cereus Species 0.000 description 1
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229930195725 Mannitol Natural products 0.000 description 1
- 108010040201 Polymyxins Proteins 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 235000013345 egg yolk Nutrition 0.000 description 1
- 210000002969 egg yolk Anatomy 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000000594 mannitol Substances 0.000 description 1
- 235000010355 mannitol Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 235000020030 perry Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07K—PEPTIDES
- C07K5/00—Peptides containing up to four amino acids in a fully defined sequence; Derivatives thereof
- C07K5/04—Peptides containing up to four amino acids in a fully defined sequence; Derivatives thereof containing only normal peptide links
- C07K5/06—Dipeptides
- C07K5/06104—Dipeptides with the first amino acid being acidic
- C07K5/06113—Asp- or Asn-amino acid
- C07K5/06121—Asp- or Asn-amino acid the second amino acid being aromatic or cycloaliphatic
- C07K5/0613—Aspartame
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/10—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic in stationary drums or troughs, provided with kneading or mixing appliances
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
- F26B17/12—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed solely by gravity, i.e. the material moving through a substantially vertical drying enclosure, e.g. shaft
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
- F26B17/18—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by rotating helical blades or other rotary conveyors which may be heated moving materials in stationary chambers, e.g. troughs
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- General Health & Medical Sciences (AREA)
- Biophysics (AREA)
- Genetics & Genomics (AREA)
- Medicinal Chemistry (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Polymers & Plastics (AREA)
- Seasonings (AREA)
- Peptides Or Proteins (AREA)
- Drying Of Solid Materials (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Plural Heterocyclic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL9101477A NL9101477A (nl) | 1991-09-02 | 1991-09-02 | Werkwijze voor het drogen en granuleren van aspartaam. |
| NL9101477 | 1991-09-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2080087C1 true RU2080087C1 (ru) | 1997-05-27 |
Family
ID=19859657
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU5052488/13A RU2080087C1 (ru) | 1991-09-02 | 1992-09-01 | Способ сушки и гранулирования аспартама |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US5355590A (enExample) |
| EP (1) | EP0530903B1 (enExample) |
| KR (1) | KR100229951B1 (enExample) |
| AT (1) | ATE153030T1 (enExample) |
| AU (1) | AU650997B2 (enExample) |
| BR (1) | BR9203423A (enExample) |
| CA (1) | CA2077198A1 (enExample) |
| DE (1) | DE69219703T2 (enExample) |
| MX (1) | MX9204998A (enExample) |
| NL (1) | NL9101477A (enExample) |
| RU (1) | RU2080087C1 (enExample) |
| TW (1) | TW283096B (enExample) |
| ZA (1) | ZA926618B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2430097C2 (ru) * | 2006-01-30 | 2011-09-27 | Вомм Импианти Е Процесси С.П.А. | Способ сушки меламина |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3165700B2 (ja) * | 1993-11-12 | 2001-05-14 | 三菱東京製薬株式会社 | 高速攪拌造粒法及び高速攪拌造粒機 |
| EP1491253A1 (en) * | 2003-06-26 | 2004-12-29 | Urea Casale S.A. | Fluid bed granulation process and apparatus |
| GB0607926D0 (en) | 2006-04-21 | 2006-05-31 | Mars Inc | Process for the production of crumb |
| US20070286903A1 (en) * | 2006-06-13 | 2007-12-13 | Becicka Brian T | Composition and method for taste masking |
| US7908765B2 (en) * | 2006-12-22 | 2011-03-22 | Collette Nv | Continuous granulating and drying apparatus |
| RU209574U1 (ru) * | 2021-10-12 | 2022-03-17 | Общество с ограниченной ответственностью "СплавТехКомплект" | Сушильно-грануляционная установка |
| CN113845506B (zh) * | 2021-10-18 | 2022-09-23 | 惠州市宙邦化工有限公司 | 一种碳酸乙烯酯的动态结晶提纯方法 |
| CN118548659B (zh) * | 2024-07-29 | 2024-10-11 | 江苏太湖新材料控股有限公司 | 一种对叔丁基邻苯二酚溶液制备用原料流化床干燥机 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1127815B (de) * | 1957-09-10 | 1962-04-12 | Alpine Ag Maschinenfabrik | Vorrichtung zum kontinuierlichen Trocknen pulverfoermigen bis koernigen Gutes |
| JPH07103154B2 (ja) * | 1986-08-13 | 1995-11-08 | 東ソー株式会社 | 安定なα−L−アスパルチル−L−フエニルアラニンメチルエステルの製造方法 |
| AU620816B2 (en) * | 1987-07-29 | 1992-02-27 | Nutrasweet Company, The | Self stabilized dipeptide sweeteners |
| US4875435A (en) * | 1988-02-24 | 1989-10-24 | Warner-Lambert Company | Fluidized bed dryer/granulator |
| US4967688A (en) * | 1989-06-09 | 1990-11-06 | Fuji Sangyo Company, Limited | Powder processing apparatus |
| US5271163A (en) * | 1992-10-05 | 1993-12-21 | Bepex Corporation | System for treating flowable materials |
-
1991
- 1991-09-02 NL NL9101477A patent/NL9101477A/nl not_active Application Discontinuation
-
1992
- 1992-07-17 US US07/914,239 patent/US5355590A/en not_active Expired - Lifetime
- 1992-08-13 TW TW081106405A patent/TW283096B/zh active
- 1992-08-27 EP EP92202607A patent/EP0530903B1/en not_active Expired - Lifetime
- 1992-08-27 DE DE69219703T patent/DE69219703T2/de not_active Expired - Fee Related
- 1992-08-27 AT AT92202607T patent/ATE153030T1/de not_active IP Right Cessation
- 1992-08-31 MX MX9204998A patent/MX9204998A/es unknown
- 1992-08-31 CA CA002077198A patent/CA2077198A1/en not_active Abandoned
- 1992-09-01 ZA ZA926618A patent/ZA926618B/xx unknown
- 1992-09-01 RU SU5052488/13A patent/RU2080087C1/ru not_active IP Right Cessation
- 1992-09-01 AU AU22043/92A patent/AU650997B2/en not_active Ceased
- 1992-09-01 BR BR929203423A patent/BR9203423A/pt not_active Application Discontinuation
- 1992-09-02 KR KR1019920015891A patent/KR100229951B1/ko not_active Expired - Fee Related
Non-Patent Citations (1)
| Title |
|---|
| 1. Патент ЕРВ N 0256515, Мкл. С О7 К 5/06, 1988. * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2430097C2 (ru) * | 2006-01-30 | 2011-09-27 | Вомм Импианти Е Процесси С.П.А. | Способ сушки меламина |
Also Published As
| Publication number | Publication date |
|---|---|
| BR9203423A (pt) | 1993-04-06 |
| DE69219703T2 (de) | 1997-12-11 |
| NL9101477A (nl) | 1993-04-01 |
| AU650997B2 (en) | 1994-07-07 |
| ZA926618B (en) | 1993-03-25 |
| AU2204392A (en) | 1993-03-11 |
| MX9204998A (es) | 1993-03-01 |
| EP0530903A1 (en) | 1993-03-10 |
| TW283096B (enExample) | 1996-08-11 |
| US5355590A (en) | 1994-10-18 |
| DE69219703D1 (de) | 1997-06-19 |
| KR930005554A (ko) | 1993-04-20 |
| EP0530903B1 (en) | 1997-05-14 |
| KR100229951B1 (ko) | 1999-11-15 |
| ATE153030T1 (de) | 1997-05-15 |
| CA2077198A1 (en) | 1993-03-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20030902 |